• Title/Summary/Keyword: Water casting method

Search Result 120, Processing Time 0.023 seconds

Rheology of Slurries and Effects of Polymer Volume Ratio in Aqueous PZT Tape Casting

  • Yoon, Seok-Jin;Shin, Hyo-Soon;Lee, Dong-Kyun;Kang, Chong-Yun;Park, Ji-Won;Kim, Hyun-Jai
    • The Korean Journal of Ceramics
    • /
    • v.7 no.1
    • /
    • pp.16-19
    • /
    • 2001
  • For the fast dry of the aqueous tape, the process which water was reaplaced by organic solvent was proposed. Socalled, it was the solvent washing dry. Three organic solvents (methanol, ethanol and acetone) were selected for the washing solvent. The weight loss of the washed tapes was measured to evaluate the dry rate of the tapes and dried tapes were examined the generation of the cracks with the variations of the organic solvent and the washing time. Methanol, ethanol and acetone were available organic solvents for this method. The tapes washed in methanol, ethanol and acetone were dried rapidly for twenty minutes. After thirty minutes, the weight losses were not found any more, The solvent of the lower surface tension can decreases the crack of dried tape. If solvent substitutes water completely, though it was fast dried, crack can be eliminated.

  • PDF

Cellulose acetate membrane preparation by phase inversion to estimate optimized parameters and its performance study

  • Katariya, Heena N;Patel, Tejal M
    • Membrane and Water Treatment
    • /
    • v.13 no.3
    • /
    • pp.139-145
    • /
    • 2022
  • Development in advanced separation processes leads to the significant advancement in polymeric membrane preparation methodology. Therefore, present research investigated the preparation and characterization of cellulose acetate membrane by phase inversion separation method to determine optimized operating parameters. Prepared CA membrane's performance was been analyzed in terms of % rejection and flux. Investigation was conducted to study effect of different parameters such as polymer concentration, evaporation rate, thickness of film, coagulation bath properties, temperature of polymer solution and of the coagulation bath etc. CA membrane was fabricated by taking polymer concentration 10wt% and 11wt% with zero second evaporation time and varying film thickness over non-woven polyester fabric. Effect of coagulation bath temperature (CBT) and casting solution temperature were also been studied. The experimental results from SEM showed that the surface morphology had been changed with polymer r concentration, coagulation bath and casting solution temperature, etc. Lower polymer concentration leads to lower precipitation time giving porous membrane. The prepared membrane was tested for advanced waste water treatment of relevant effluent stream in pilot plant to study flux and rejection behavior of the membrane.

Heat-Treated Polyvinyl Alcohol/Cellulose Nanocrystal Film with Improved Mechanical Properties and Water Resistance (내수성 및 기계적 물성이 향상된 열처리된 폴리비닐알코올/셀룰로오스 나노결정 필름)

  • Nguyen, Son Van;Lee, Bong-Kee
    • Journal of the Korean Society of Manufacturing Process Engineers
    • /
    • v.20 no.11
    • /
    • pp.1-8
    • /
    • 2021
  • In this study, the water resistance and mechanical properties of heat-treated polyvinyl alcohol (PVA)/cellulose nanocrystal (CNC) films were investigated. PVA is the most commonly used synthetic biodegradable polymers owing to its excellent properties. However, the water/moisture sensitivity and relatively poor mechanical properties of PVA limits its applications. Although heat treatment is a conventionally used method to improve the mechanical strength and water resistance of PVA, the effectiveness of this method is insufficient. Therefore, CNC was used to further improve the mechanical properties and water resistance of the heat-treated PVA film. PVA/CNC nanocomposites containing CNC contents of 0, 1, 3, 5, and 10 wt% were fabricated using solvent casting and subsequent heat treatment. The mechanical properties and water resistance of PVA/CNC films were significantly improved. The tensile strength and wet strength of the PVA/CNC film with a CNC content of 5 wt% (PVA/CNC 5%) were 184.5% and 136.0% higher than those of the untreated PVA, respectively. In addition, the water absorption and solubility of PVA/CNC 5% were 56.6% and 68.2% lower than those of the untreated PVA.

