• 제목/요약/키워드: Volume calibration

검색결과 252건 처리시간 0.022초

황색종 담배중 전알카로이드와 환원당 분석에 대한 불확도 측정 (Uncertainty of Total Alkaloids and Reducing Sugar Determination in Flue-cured Tobacco)

  • 백순옥;장기철;이운철;한상빈
    • 한국연초학회지
    • /
    • 제23권1호
    • /
    • pp.45-52
    • /
    • 2001
  • This study was carried out to evaluate the uncertainty in the analysis of total alkaloids and reducing sugar content in flue-cured tobacco. The sources of uncertainty associated with the analysis of total alkaloids and reducing sugar were the weighing of sample, the preparation of extracting solution, the addition of extracting solution into the sample, the preparation of standard solution, the precision of calibration curve for standard solution, the reproducibility of analysis, and the determination of water content in tobacco, etc. For the calculating uncertainties, Type A of uncertainty was evaluated by the statistical analysis of a series of observation, and Type B by the information based on supplier’s catalogue and/or certificated of calibration. It was shown that the main source of uncertainty was caused by the calibration curve of standard solution, the reproducibility of analysis, the volume measurement of 1$m\ell$, and the purity of nicotine reference material in the preparation of standard solution. The uncertainty in the addition of extracting solution, the sample weighing, the volume measurement of 100$m\ell$, and the determination of water content of tobacco contributed relatively little to the overall uncertainty. The expanded uncertainty of total alkaloids and reducing sugar in flue-cured tobacco at 95% level of confidence was $\pm$0.12% and $\pm$0.54%, respectively.

  • PDF

다중 측정 좌표계를 이용한 로봇 캘리브레이션 방법 연구 (Study on Robot Calibration Using Multi-measurement Coordinate System)

  • 임생기;김정태;범진환;최재성
    • 한국정밀공학회지
    • /
    • 제16권3호통권96호
    • /
    • pp.164-173
    • /
    • 1999
  • Robot calibration needs accurate measurements of robot end-effector position at a number of different robot configurations. One of the efficient ways of the measurement is "Touching on Jig" method suggested in [7], which utilizes a touch sensor and a fixture consisting of various sizes of blocks. By moving the end-effector to touch the surface of a block whose position relative to the other is known, the end-effector position relative to the fixture coordinate system can be obtained at the instant of touching. However, the global size of fixture is too small to cover the various configurations of the robot. Because of the manufacturing difficulties, the fixture cannot be manufactured large enough for well distributed position measurement. It results in the improvement of robot accuracy only in the limited space near to the fixture rather than over the whole space of the robot working volume. The paper proposes a method to resolve the above problem by measuring the end-effector positions with respect to several different coordinate system using the same measurement devices. It is found that the proposed method leads the improvements of robot position accuracy over the large space of working volume. The experimental studies are performed to show the validity of the method and their results are discussed.

  • PDF

부피 측정을 위한 초음파 팬텀 개발 (Development of Ultrasound Phantom for Volume Calibration)

  • 김혜영;이지혜;이경자;서현숙;이레나
    • 한국의학물리학회지:의학물리
    • /
    • 제19권4호
    • /
    • pp.227-230
    • /
    • 2008
  • 본 연구에서는 2차원 초음파 시스템의 체적 측정 정확성을 측정하기 위한 초음파 팬텀을 설계 및 제작하였다. 팬텀은 체적 측정용 타겟과 백그라운드 물질로 구성되었다. 백그라운드 물질은 agarose gel과 물을 혼합하여 만들었다. 타켓은 모양과 부피를 변화시키기 위하여 신축성 있는 물질로 선택하였고 타겟에 물을 채운 후 백그라운드 물질에 삽입하였다. 2차원 초음파 시스템의 정확성을 평가하기 위하여 세가지 형태의 타겟(구형, 2가지 형태의 타원형, 삼각 기둥형)을 제작하였다. 타원형의 경우, 하나는 길이와 폭의 크기가 비슷하도록 제작하였고(타원 1) 다른 하나는 길이가 폭보다 2배 이상인 모양(타원 2)으로 제작하였다. 각각 형태의 타겟 부피는 94 cc에서 450 cc까지 변화하였고 2차원 초음파 장비(128XP, ACUSON)를 이용하여 정확성을 측정하였다. 구 모양의 타겟에 삽입된 물의 실제 체적과 측정된 체적 간의 차는 6.7에서 11% 이다. 타원형 타겟의 경우 타원 1은 9.2에서 10.5% 사이의 차이를 보이는데 타원 2의 경우는 25.7%의 오차가 있다. 삼각기둥 형태의 경우는 실제체적과 측정체적간 20.8에서 35%의 차이를 보였다. 쉽고 간편한 방법의 초음파 팬텀의 제작 방법을 소개하였고 제작된 팬텀을 이용할 경우 초음파 시스템의 부피 측정 정확성을 평가할 수 있음을 입증하였다.

