• 한국약용작물학회지
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• 제21권2호
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• pp.97-104
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• 2013

The objective of this study is to investigate the optimal condition for macerating enzymatic extraction process that leads to the highest yield and the largest extracted amount of bio-active contents from Rubus coreanus Miq. fruit. The optimal extraction conditions were found as the following: The initial amount of the water added to the fruit was 20 ~ 30% by weight. The mixing ratio used for the macerating enzyme was 4 : 1 : 2 (w : w : w) for cellulase:pectinase:amylogucosidase, and the amount of the macerating enzyme added was 2% by weight. The extraction process was done at a temperature of $45{\sim}50^{\circ}C$ for 10 hours. The extraction yields on Rubus coreanus Miq. fruit by macerating enzymatic extraction process was increased by 84.3% compared to that of hot-water extraction process. The amounts of organic acids and vitamin found in the extract were also higher. The amount of polyphenol and anthocyanin contents in the extract were 185% and 257% of those from hot-water extraction, respectively. These results suggest that macerating enzymatic extraction is an effective method to boost extraction yield and to increase the amount of extraction of bio-active contents from Rubus coreanus Miq. fruit.

• International Journal of Industrial Entomology and Biomaterials
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• 제26권2호
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• pp.113-118
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• 2013

In this study, silk sericin films were prepared using different extraction methods, and the molecular conformation of sericin was examined using Fourier-transform infrared spectroscopy with attenuated total reflection geometry. Additionally, the effect of the film side (air-facing side or plate-facing side) on the molecular conformation of the sericin films was investigated. Interestingly, the molecular conformation of the sericin film depended on the film side. The molecular conformation of air-facing side of the sericin film was significantly influenced by extraction solution and time. The ${\beta}$-sheet crystallization and the crystallinity index of the sericin film markedly increased with an increase in the extraction time in hot water. The order of the crystallinity indices for the sericin films obtained with different extraction solutions was as follows: citric acid solution > urea solution >> hot water. In contrast, no remarkable differences were observed in the molecular conformation of the plate-facing side of the sericin film after extraction in hot water for different time periods. Urea and citric acid solution extractions showed remarkably higher crystallinity indices for sericin than those obtained after hot water extraction. However, no significant differences were observed in the crystallinity index of sericin between urea and citric acid solution extraction in plate-facing side of the film.

• 설비공학논문집
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• 제13권7호
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• pp.549-556
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• 2001

Heat flow characteristics during hot water extraction process was studied experimentally. Data were taken at various outlet port type for the fixed inlet port type, inlet-outlet temperature differences and mass flow rates. In this study, the temperature distribution in a storage tank and an outlet temperature were measured to predict a flow pattern in the storage tank, and a hot water extraction efficiency was analysed with respect to the variables dominating a extraction process. Experimental results show that the extraction efficiency is high in a low flow rate in case of using modified distributor I(MDI) as a outlet port type.

• 한국식품영양학회지
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• 제24권3호
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• pp.458-463
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• 2011

The effect of subcritical water for the extraction of total polyphenols and flavonoids from apple peel was investigated, and then the antioxidant activity of the extracts was estimated. Maximum yields of total polyphenolic compounds($36.4{\pm}1.9mg$ quercetin equivalent(QE)/g dried material) and flavonoids($9.9{\pm}0.8mg$ QE/g dried material) were obtained by subcritical water extraction(SWE) with operating conditions of $190^{\circ}C$, 1,300 psi, and 20 min. Furthermore, the highest antioxidant activity($76.1{\pm}1.1%$) was observed in the extract obtained from SWE using the same conditions. The flavonoids from the SWE of apple peel were compared to three conventional extraction methods in terms of their extraction efficiency and antioxidant activity. The SWE was significantly more effective than hot water ($90^{\circ}C$), methanol, and ethanol extraction for flavonoid yield by 4.7-, 2.2-, and 1.3-fold, respectively, and for antioxidant activity by 11.0-, 4.9, and 2.8-fold, respectively.

• 동의생리병리학회지
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• 제23권6호
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• pp.1416-1422
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• 2009

To observe the difference and change of the efficacy and ingredient appearing according to whether semen zizyphi spinosae has been roasted and its extraction method, locomotor activity, anticonvulsant activity, sleeping effect of each hot water and UMPM low temperature extracts of roast and raw semen zizyphi spinosae were measured through animal tests. Roast semen zizyphi spinosae showed superior pharmacological efficacy than raw semen zizyphi spinosae. Also, hot water extraction method showed superior pharmacological efficacy than low temperature extraction method(UMPM) that uses ultrasonic waves and microwaves. In short, it was shown that herbal medicine's extraction method needs to maximize medicinal effects by trying optimum extraction methods according to efficacy by considering characteristics of each herbal medicine. Together, there's also the need for in-depth studies on water-soluble ingredients of semen zizyphi spinosae that may be extracted through full hot water extraction method.

• 대한원격탐사학회지
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• 제31권4호
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• pp.337-346
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• 2015

Water body extraction based on backscatter information is an essential process to analyze floodaffected areas from Synthetic Aperture Radar (SAR) image. Water body in SAR image tends to have low backscatter values due to homogeneous surface of water, while non-water body has higher backscatter values than water body. Non-water body, however, may also have low backscatter values in high resolution SAR image such as Kompsat-5 image, depending on surface characteristic of the ground. The objective of this paper is to present a method to increase backscatter contrast between water body and non-water body and also to remove efficiently misclassified pixels beyond true water body area. We create an entropy image using a Gray Level Co-occurrence Matrix (GLCM) and classify the entropy image into water body and non-water body pixels by thresholding of the entropy image. In order to reduce the effect of threshold value, we also propose Water Body Texture Index (WBTI), which measures simultaneously the occurrence of repeated water body pixel pair and the uniformity of water body in the binary entropy image. The proposed method produced high overall accuracy of 99.00% and Kappa coefficient of 90.38% in water body extraction using Kompsat-5 image. The accuracy analysis indicates that the proposed WBTI method is less affected by the choice of threshold value and successfully maintains high overall accuracy and Kappa coefficient in wide threshold range.

