• 제목/요약/키워드: Water solvent

검색결과 2,078건 처리시간 0.028초

전자종이용 티타니아 나노입자의 합성 및 물성 평가 (Synthesis and Characterization of Physical Properties of Titania Nanoparticle for Electronic Paper)

  • 홍성제;한정인
    • 한국전기전자재료학회논문지
    • /
    • 제18권10호
    • /
    • pp.929-935
    • /
    • 2005
  • In this paper, synthetic conditions of titania nanparticle was investigated to enhance its uniformity of the particle size as a child particle on organic mother particle of liquid powder type electronic paper. The physical properties are very important to improve the uniformity of electrical charging properties Concentration of titania raw material ($C_9H_{19}NO_4Ti$) in the ethanol solvent, pH, and concentration of the solution in the D.I. water were selected as parameters. As a result, ultrafine and well crystallized titania nanoparticle with good uniformity could be synthesized as the concentration of the $C_9H_{19}NO_4Ti$ in the ethanol solvent, pH of the solution, and the amount of the D.I. water were increased. Using the optimized conditions, the titania nanparoticle with uniformly ultrafime size of 10 nm could be synthesized.

Micellization of Amphiphilic Random Copolymers in Mixtures of Water and Methanol

  • Mori, Takuya;Hashidzume, Akihito;Sato, Takahiro
    • 한국고분자학회:학술대회논문집
    • /
    • 한국고분자학회 2006년도 IUPAC International Symposium on Advanced Polymers for Emerging Technologies
    • /
    • pp.287-287
    • /
    • 2006
  • Amphiphilic random copolymers can form various types of micelles in aqueous media depending on the balance between two opposite interactions- electrostatic repulsion and hydrophobic attraction. This balance can change by addition of some organic solvent to the aqueous solution, and as a result, we can control the micellar structure and micellization equilibrium by changing the solvent content. In the present study, we have investigated the micellization equilibrium of an amphiphilic statistical copolymer consisting of sodium 2-(acrylamido)-2- methylpropanesulfonate and hexyl methacrylate in mixtures of water and methanol by sedimentation equilibrium and fluorescence.

  • PDF

산초와 초피 잎의 항균활성 (Antimicrobial Activities of Zonthoxylum schinifolium and Zanthoxylum piperitum Leaves)

  • 김정;조영수;서권일;주옥수;심기환
    • 한국식품저장유통학회지
    • /
    • 제7권2호
    • /
    • pp.195-200
    • /
    • 2000
  • Yields of various solvent extracts for Zanthoxylum schinifolium and Z. piperitum leaves were higher in ethanol extract layer. Ethanol Extract in sancho and chopi leaves was fractionated with different solvents, such as hexane, chloroform, ethyl acetate, butanol and water, yields of hexane fraction was higher. In the solvent extracts using methanol, ethanol, hexane, chloroform, and water, ethanol extract showed the most effective antimicrobial activities. Ethanol extract in sancho and chopi leaves was fractionated, the most antimicrobial activities of sancho leaf were ethyl acetate fraction, and chopi leaf were chloroform fraction.

  • PDF

수-유기용매혼합용매중의 산-염기지원약에 관한 연구 (Behaviour of Acid-Base Indicators in the Aqueous Organic Solutions.)

  • 용군호
    • 약학회지
    • /
    • 제19권1호
    • /
    • pp.30-35
    • /
    • 1975
  • pKi values and sensitivity of acid-base indicators in the mixed solvent systems of water-alcohols and water-acetone at differential pH and in concentration media were determined by spectrophotometric method. When the concentration of the organic solvents were increased, the pKi values of sulfophthalein indicators, thymol blue and bromcresol purple, became larger whereas those of an axo indicator, methyl yellow, became smaller nad the pH values of the equivalent points of acids became smaller and the pH values of the equivalent points of acids became higher than those in the aqueous solution. potassium bicarbonate, a standard compound used in the organic solvent systems without a prerequisite procedure of expelling carbon dioxide by boiling.

  • PDF

가미의이인탕(加味薏苡仁湯)의 투염증작용(投炎症作用)에 대(對)한 실험적(實驗的) 연구(硏究) (STUDIES ON THE ANTI-INFLAMMATORY EFFECT OF THE KAMI EUI YEE IN TANG ON RAT)

  • 윤태여
    • 대한한방내과학회지
    • /
    • 제1권1호
    • /
    • pp.64-69
    • /
    • 1976
  • Kami Eui In Tang is being used as a treatment oral medicament on the appendicitis and peritonitis without surgical operation resulting good effect. The component of the medicament are as follow : Coix ma yuen, Paeonia moutan, Patrinia scabiosifolia, Rheum, Coreanum, Cory-dalis nakaii, Trichosanthes kirilowii, Lonicera japonica, Prunus persica, Tarxacum officinale, Author tried to make clear the ant inflammatory effect on rat paw which has become edema formation by carrageenin and detect the active ingredients by thin layer chromatography method. The material was extracted with three kind of solvent; distilled water, 50% ethyl alcohol, and ether which were immersed in material for 48 hours and concentrated to 10ml by evaporation of solvents. The result was as follow: 1. The anti-inflammatory effect of the sample material on the. edema formed at the rat paw was obviously clear. 2. Many spots of active ingredients were detected on the silica gel G plate spotted by ether extracted material than water one. 3. The good developing solvent was the mixture of $CHCl_3$ ; Acetone : Diethylamine (5:4:1).

