• Title/Summary/Keyword: Volatile organic acids

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Studies on Nutritional Compositions of the Jehotang 2. Organic Acid Content and Volatile Aroma Components (제호탕(醍蝴湯)의 일반영양성분에 관한 연구 2. 유기산 및 휘발성 향기성분 조성)

  • 윤숙자;조후종
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.25 no.4
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    • pp.654-658
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    • 1996
  • Organic acid content and volatile aroma components in Jehotang were investigated. Organic acids were detceted by HPLC and it is composed of formic acid(0.07%). lactic acid(0.22%) acetic acid (0.32%), and citric acid(3.17%), the last of which is one of the noteworthy features of Jehotang contributing greatly to its sour flavor and taste. Among the 39 volatile aroma components, whose peaks were identified by GC/MSD, and whose structures were analyzable, 17 kinds of hydrocarbon(30.81%) one kind of aldehyde(7.18%), 2 kinds of ketone(4.79%), 8 kinds of terpene(25.96%) a variety of acids (16%), 2 kinds of alcohol(5.42%), 2 kinds of phenol(2.76%) and 3 kinds of the others(7.68%) were found. The hydrocarbons, terpenes and acids occupied 70% of the aroma components, contributing to and also composing the particular flavor of Jehotang. Extracted pigments from the Jehotang showed maximum light absorbance in the wave length ranges of 200~400nm, showing a high degree of light adsorption of yellow to red color.

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Studies on the Chemical Composition of Major Fruits in Korea -On Non-volatile Organic Acid and Sugar Contents of Apricot (maesil), Peach, Grape, Apple and Pear and its Seasonal Variation- (한국산(韓國産) 주요과실류(主要果實類)의 화학성분(化學成分)에 관(關)한 연구(硏究) -매실, 복숭아, 포도, 사과 및 배의 주요품종별(主要品種別) 계절적(季節的) 비휘발성(非揮發性) 유기산(有機酸) 및 당(糖)의 함량변화(含量變化)-)

  • Lee, D.S.;Woo, S.K.;Yang, C.B.
    • Korean Journal of Food Science and Technology
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    • v.4 no.2
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    • pp.134-139
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    • 1972
  • The contents and their seasonal changes of non-volatile organic acids and sugars of various fruits in Korea, apricot(maesil), peach, grape, apple and pears were measured. The organic acid contents were determined by gas chromatography and the free sugars were detected by thin layer chromatography. The results were as follows: 1) The common non-volatile organic acids found in those fruits were oxalic, fumaric, succinic, maleic, tartaric and citric acids: though their contents varied from almost none to 3430mg/100g. 2) Malic acid was contained in all above fruits with generally the highest contents ranging $18{\sim}3430mg/100g$ among different fruits. In every fruits oxalic was the least contained among other organic acids, almost none to trace except apricot(maesil) which contained 10.8mg/100g. 3) It seemed that generally all the non-volatile acids contents decreased after ripening except maleic acid and the cases of an apple and a pear varieties where they increased. 4) Glucose and fructose were detected in all fruits both matured and unripened by thin layer chromatography. Maltose was found in apricot(maesil), peach, grape and apple. Sucrose was detected in apricot(maesil), peach, grape, apple and pear.

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Recovery of Dissolved Volatile Fatty Acids from Liquid Sludge using Anaerobic Membrane-fermenter System (혐기성 분리막을 이용한 액상 슬러지로부터의 용해성 저급 지방산의 회수)

  • Kim, Jong-Oh;Kim, Seog-Ku;Kim, Ree-Ho
    • Journal of Korean Society on Water Environment
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    • v.20 no.2
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    • pp.183-189
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    • 2004
  • The performance of a membrane-coupled anaerobic fermenter system for the recovery of volatile fatty acids (VFAs) from liquid organic sludge was experimentally investigated. Permeation flux was stably kept around $0.2(m^3/m^2/day)$ during operational period. The membrane-coupled fermenter showed 2.2 times higher VFAs concentration and higher VFAs forming rate than those of fermenter without membrane. The fermenter with membrane proved to be an effective system for the recovery of soluble organic materials from liquid sludge.