• 분석과학
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• 제8권4호
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• pp.1089-1094
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• 1995

Methods for the measurement of copper(II) complexing capacity (CuCC) of natural waters by using the back-extraction of bis(benzoyl-trifluoroacetonate)copper(II) and the extraction rate of dithizonato-copper(II) complex were described. Experimental results show that the CuCC of the Kiryu river water samples from urban area were consistently larger than those from up-stream, due to a ligand which originated from human activities.

• 산업식품공학
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• 제23권1호
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• pp.22-29
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• 2019

본 연구는 밀 배아의 기능성 물질인 2,6-DMBQ와 아라비노자일란 추출 효율을 증가시키기 위하여 상업용 효소인 Celluclast 1.5L을 사용하여 추출하였다. 추출 시 온도는 30, 45, 60℃였고, 추출 시간은 0, 6, 12, 18, 24, 30시간 추출 후 상등액 pH 변화와 건조물을 분석하였다. 추출물의 pH는 WEWG와 ETWG 모두 추출 온도 30℃에서는 18시간 추출 시부터 급격하게 감소하였으며, 45℃는 12시간부터 감소하였고, 60℃는 다른 추출 온도와 비교하여 큰 변화는 없었다. 2,6-DMBQ는 WEWG와 ETWG 모두 추출 시간이 경과함에 따라 증가하였다. 추출 온도 30℃에서 가장 높은 함량으로 추출되었으며, 30시간 추출할 때 2,6-DMBQ 함량은 ETWG에서 WEWG 보다 추출 온도 30℃에서 27.60%, 45℃에서 65.03%, 60℃에서 151.05% 증가하였다. 수용성 아라비노자일란 함량은 WEWG와 비교하여 ETWG가 높게 측정되었으며, 효소 처리 후 60℃에서 15.23±0.08 mg/g으로 가장 높은 함량으로 나타났다. 30시간 추출 시 ETWG와 WEWG에서의 수용성 아라비노자일란 함량을 비교했을 때 30℃에서 7.92%, 45℃에서 31.20%, 60℃에서 54.38% 증가하였다. 본 연구 결과는 제분 부산물인 밀 배아에 항염 활성을 보유하는 기능성 소재로서의 활용을 위한 기초자료로 이용될 수 있을 것으로 판단된다.

• 생약학회지
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• 제38권1호
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• pp.56-61
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• 2007

This study was carried out to investigate the optimum conditions for extraction of acidic polysaccharides from red ginseng marc produced by manufacturing alcoholic extract from red ginseng. Method of carbazole-sulfuric acid was applied to determine the amount of acidic polysaccharides in red ginseng marc. The amounts of acidic polysaccharides in water extract of red ginseng marc were increased with increasing extraction temperature. The contents of acidic polysaccharides were not significantly different despite of the extraction time increasing from 6 hours to 48 hours. The contents of starch in water-extract of red ginseng marc were increased with increasing extraction temperature. The starch amounts in water extract of red ginseng marc extracted for 48 hours were increased. The yields of polysaccharide precipitated from water-extract of red ginseng marc were increased with increasing extraction temperature. The hydration rate of acidic polysaccharides and starch from water-extract of red ginseng marc were decreased with increasing extraction temperature. The contents of starch were not significantly different despite of the extraction time increasing from 6 hours to 48 hours at $8^{\circ}C$. However, the rehydration rate of acidic polysaccharide for 48 hours were decreased at $8^{\circ}C$. The rehydration rate of acidic polysaccharide and starch extracted from 6 hours to 24 hours at $25^{\circ}C$ were not significantly different, but those extracted for 48 hours were increased. From the above results, we suggest that by altering the extraction conditions in red ginseng marc it is possible to develop optimum conditions for extraction that modulate the proportions of acidic polysaccharide and starch.

• 한국자원식물학회지
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• 제32권6호
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• pp.723-729
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• 2019

Fagopyrum esculentum (Buckwheat) is a globally used alternative crop that contains several useful substances with various effects; however, many of these substances (rutin, quercetin, etc.) are water insoluble. To extract these substances, alcohols is required, which is inconvenient because these solvents cause diverse problems. Many studies are underway to achieve effective extraction of these substances with water. Among of these studies, microwave assisted water extraction (MAE) has been performed extensively. In this study, we performed the extraction in various solvents and/or microwave from Fagopyrum esculentum. The analysis of the content of useful substances and the bioactivity were performed and shown to increase in MAE. Liquid chromatography-mass was performed in order to identify of the useful water-insoluble substances. Catechin, quercetin, and rutin, which are all insoluble in water, were hardly extracted with water even on heating (4.4 ppb, 3.9 ppb and 60.3 ppb, respectively). However, MAE was found to extract much more of these substances than water (1204 ppb, 110.8 ppb and 2946 ppb, respectively). Although less efficient than alcohols, MAE showed much higher efficiency than simple water extraction. These results indicate that water extraction using microwave technology is effective in cases where it is difficult to extract useful substances using water.