Applicability of Air Cooling Heat-treatment for a Duplex Stainless Steel Casting (2상 스테인레스 주강의 공냉 열처리 적용 가능성)

  • Kim, Bong-Whan;Yang, Sik;Shin, Je-Sik;Lee, Sang-Mok;Moon, Byung-Moon
    • Journal of Korea Foundry Society
    • /
    • v.26 no.1
    • /
    • pp.17-26
    • /
    • 2006
  • The substitution of cooling method from water quenching to air cooling after solution heat treatment was aimed for the development of a convenient and economical heat treatment process of duplex stainless steels without deterioration of mechanical and corrosion resistant properties for the industry. In order to achieve this goal, the mechanical properties and corrosion properties of a ASTM A890-4A duplex stainless steel were systematically investigated as functions of casting condition and cooling method after solution heat treatment. A 3-stepped sand mold and a permanent Y-block mold were used to check the effects of solidification structure and cooling rate after solution heat treatment. The microstructural characteristics such as the ferrite/austenite phase ratio and the precipitation behavior of ${\sigma}$ phase and carbides were investigated by combined analysis of OM and SEM-EDX with an aid of TTT diagram. Hardness and tension test were performed to evaluate the mechanical properties. Impact property at $-40^{\circ}C$ and corrosion resistance were also examined to check the possibility of the industrial application of this basic study. Throughout this investigation, air-cooling method was proved to effectively substitute for water-quenching process after the solution heat treatment, when the duplex stainless steel was sand mold cast with a thickness below 15 mm or permanent mold cast with a thickness below 20 mm.

Preparation of Porous Separators for Zn Air Batteries Through Phase Inversions of Polyethersulfone-PVP Solutions (Polyethersulfone-PVP 용액의 상전이를 통한 아연공기전지의 다공성 분리막 제조)

  • Cho, Yu Song;Koo, Ja-Kyung
    • Membrane Journal
    • /
    • v.24 no.1
    • /
    • pp.10-19
    • /
    • 2014
  • Porous flat sheet membranes for separators in Zn air batteries were prepared with polyethersulfone (PES) solutions by immersion precipitation phase inversion method. PES/polyvinylpyrrolidone(PVP)/N-methylpyrrolidone(NMP) mixtures were used for casting solutions and water was used for coagulant. With the separators, Zn air batteries were fabricated. The separators were characterized by means of stress-strain test, impedance test and SEM. The Zn air batteries were tested by current interrupt method (CIM) and galvanostatic discharge method. The tensile strength increased with increasing PES content in the casting solution while the ionic conductivity decreased. On the other hand, the ionic conductivity increased while the tensile strength decreased with increasing PVP content. The effect of ionic conductivity trend of the separator in the Zn air battery was confirmed through current interrupt method and galvanostatic discharge method experiments. The battery with the separator from casting solution with higher PES content showed higher IR drop and lower discharge capacity. And the battery with the separator from casting solution with higher PVP content showed lower IR drop and higher discharge capacity.

Fabrication and Energy Harvesting Characteristics of Water Energy Harvester Using Piezoelectric Ceramic Bimorph Cantilever (바이몰프형 압전세라믹 캔틸레버를 이용한 수력에너지 하베스터 모듈 제작 및 발전 특성)

  • Kim, Kyoung-Bum;Kim, Chang-Il;Yun, Ji-Sun;Jeong, Young Hun;Nahm, Jung Hee;Cho, Jeong-Ho;Paik, Jong-Hoo;Nahm, Sahn;Seong, Tae-Hyeon
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
    • /
    • v.25 no.12
    • /
    • pp.943-948
    • /
    • 2012
  • A new water energy harvester module, which is composed of piezoelectric bimorph cantilevers, harvesting circuit and a shaft with 16 impellers at a center axis, was fabricated for energy harvesting application. High energy density $Pb(Zr_{0.54}Ti_{0.46})O_3$ + 0.2 wt% $Cr_2O_3$ + 1.0 wt% $Nb_2O_5$ (PZT-CN) thick film obtained by tape casting method was used for the bimorph cantilever. The PZT-CN bimorph cantilever with a proof mass of 49 g exhibited extremely high output power of 22.5 mW (24 $mW//cm^3$) at resonance frequency of 11 Hz. In addition, the fabricated water energy harvester has a cylindrical structure with 48 bimorph cantilevers clamped at inner surface. A significantly high output power of 433 mW was obtained at a rotation speed of 120 rpm with a resistive load of $500{\Omega}$ for the water energy harvester.

