• Journal of Ceramic Processing Research
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• v.20 no.5
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• pp.499-504
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• 2019

The effect of coating thickness on the contact fatigue and wear of thermal barrier coatings (TBCs) are investigated in this study. The same bondcoat material thickness (250 ㎛) are used for each sample, which allows the effect of the coating thickness of the topcoat to be investigated. TBCs with different coating thicknesses (200, 400, and 600 ㎛) are prepared by changing processing parameters such as the feeding rate of the feedstock, spraying speed, and spraying distance during APS(air plasma spray) coating. The damage size on the surface are strongly affected by the coating thickness effect. Although the damage size from contact fatigue using a spherical indenter diminish at a TBC of 200 ㎛, a high wear resistance such as a low friction coefficient and little mass change are found at a TBC of 600 ㎛. These results indicate that the coating thickness strongly affects the mechanical behavior in TBCs during gas turbine operation.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 2002.04a
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• pp.43-47
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• 2002

In this study, through the experimental results of grinding ratio, grinding force and surface roughness with the obtained wear amount of diamond wheel and ceramic material during the grinding process, the following conclusions could be found. In the case of $Si_3N_4$, the wear of diamond wheel is large while the grinding force is stable and the range of change in surface roughness is small. for the case of $AL_2O_3$ and $ZrO_3$, while the wear of diamond wheel is getting smaller, the grinding force is increasing but the value of surface roughness is decreasing. For grinding with the vitrified bond wheel, it seems that the self-sharpening can be found for $Si_3N_4$ and the glazing effect of the cutting edge for $AL_2O_3$ and $ZrO_3$.

• Tribology and Lubricants
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• v.18 no.5
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• pp.324-332
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• 2002

In order to enhance the thermal stability of binder materials of bonded type solid lubricants, several metal-alkoxide based sol-gel materials such as methyltrimethoxysilane(MTMOS), titaniumisopropoxide$(Ti(Opr^i)_4),$ zirconiumisopropoxide $(Zr(Opr^i)_4)$ and aluminumbutoxide$(Al(Obu^t)_4)$ were chemically modified by epoxy-, acrylic- and fluoro-silane compounds, respectively. Friction and wear characteristics of these hybrid ceramic materials were tested with a micro tribo-tester, and evaluated with respect to both heat-curing temperature and the time. Test results generally showed that hybrid ceramic materials modified by epoxy-silane compounds had a low friction compared to others. And the higher het-curing temperature and the longer heat treatment time resulted in the higher friction and the lower wear. IR spectroscopic analyses revealed that these results were caused mainly by the increased metal oxide content in hybrid ceramics when the heat-curing temperature was over $320^{\circ}C.$

• Proceedings of the Korean Society For Composite Materials Conference
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• 1999.11a
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• pp.239-241
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• 1999

Recently, the friction and wear behaviors of UHMWPE, ceramic and metal is being researched actively for the use as an artificial hip-joint. In this study, because of good wear properties of carbon fiber, we made experiments about the friction and wear of carbon fiber reinforced epoxy composite under the lubricative and the dry condition. The possibilities of carbon-carbon composite for the artificial hip joint application was studied from this results.

• Journal of the Korean Ceramic Society
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• v.31 no.9
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• pp.1069-1075
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• 1994

When ceramics are used as the parts of an engine and a machine, the tribological properties are very important. For the preparation of the resistance material for wear applications by the method of Reaction-Bonded Sintering, metal silicon and carbon black are mixed up into SiC powder, and Al2O3 and Fe2O3 are put as an additive. As the general properties, the bending strength and water absortion are measured in the normal temperature and the phase changies are investigated with XRD. The property of the resistance for wear applications is measured with the amount of friction and wear, friction coefficient and maximum asperties. And, the surface of wear is observed with SEM. With the results of this study, the optimal mol ratio of Si : C and the suitable quantity of the mixture of SiC are 7 : 3 and 40 wt%, respectively. In the case of the addition of Al2O3 (2 wt%), the resistance for friction and wear applications is prominent. The bending strength showed the highest peak when Al2O3 (4 wt%) and Fe2O3 (4 wt%) were added. The properties of friction and wear were related with the propagation velocity of crack rather than the bending strength.

