• Title/Summary/Keyword: Water extraction

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Optimization of Macerating Enzymatic Extraction Process and Components Change of Extract of Rubus coreanus Miq. Fruit (복분자의 효소 추출 공정의 최적화 및 성분 변화)

  • Ryu, Il Hwan;Kwon, Tae Oh
    • Korean Journal of Medicinal Crop Science
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    • v.21 no.2
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    • pp.97-104
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    • 2013
  • The objective of this study is to investigate the optimal condition for macerating enzymatic extraction process that leads to the highest yield and the largest extracted amount of bio-active contents from Rubus coreanus Miq. fruit. The optimal extraction conditions were found as the following: The initial amount of the water added to the fruit was 20 ~ 30% by weight. The mixing ratio used for the macerating enzyme was 4 : 1 : 2 (w : w : w) for cellulase:pectinase:amylogucosidase, and the amount of the macerating enzyme added was 2% by weight. The extraction process was done at a temperature of $45{\sim}50^{\circ}C$ for 10 hours. The extraction yields on Rubus coreanus Miq. fruit by macerating enzymatic extraction process was increased by 84.3% compared to that of hot-water extraction process. The amounts of organic acids and vitamin found in the extract were also higher. The amount of polyphenol and anthocyanin contents in the extract were 185% and 257% of those from hot-water extraction, respectively. These results suggest that macerating enzymatic extraction is an effective method to boost extraction yield and to increase the amount of extraction of bio-active contents from Rubus coreanus Miq. fruit.

The Effect of Extraction Conditions and Film Side on the Molecular Conformation of Silk Sericin Film

  • Jo, Yoon Nam;Bae, Do Gyu;Um, In Chul
    • International Journal of Industrial Entomology and Biomaterials
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    • v.26 no.2
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    • pp.113-118
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    • 2013
  • In this study, silk sericin films were prepared using different extraction methods, and the molecular conformation of sericin was examined using Fourier-transform infrared spectroscopy with attenuated total reflection geometry. Additionally, the effect of the film side (air-facing side or plate-facing side) on the molecular conformation of the sericin films was investigated. Interestingly, the molecular conformation of the sericin film depended on the film side. The molecular conformation of air-facing side of the sericin film was significantly influenced by extraction solution and time. The ${\beta}$-sheet crystallization and the crystallinity index of the sericin film markedly increased with an increase in the extraction time in hot water. The order of the crystallinity indices for the sericin films obtained with different extraction solutions was as follows: citric acid solution > urea solution >> hot water. In contrast, no remarkable differences were observed in the molecular conformation of the plate-facing side of the sericin film after extraction in hot water for different time periods. Urea and citric acid solution extractions showed remarkably higher crystallinity indices for sericin than those obtained after hot water extraction. However, no significant differences were observed in the crystallinity index of sericin between urea and citric acid solution extraction in plate-facing side of the film.

A Study on Heat Flow Characteristics during Hot Water Extraction Process (온수추출과정의 열유동 특성에 관한 연구)

  • 장영근;박정원
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.13 no.7
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    • pp.549-556
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    • 2001
  • Heat flow characteristics during hot water extraction process was studied experimentally. Data were taken at various outlet port type for the fixed inlet port type, inlet-outlet temperature differences and mass flow rates. In this study, the temperature distribution in a storage tank and an outlet temperature were measured to predict a flow pattern in the storage tank, and a hot water extraction efficiency was analysed with respect to the variables dominating a extraction process. Experimental results show that the extraction efficiency is high in a low flow rate in case of using modified distributor I(MDI) as a outlet port type.

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Efficient Flavonoid Extraction from Apple Peel by Subcritical Water and Estimation of Antioxidant Activity (아임계수를 이용한 사과 과피 플라보노이드의 효율적 추출 및 항산화 활성 평가)

  • Cheigh, Chan-Ick;Yoo, Seo-Yeon;Chung, Myong-Soo
    • The Korean Journal of Food And Nutrition
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    • v.24 no.3
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    • pp.458-463
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    • 2011
  • The effect of subcritical water for the extraction of total polyphenols and flavonoids from apple peel was investigated, and then the antioxidant activity of the extracts was estimated. Maximum yields of total polyphenolic compounds($36.4{\pm}1.9mg$ quercetin equivalent(QE)/g dried material) and flavonoids($9.9{\pm}0.8mg$ QE/g dried material) were obtained by subcritical water extraction(SWE) with operating conditions of $190^{\circ}C$, 1,300 psi, and 20 min. Furthermore, the highest antioxidant activity($76.1{\pm}1.1%$) was observed in the extract obtained from SWE using the same conditions. The flavonoids from the SWE of apple peel were compared to three conventional extraction methods in terms of their extraction efficiency and antioxidant activity. The SWE was significantly more effective than hot water ($90^{\circ}C$), methanol, and ethanol extraction for flavonoid yield by 4.7-, 2.2-, and 1.3-fold, respectively, and for antioxidant activity by 11.0-, 4.9, and 2.8-fold, respectively.