Rapid Gas Chromatographic Screening of Alcoholic Beverages for Volatile and Nonvolatile Organic Acids (기체크로마토그래피법에 의한 알코올 음료내 휘발성 및 비휘발성 유기산의 신속한 스크리닝)

  • Kim, Jung-Han;Kim, Kyoung-Rae;Chai, Jeong-Young;Park, Hyung-Kook;Choi, Kyoung-Sook
    • Korean Journal of Food Science and Technology
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    • v.26 no.2
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    • pp.162-166
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    • 1994
  • A rapid gas chromatographic (GC) profiling method for the simultaneous analysis of volatile and nonvolatile organic acids was applied to alcoholic beverages (white wine, red wine, brandy, and beer). It involves the solid-phase extraction of organic acids using Chromosorb P as the sorbent and diethyl ether as the eluent with subsequent triethylamine treatment. The resulting triethylammonium salts of acids were directly converted to volatile tert.-butyldimethylsilyl derivatives, which were analyzed by dual-capillary column GC and GC-mass spectrometry. From the alcoholic beverages studied, more than 29 organic acids were detected. When the simplified retention infer (RI) spectra of organic acids, and the direct comparisor method between alcoholic beverages and a test sample were attempted to identify a test sample, it was quickly recognized to be a red wine with the 998 ppt match quality value.

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Measurements of Volatile Organics, Newly Designated Offensive Odorants in Korea in 2008 and 2010: a Case Study on Gutter System (2008년과 2010년 지정 VOC 계열 신규악취성분들에 대한 분포특성 조사: 도심 하수환경 중 빗물받이에 대한 연구)

  • Ahn, Ji-Won;Hong, One-Feel;Lee, Eun-Hee;Kim, Ki-Hyun
    • Journal of Korean Society for Atmospheric Environment
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    • v.26 no.3
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    • pp.305-317
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    • 2010
  • In this research, a total of 11 newly designated offensive odorants in Korea in 2008 and 2010 (styrene (S), toluene (T), p-xylene (p-X), methyl ethyl ketone (MEK), methyl isobutyl ketone (MIBK), butyl acetate (BuAc), isobutyl alcohol (i-BuAl), propionic acid (PA), butyric acid (BA), isovaleric acid (IA), and valeric acid (VA)) were selected as target compounds and analyzed from two types of gutter system in the urban environment. Because of the environmental significance of these compounds as offensive odorants, the results are meaningful enough to explore their behavior and distribution in the urban environmental systems. In the course of this study, samples were collected three times a day from two different gutter systems representing the wet (W) and dry (D) conditions. A large fraction of volatile organic compounds (VOCs) data fell into method detection limit (MDL) range with exceptions of toluene, p-xylene, and methyl ethyl ketone. In contrast, the results of organic fatty acids were distinguished by the relative dominance of butyric acid and propionic acid over others. If the concentration data of all odorants were converted into odor intensity (OI), the results of aromatics, ketones, acetate, and alcohol groups approached zero level. However, odor intensity of organic fatty acids was noticeably higher with the value of 2.8 (on average) from both W and D system, suggesting their potent roles as odorants in gutter system.

Determination of the effective components in the various parts of Luffa cylindrica (L.) Roemer and development to remove the flesh from its fruit : (I) -Determination of chemical components in the various parts of Luffa cylindrica(L.) Roemer by GC and GC/MS- (수세미외의 부위별(部位別) 유효성분(有效成分) 조사(調査) 및 사과락중(絲瓜絡中) 육질제거(肉質除去) 방법(方法) 개발(開發) 연구(硏究) : (I) -수세미외의 부위별 화학성분 분석-)

  • Chang, Ki-Woon;Moon, Chang-Sick;Lee, He-Duck;Lee, Chang-Jun;Lee, Un-Chul
    • Applied Biological Chemistry
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    • v.34 no.4
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    • pp.366-372
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    • 1991
  • The volatile components, normal hydrocarbons, organic acids, and nonvolatile fatty acids in the various parts of Luffa cylindrica(L.) Roemer(sponge-gourd) were analyzed by GC and GC/MS. More than 150 volatile components were separated and thirty seven components were identified and quantified. The contents of essential oil were 0.05%, 0.05%, and 0.08% on a dried weight base in leaves, stem, and seeds respectively. Fruit juice and sap contained 0.06% and 0.03% oil on the fresh weight base. Twenty six components of normal hydrocarbons in leaves, stem, seed, and unripe fruit were separated, identified, and quantified. The total concentrations of the hydrocarbons were $75.5\;{\mu}g/g$ in leaf, $52.0\;{\mu}g/g$ in stem, $46.6\;{\mu}g/g$ in fruit juice, and $32.8\;{\mu}g/g$ in seed fractions. The major hydrocarbons in leaves, stem, and fruit juice were $nC_{25}$, $nC_{27}$, $nC_{29}$, and $nC_{31}$, $nC_{16}$, $nC_{17}$, $nC_{18}$, and $nC_{19}$ were abundant in seeds mainly. The concentration of malonic acid among the five organic acids was highest in leaves, stem, and flowers. Unripe fruit contained 24.5 mg/g of the five organic acids and malic and citric acids were higher. The concentrations of palmitic, linoleic, and linolenic acids were higher concentration in the various parts of sponge-gourd and palmitic acid was distributed in the most parts. The concentrations of organic and fatty acids in the sap were negligible.