• Journal of the Korean Ceramic Society
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• v.35 no.7
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• pp.740-748
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• 1998

The inertia friction properties of C/C composites manufactured by the processes of pressure and at-mospheric carbonizaton with a commerciallized and two kinds of modified coal-tar pitch as a matrix pre-cursor were investigated. The modifications of a pitch such as the introduction of mesophase and the ad-dition of sulphur into a raw pitch were not effective for a impregnation efficiency conducted in a vacuum and at the same time in a pressure of 5kg/cm2 due to the increase of the pitch viscosity. There was not a difference in the densification increment between the pitch modifications however it was revealed that a pressure carbonization was more advantageous than an atmospheric in the densification and the formation of anisotropic carbon matrix. The friction and wear propertis of C/C having higher degree of matrix cry-stallization higher density and hardness of friction surface showed superiority. As the braking energy was increased the friction coefficients were decreased and reached almost same level at the high kinetic energy of 99.6kJ. The wear trends at 99.6kJ were different from the behaviors of friction ceofficient under the same energy in which an oxidation wear is being considered along with a mechnical wear although the wear rates were almost similar to the friction coefficient at the low energy.

• Journal of the Korean Ceramic Society
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• v.40 no.6
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• pp.525-529
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• 2003

Biotribological properties, such as wear rate and friction coefficient, of 3Y-TZP and Low Temperature Degradation (LTD) free materials were investigated via a ball(SiC)-on-plate sliding wear test to evaluate the relationship between wear mechanism and phase transformation. Wear test was conducted with a sliding speed of 0.035 m/s at room temperature and at 25$0^{\circ}C$ in air under a normal load of 49 N, respectively. Although friction coefficient of 3Y-TZP was the lowest due to the fine grain size, the highest wear loss and rate were observed due to the debris of monoclinic grains introduced during sliding and their values increased drastically with raising temperature. However, the biotribological properties of LTD-free materials were insensitive to temperature due to the inertness of the phase transformation, suggesting that they may be applicable to the biomechanical parts.

• Journal of the Korean Ceramic Society
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• v.46 no.5
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• pp.505-509
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• 2009

In this study, bulk nano-crystalline $Si_3N_4$ ceramics were fabricated by spark plasma sintering (SPS) and their mechanical properties, in particular wear, were investigated. A wide range of grain sizes, from 80 nm and 250 nm were obtained by varying sintering conditions ($1550^{\circ}C$-5 min to $1650^{\circ}C$-20 min). The elastic modulus of obtained ceramics was ${\sim}250$ GPa and hardness was in the range of $13{\sim}14$ GPa. The indentation fracture toughness increased from $2.58MPa{\cdot}m^{1/2}$ to $3.24MPa{\cdot}m^{1/2}$ with increasing sintering temperature possibly due to the elongated grains. Sliding wear tests revealed at least an order magnitude improvement in wear resistance with grain refinement. Microstructure analysis indicated that nano-$Si_3N_4$ specimens worn mainly through delamination and microcracking, while that of coarser specimens revealed severe wear with grain debonding and fracture.

• Journal of the Korean Ceramic Society
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• v.31 no.1
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• pp.25-30
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• 1994

W-Ti-C-N based multiphase hard materials have been prepared from WC/TiN powder mixture. By sintering at and above 190$0^{\circ}C$, the two phases of powder mixture has transformed into intermixed W, W2C and Ti(C, N) phases. For the temperature range between 180$0^{\circ}C$ and 210$0^{\circ}C$, the sintered or hot pressed samples show maximum density and hardness. The seems that metallic W grains enhance the fracture toughness of materials. The wear resistance of the material is found to increase with increasing hardness.

• Journal of the Korean Society for Precision Engineering
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• v.12 no.6
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• pp.112-119
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• 1995

Early fracture and cutting force of ceramic tool for hardened STC3 steel was investigated in this study. It was found that early fracture of ceramic tool was mostly occurred before normal wear was progressed beyond a critical cutting speed and normal wear was performed under the critical cutting speed. The relationships among critical cutting speed, which was a cause of early fracture, suggested cutting cross section, that is, maximum thickness of cut and width of cut, and cutting force were examined. The following conclusions were obtained: (1)Critical cutting speed showed a high value in the case of small maximum thickness of cut and large nose radius, but was not influenced by width of cut, (2)Principal, feed and radial force, respectively, showed the proportional value to constant cutting area, width of cut and maximum thickness of cut orderly, (3)Occurrence of early fracture was dependent upon radial force.