  • PDF

삼차원 좌표 측정을 위한 부피 간섭계의 오차분석 및 성능평가 (Error analysis and Performance test of the Volumetric interferometer for Absolute distance measurement)

  • 이혁교;주지영;김승우
    • 한국정밀공학회:학술대회논문집
    • /
    • 한국정밀공학회 2002년도 추계학술대회 논문집
    • /
    • pp.387-390
    • /
    • 2002
  • In this paper, we accomplish uncertainty evaluation and performance test of the volumetric interferometer using two spherical wavefronts emitted from the ends of two single mode fibers. We verify that the volumetric interferometer has the volume uncertainty of 690nm through the error analysis and it has the resolution of 0.1 0.1$\mu\textrm{m}$ for x axis which is the same order of repeatability for x axis. Also, we obtain the systematic error of $1\mu\textrm{m}$ for $60\times 60\times 20 mm^3$ working volume using self-calibration with an artifact plate.

  • PDF

척추 방사선수술 시 다엽콜리메이터 위치 오차의 임상적 위험성 평가 (Evaluation of Clinical Risk according to Multi-Leaf Collimator Positioning Error in Spinal Radiosurgery)

  • 강동진;오건;신영주;강진규;정재용;이보람
    • 대한방사선기술학회지:방사선기술과학
    • /
    • 제46권6호
    • /
    • pp.527-533
    • /
    • 2023
  • The purpose of this study is to evaluate the clinical risk of spinal radiosurgery by calculating the dose difference due to dose calculation algorithm and multi-leaf collimator positioning error. The images acquired by the CT simulator were recalculated by correcting the multi-leaf collimator position in the dose verification program created using MATLAB and applying stoichiometric calibration and Monte Carlo algorithm. With multi-leaf collimator positioning error, the clinical target volume (CTV) showed a dose difference of up to 13% in the dose delivered to the 95% volume, while the gross tumor volume (GTV) showed a dose difference of 9%. The average dose delivered to the total volume showed dose variation from -8.9% to 9% and -10.1% to 10.2% for GTV and CTV, respectively. The maximum dose delivered to the total volume of the spinal cord showed a dose difference from -14.2% to 19.6%, and the dose delivered to the 0.35 ㎤ volume showed a dose difference from -15.5% to 19.4%. In future research, automating the linkage between treatment planning systems and dose verification programs would be useful for spinal radiosurgery.

3차원 Volume PIV의 개발 (Development of 3-D Volume PIV)

  • 최장운;남구만;이영호;김미영
    • 대한기계학회논문집B
    • /
    • 제27권6호
    • /
    • pp.726-735
    • /
    • 2003
  • A Process of 3-D Particle image velocimetry, called here, as '3-D volume PIV' was developed for the full-field measurement of 3-D complex flows. The present method includes the coordinate transformation from image to camera, calibration of camera by a calibrator based on the collinear equation, stereo matching of particles by the approximation of the epipolar lines, accurate calculation of 3-D particle positions, identification of velocity vectors by 3-D cross-correlation equation, removal of error vectors by a statistical method followed by a continuity equation criterior, and finally 3-D animation as the post processing. In principle, as two frame images only are necessary for the single instantaneous analysis 3-D flow field, more effective vectors are obtainable contrary to the previous multi-frame vector algorithm. An Experimental system was also used for the application of the proposed method. Three analog CCD camera and a Halogen lamp illumination were adopted to capture the wake flow behind a bluff obstacle. Among 200 effective particle s in two consecutive frames, 170 vectors were obtained averagely in the present study.