Study on the Comparison of Effects by Extraction Methods of Roast and Raw Semen Zizyphi Spinosae (생산조인(生酸棗仁)과 초산조인(炒酸棗仁)의 추출방법에 따른 효능비교연구)

  • Lee, Eun-Kyoung;Hong, Hak-Gi;Chong, Myong-Soo
    • Journal of Physiology & Pathology in Korean Medicine
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    • v.23 no.6
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    • pp.1416-1422
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    • 2009
  • To observe the difference and change of the efficacy and ingredient appearing according to whether semen zizyphi spinosae has been roasted and its extraction method, locomotor activity, anticonvulsant activity, sleeping effect of each hot water and UMPM low temperature extracts of roast and raw semen zizyphi spinosae were measured through animal tests. Roast semen zizyphi spinosae showed superior pharmacological efficacy than raw semen zizyphi spinosae. Also, hot water extraction method showed superior pharmacological efficacy than low temperature extraction method(UMPM) that uses ultrasonic waves and microwaves. In short, it was shown that herbal medicine's extraction method needs to maximize medicinal effects by trying optimum extraction methods according to efficacy by considering characteristics of each herbal medicine. Together, there's also the need for in-depth studies on water-soluble ingredients of semen zizyphi spinosae that may be extracted through full hot water extraction method.

Water body extraction in SAR image using water body texture index

  • Ye, Chul-Soo
    • Korean Journal of Remote Sensing
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    • v.31 no.4
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    • pp.337-346
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    • 2015
  • Water body extraction based on backscatter information is an essential process to analyze floodaffected areas from Synthetic Aperture Radar (SAR) image. Water body in SAR image tends to have low backscatter values due to homogeneous surface of water, while non-water body has higher backscatter values than water body. Non-water body, however, may also have low backscatter values in high resolution SAR image such as Kompsat-5 image, depending on surface characteristic of the ground. The objective of this paper is to present a method to increase backscatter contrast between water body and non-water body and also to remove efficiently misclassified pixels beyond true water body area. We create an entropy image using a Gray Level Co-occurrence Matrix (GLCM) and classify the entropy image into water body and non-water body pixels by thresholding of the entropy image. In order to reduce the effect of threshold value, we also propose Water Body Texture Index (WBTI), which measures simultaneously the occurrence of repeated water body pixel pair and the uniformity of water body in the binary entropy image. The proposed method produced high overall accuracy of 99.00% and Kappa coefficient of 90.38% in water body extraction using Kompsat-5 image. The accuracy analysis indicates that the proposed WBTI method is less affected by the choice of threshold value and successfully maintains high overall accuracy and Kappa coefficient in wide threshold range.

Complexing Capacity - A Measure of Evaluating Water Quality

  • Akaiwa, Hideo;Itabashi, Hideyuki
    • Analytical Science and Technology
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    • v.8 no.4
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    • pp.1089-1094
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    • 1995
  • Methods for the measurement of copper(II) complexing capacity (CuCC) of natural waters by using the back-extraction of bis(benzoyl-trifluoroacetonate)copper(II) and the extraction rate of dithizonato-copper(II) complex were described. Experimental results show that the CuCC of the Kiryu river water samples from urban area were consistently larger than those from up-stream, due to a ligand which originated from human activities.