Evaluation of the Characteristics of the Aluminum Alloy Casting Material by Heat Treatment (AC8A 알루미늄합금 주조재의 열처리에 의한 특성 평가)

  • Lee, Syung Yul;Park, Dong Hyun;Won, Jong Pil;Kim, Yun Hae;Lee, Myung Hoon;Moon, Kyung Man;Jeong, Jae Hyun
    • Corrosion Science and Technology
    • /
    • v.11 no.6
    • /
    • pp.280-285
    • /
    • 2012
  • Aluminum is on active metal, but it is well known that its oxide film plays a role as protective barrier which is comparatively stable in air and neutral aqueous solution. Thus, aluminum alloys have been widely applied in architectural trim, cold & hot-water storage vessels and piping etc., furthermore, the aluminum alloy of AC8A have been widely used in mold casting material of engine piston because of its properties of temperature and wear resistance. In recent years, the oil price is getting higher and higher, thus the using of low quality oil has been significantly increased in engines of ship and vehicle. Therefore it is considered that evaluation of corrosion resistance as well as wear resistance of AC8A material is also important to improve its property and prolong its lifetime. In this study, the effect of solution and tempering heat treatment to corrosion and wear resistance is investigated with electrochemical method and measurement of hardness. The hardness decreased with solution heat treatment compared to mold casting condition, but its value increased with tempering heat treatment and exhibited the highest value of hardness with tempering heat treatment temperature at $190^{\circ}C$ for 24hrs. Furthermore, corrosion resistance increased with decreasing of the hardness, and decreased with increasing of the hardness reversely. As a result, it is suggested that the optimum heat treatment to improve both corrosion and wear resistance is tempering heat treatment temperature at $190^{\circ}C$ for 16hrs.

Preparation of Polysulfone Microfiltration Membranes by a Sulfonated Polyethersulfone Additive (술폰산기를 가지는 폴리에테르술폰 첨가제를 이용한 폴리술폰 정밀여과막의 제조)

  • Kim, Nowon;Jung, Boram
    • Membrane Journal
    • /
    • v.27 no.3
    • /
    • pp.273-283
    • /
    • 2017
  • Polysulfone (PSF) is one of an important polymer that has been widely used in the manufacture of asymmetric microfiltration (MF) membranes. PSF membrane is considered as hydrophobic membrane that easily fouled during membrane operation process. The blending method is an effective method for improving the fouling resistance of PSF membranes. sPES (sulfonated polyethersulfone) is one of the useful polymers that can be used in PSF polymer blend method to improve hydrophilicity of PSF membranes. In this study, microfiltration polymer membranes were prepared by using PSF/sPES/PVP/BE/DMF casting solution and water coagulant. The morphology of MF membranes was changed by addition of a small amount of sPES in casting solution. The morphology of the sPES added membranes was changed into a highly asymmetric structure. The active layer grew and mean pore size was decreased by addition of sPES. However, the water flux of PSF/sPES/DMF/PVP/BE membrane was higher than that of PSF/DMF/PVP/BE membrane.

Application of Waste Foundry Sand to Concrete-Based Product Having Low Water Cement Ratio (낮은 W/C비를 갖는 콘크리트 제품에 대한 폐주물사의 적용)

  • 이대경;김동주;조홍준;김진만
    • Proceedings of the Korea Concrete Institute Conference
    • /
    • 2001.11a
    • /
    • pp.79-84
    • /
    • 2001
  • Because the WFS(Waste Foundry Sand), by-product of a casting factory, is generally a smaller particle than a fine aggregate, it has a bad influence on quality of concrete. Especially, the grading of aggregate is a very important factor in the case of concrete-based products having low water cement ratio manufactured by vibration and pressing method. Therefore, it is necessary to use WFS with the suitable grading of aggregate that it don't has a bad Influence on the quality of concrete-based products. This study investigated the suitable using proportion of WFS by means of the composition method of aggregate suggested by Driscoll. The results showed that it was desirable to use 10% of WFS since higher strength was developed with that amount.

  • PDF

Finite Element Analysis on Phase-Change Process of Pure Water (유한요소법을 이용한 순수 물의 상변화 과정에 대한 수치해석)

  • Hong Y. D.;Cha K. S.;Seo S. J.;Park C. G.
    • Journal of computational fluids engineering
    • /
    • v.7 no.4
    • /
    • pp.1-7
    • /
    • 2002
  • The phase-change transformation processes are relevant in many engineering applications. In particular, this phenomenon plays an important role in the extraction and fabrication operations in the metallurgical industry. The control of the heat transfer and fluid flow patterns is important to achieve casting quality and competitive production times. In the present study, a simple finite-element algorithm is developed for solid-liquid phase change problems. Natural convection in the liquid phase due to the temperature dependency of water density is considered by a numerical model. The predictions are compared with measurements by the particle image velocimetry(PIV). to show that the calculation results are in good agreement with the experiment results.