A Noise Re-radiation Calibration Technique in Interferometric Synthetic Aperture Radiometer for Sub-Y-type Array at Ka-Band

  • Seo Seungwon;Kim Sunghyun;Choi Junho;Park Hyuk;Lee Hojin;Kim Yonghoon;Kang Gumsil
    • 대한원격탐사학회:학술대회논문집
    • /
    • 대한원격탐사학회 2004년도 Proceedings of ISRS 2004
    • /
    • pp.577-580
    • /
    • 2004
  • To overcome with large size noise source distribution network design difficulty in interferometric radiometer system, especially for sub-Y-type array, a new on-board calibration technique using noise re-radiation is proposed in this paper. The suggested calibration technique is using noise re-radiation effect of center antenna after noise source injection from matched load. This approach is especially proper to sub-Y-type array interferometric synthetic aperture radiometer in mm-wave frequency band. Compared with noise injection network of a conventional synthetic aperture radiometer, the system mass, volume, and hardware complexity is reduced and cost-effective. Only one internal noise source, matched load, is used for injection using noise re-radiation technique a small set of sub-Y receiver channels is calibrated. Detailed calibration scenario is discussed and simulation results about noise re­radiation effect are presented.

  • PDF

구조-음향 상반성 원리를 이용한 공기기인 소음원의 강도 추정 및 소음 합성 (The Use of Vibro-acoustical Reciprocity to Estimate Source Strength and Airborne Noise Synthesis)

  • 김윤재;변재환;강연준;홍진철;권오준;강구태
    • 한국소음진동공학회논문집
    • /
    • 제19권1호
    • /
    • pp.42-49
    • /
    • 2009
  • In this paper, an alternative method was introduced to conduct a transfer path analysis for airborne noise. The method used the transfer function matrix composed of acoustic transfer functions that are referenced by the input voltage of a calibration source. A calibration factor which is converting a virtual voltage to source strength was deduced by vibro-acoustical reciprocity theorem. The calibration factor is then multiplied to the virtual input voltage to estimate the operational source strength. Three loudspeakers were used to noise sources of acrylic half car model. The method was applied to airborne noise transfer path analysis of the half car. The estimated source strength by transfer path analysis was compared the deduced source strength by vibro-acoustical reciprocity to verify the method.

파이프 프루버의 측정불확도에 관한 연구 (A Study on the Measurement Uncertainty of Pipe Prover)

  • 임기원
    • 대한기계학회논문집B
    • /
    • 제24권10호
    • /
    • pp.1388-1398
    • /
    • 2000
  • A pipe prover is a flowmeter calibrator used in flow measurement field. Gravimetric and volumetric methods were applied to determine the basic volume of the pipe prover. Uncertainty of its basic volume measurement was evaluated in accordance with the procedure recommended by International Organization for Standardization. The combined standard uncertainty of determining the basic volume was estimated from the sensitivity coefficient and the standard uncertainty of independent variables. It was found that the uncertainties of the weighing and volume measurements have dominant influence on that of the basic volume determination. With the quantitative analysis of the sensitivity coefficient, the contribution of the each variable uncertainty to the combined standard uncertainty of the basic volume is shown clearly.

Phase Identification of Nano-Phase Materials using Convergent Beam Electron Diffraction (CBED) Technique

  • Kim, Gyeung-Ho;Ahn, Jae-Pyoung
    • Applied Microscopy
    • /
    • 제36권spc1호
    • /
    • pp.47-56
    • /
    • 2006
  • Improvements are made to existing primitive cell volume measurement method to provide a real-time analysis capability for the phase analysis of nanocrystalline materials. Simplification is introduced in the primitive cell volume calculation leading to fast and reliable method for nano-phase identification and is applied to the phase analysis of Mo-Si-N nanocoating layer. In addition, comparison is made between real-time and film measurements for their accuracy of calculated primitive cell volume values and factors governing the accuracy of the method are determined. About 5% accuracy in primitive cell determination is obtained from camera length calibration and this technique is used to investigate the cell volume variation in WC-TiC core-shell microstructure. In addition to chemical compositional variation in core-shell type structure, primitive cell volume variation reveals additional information on lattice coherency strain across the interface.