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Changes in 2,6-dimethoxy-1,4-benzoquinone and Water Extractable Arabinoxylan Content of Wheat Germ Extract by Enzyme Treatment (효소처리에 따른 밀 배아 추출물의 2,6-dimethoxy-1,4-benzoquinone과 수용성 아라비노자일란 함량 변화)

  • Lee, Jae-Kang;Lee, Jung-Hun;Choi, Yong-Hyun;Choi, Yong-Seok;Ryu, Gi-Hyung
    • Food Engineering Progress
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    • v.23 no.1
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    • pp.22-29
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    • 2019
  • This study was carried out using Celluclast 1.5L to increase the content of 2,6-DMBQ and water extractable arabinoxylan in wheat germ extract. Extraction temperatures were 30℃, 45℃ and 60℃. The extraction times were 0, 6, 12, 18, 24 and 30 h. The pH of the extract decreased rapidly from 18 h at 30℃ in both water- and enzyme-treated extracts. 2,6-DMBQ of water- and enzyme-treated extracts increased with the extraction time. At 30-hour extraction time, enzyme-treated extract increased 27.60% at 30℃ extraction temperature than water extraction. Extraction temperatures of 45℃ and 60℃ were increased by 65.03% and 151.05%, respectively. The highest content of water-extractable arabinoxylan was 15.23±0.08 mg/g when the enzyme was treated at an extraction temperature of 60℃ for 30 h. At 30=hour extraction time, enzyme-treated extract increased 7.92% at 30℃ extraction temperature compared to water extraction. Extraction temperatures of 45℃ and 60℃ were increased by 31.20% and 54.38%, respectively.

Conditioning of the Extraction of Acidic Polysaccharide from Red Ginseng Marc (홍삼박으로부터 산성다당체의 최적 추출 조건 분석)

  • Chang, Eun-Ju;Park, Tae-Kyu;Han, Yong-Nam;Hwang, Keum-Hee
    • Korean Journal of Pharmacognosy
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    • v.38 no.1
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    • pp.56-61
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    • 2007
  • This study was carried out to investigate the optimum conditions for extraction of acidic polysaccharides from red ginseng marc produced by manufacturing alcoholic extract from red ginseng. Method of carbazole-sulfuric acid was applied to determine the amount of acidic polysaccharides in red ginseng marc. The amounts of acidic polysaccharides in water extract of red ginseng marc were increased with increasing extraction temperature. The contents of acidic polysaccharides were not significantly different despite of the extraction time increasing from 6 hours to 48 hours. The contents of starch in water-extract of red ginseng marc were increased with increasing extraction temperature. The starch amounts in water extract of red ginseng marc extracted for 48 hours were increased. The yields of polysaccharide precipitated from water-extract of red ginseng marc were increased with increasing extraction temperature. The hydration rate of acidic polysaccharides and starch from water-extract of red ginseng marc were decreased with increasing extraction temperature. The contents of starch were not significantly different despite of the extraction time increasing from 6 hours to 48 hours at $8^{\circ}C$. However, the rehydration rate of acidic polysaccharide for 48 hours were decreased at $8^{\circ}C$. The rehydration rate of acidic polysaccharide and starch extracted from 6 hours to 24 hours at $25^{\circ}C$ were not significantly different, but those extracted for 48 hours were increased. From the above results, we suggest that by altering the extraction conditions in red ginseng marc it is possible to develop optimum conditions for extraction that modulate the proportions of acidic polysaccharide and starch.

Effect of Microwave Assisted Water Extraction on Insoluble Phenolic Compounds through Bioactivity of Fagopyrum esculentum

  • Kim, Hyun Gi;Kim, Yong Ju;Lian, Thang Tung;Song, Sueng Yeob;Bang, Kuek Soo
    • Korean Journal of Plant Resources
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    • v.32 no.6
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    • pp.723-729
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    • 2019
  • Fagopyrum esculentum (Buckwheat) is a globally used alternative crop that contains several useful substances with various effects; however, many of these substances (rutin, quercetin, etc.) are water insoluble. To extract these substances, alcohols is required, which is inconvenient because these solvents cause diverse problems. Many studies are underway to achieve effective extraction of these substances with water. Among of these studies, microwave assisted water extraction (MAE) has been performed extensively. In this study, we performed the extraction in various solvents and/or microwave from Fagopyrum esculentum. The analysis of the content of useful substances and the bioactivity were performed and shown to increase in MAE. Liquid chromatography-mass was performed in order to identify of the useful water-insoluble substances. Catechin, quercetin, and rutin, which are all insoluble in water, were hardly extracted with water even on heating (4.4 ppb, 3.9 ppb and 60.3 ppb, respectively). However, MAE was found to extract much more of these substances than water (1204 ppb, 110.8 ppb and 2946 ppb, respectively). Although less efficient than alcohols, MAE showed much higher efficiency than simple water extraction. These results indicate that water extraction using microwave technology is effective in cases where it is difficult to extract useful substances using water.