  • PDF

고체상 추출법을 이용한 Phthalate Esters의 분석방법 연구 (A Study on Analytical Method of Phthalate Esters in Water by SPE(Solid-Phase-Extraction))

  • 홍성희;한개희;이찬형;이순화
    • 한국환경과학회지
    • /
    • 제12권1호
    • /
    • pp.81-86
    • /
    • 2003
  • The study was carried out to evaluate the new analytical method of phthalate esters(diethylphthalate, di-n-butylphthalate, butylbenzylphthalate, bis(2-ethylhexyl)phthalate), one of the endocrine disruptors, which were performed by GC/MS-SIM(selected ion monitoring). The phthalate esters were extracted from water samples using solid-phase extraction on $C_{18}$ columns. It investigated that the extraction recovery rate of phthalate esters with different solvents and solvent volume. The optimal solvent was dichloromethane and proper volume of dichloromethane for recovery of phthalate esters was 4 mL. There were good linearities(above $R^2$=0.9975) in the range 0.01~0.50mg/L, and the detection limits were below 0.01~0.03$\mu\textrm{g}$/L. The recovery rates, RSD and MDLs for phthalate esters were 80~114%, 5.0~8.1% and 0.03~0.11$\mu\textrm{g}$/L, respectively. This method shows a good precision of phthalate esters.

Microwave Heat Dyeing of Polyester Fabric

  • Kim, Sam-Soo;Lee, Su-Gyung m;Ghim, Han-Do;Kim, Joon-Ho;Lyoo, Won-Seok
    • Fibers and Polymers
    • /
    • 제4권4호
    • /
    • pp.204-209
    • /
    • 2003
  • The effect of padding solution on the microwave heat dyeing of polyester fabric was studied extensively. Polyester fabrics were impregnated in aqueous urea solution and aqueous sodium chloride solution for 10 min and then dyed for 7 min by microwave apparatus (2450 MHz, 700 W) under optimum conditions which provide good exhaustion. Aqueous solutions of urea and sodium chloride showed more effective than water as a padding solution for microwave heat dyeing. The type of solvent added in padding media and its concentration significantly affects the K/S values of dyed polyester fabric. Added solvents such as n-hexane, acetone, and dimethyl formamide were also more effective than 100 % water as padding media for the microwave heat dyeing. It is supposed that the effect of used solvents on dyeing property of polyester fabrics depends on the solubility parameter difference between solvent and polyester fabric.

수분무 STS 316L 분말사출성형체의 탈지 및 소결공정에 따른 인장 특성 (Effect of Debinding and Sintering Conditions on the Tensile Properties of Water-atomized STS 316 L Parts by Powder Injection Molding)

  • 윤태식;성환진;안상호;이종수
    • 한국분말재료학회지
    • /
    • 제9권4호
    • /
    • pp.218-226
    • /
    • 2002
  • The purpose of the present study is to investigate the influence of thermal debinding and sintering conditions on the sintering behavior and mechanical properties of PIMed 316L stainless steel. The water atomized powders were mixed with multi-component wax-base binder system, injection molded into flat tensile specimens. Binder was removed by solvent immersion method followed by thermal debinding, which was carried out in air and hydrogen atmospheres. Sintering was done in hydrogen for 1 hour at temperatures ranging from 1000℃ to 1350℃ The weight loss, residual carbon and oxygen contents were monitored at each stage of debinding and sintering processes. Tensile properties of the sintered specimen varied depending on the densification and the characteristics of the grain boundaries, which includes the pore morphology and residual oxides at the boundaries. The sinter density, tensile strength (UTS), and elongation to fracture of the optimized specimen were 95%, 540 MPa, and 53%, respectively.

DNA Damage Protection and Anti-inflammatory Activity of Different Solvent Fractions from Aruncus dioicus var. kamtschaticus

  • Zhang, Qin;Kim, Hye-Young
    • 한국자원식물학회지
    • /
    • 제27권6호
    • /
    • pp.714-719
    • /
    • 2014
  • This study investigated DNA damage protection and anti-inflammatory activity of different solvent fractions from Aruncus dioicus var. kamtschaticus (A. dioicus) aerial parts water extract. As for DNA damage protection, distilled water ($H_2O$) fraction displayed the most powerful protection for DNA damage at a concentration of 1 mg/ml. As for anti-inflammatory activity, dichloromethane ($CH_2Cl_2$) fraction exhibited the highest NO inhibition activity, ranging from 61% to 19% ($10-40{\mu}g/ml$). Furthermore, the levels of pro-inflammatory cytokines mRNA expressions and intracellular reactive oxygen species (ROS) were employed to verify the anti-inflammatory activity of the $CH_2Cl_2$ fraction on further researches. It could be concluded that A. dioicus had a significantly effect of DNA damage protection and anti-inflammatory activity which also as an essential edible vegetable and medicinal species.

생강중 게르마늄 성분에 관한 연구 (Studies on the Germanium Components of Zingiberis Rhizoma)

  • 백남호;박만기;최승호;문동철
    • 약학회지
    • /
    • 제25권4호
    • /
    • pp.193-197
    • /
    • 1981
  • Germanium (Ge) content in Zingiberis Rhizoma was determined by flameless atomic absorption spectrometry with a graphite tube atomizer. The Ge content of the cortical layer was 65.mu.g/g, the central cylinder, $98\mu$g/g and the total, $87\mu$g/g. In the effect of the extraction of Ge by various solvents, polar solvent was more effective than the nonpolar one, Especially, water was the most effective solvent. The water extract of Zingiberis Rhizoma, separated by sephadex G-25 gel filtration, was fractionated into 2 peaks at 254nm. Both the peaks showed atomic absorptions of Ge. It may be concluded that the Ge components of Zingiberis Rbizoma exist as the form of an aqueous organic compounds or associated forms with proteins.

  • PDF