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Deodorization of Swine Wastewater by Rhodospirillum rubrum N-1 (Rhodospirillum rubrum N-1을 이용한 양돈폐수의 악취제거)

  • Choi, Kyung-Min;Kim, Jong-Seung
    • Journal of the Korea Organic Resources Recycling Association
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    • v.6 no.1
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    • pp.13-20
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    • 1998
  • Rhodospirillum rubrum N-1 was inoculated to manipulated swine wastewater of 20,000 mg/L as Biochemical Oxygen Demand (BOD) to study the effect of aeration on swine wastewater deodorization. Biological and physico-chemical parameters were determined at 1 day interval for 9 days. Removals of BOD, volatile fatty acids (VFAs), and phosphate were 54.6%, 87.0%, and 54.5%, respectively. No significant changes were observed in the concentrations of total nitrogen, total phosphorus, nitrate, nitrite, hydrogen sulfide, and mercaptane.

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Studies on Chemical Composition of Raspberry (Free Amino Acids, Non-Volatile Organic Acids and Sugar) (나무딸기의 화학적(化學的) 성분(成分) 조성(組成)에 관한 연구(硏究) (유리아미노산, 유기산 및 유리당))

  • Joo, Kwang-Jee
    • Journal of Nutrition and Health
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    • v.11 no.3
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    • pp.21-24
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    • 1978
  • In order to estimate the chemical composition of Raspberry (IR Crataegifalius), the free amino acids were analyzed by amino acid autoanalyzer, and organic acids contents were determined by gas chromatography and the free sugars were detected by paper chromatography. The results obtained were as follows: 1) The free amino acids found in Raspberry were 18 kinds of them, especially, all essential amino acids were showed, and lysine was abundant among them, consequently it was found that the composition of amino acids in Raspberry is more superior than those of the other fruits. 2) The organic acids in Raspberry were found citric acid, tartaric acid, malic acid and fumaric acid. It was found that the quantity of the organic acids was less than those of other common fruits. 3) Sugar such as glucose, fructose, maltose and mannose were detected by paper chromatography.

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The Effects of Curing Variables on Quality and Chemical Properties of Oriental Tobacco (건조조건에 따른 오리엔트종 잎담배의 품질과 화학적 특성)

  • 류명현;이철환
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.34 no.2
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    • pp.204-210
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    • 1989
  • Normally cultured, harvested and yellowed leaves of aromatic tobacco variety. KA 101 were sun-cured under conventional polyethylene film house, air-cured in burley curing barn, and bulk-cured at three temperatures of 40$^{\circ}C$, 50$^{\circ}C$ and 60$^{\circ}C$. respectively, to investigate the effects of curing conditions on quality and chemical properties of leaf tobacco. Air-cured leaves had the poorest quality by price with little difference between that of sun-cured and three bulk-cured ones. Air-cured leaves were higher in ammonia nitrogen, protein nitrogen, total nitrogen, ash content and pH, but lower in sugar content when it compared with those of sun-cured and three bulk-cured ones. The curing variables tested did not affect the content of pet. ether ext. and volatile organic acids. The content of pet. ether ext., volatile organic acids, and most of volatile neutrals tended to decrease or not to change as the bulk-curing temperature increased. A quality index, (volatile organic acids, mg/l00g+% pet. ether ext.) / %(ash+pH) x 10, was found to be most accurate and easy to apply for the quality evaluation of aromatic tobaccos.

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Changes in Organic acids, Free Sugars, and Volatile Flavor Compounds in Fig (Ficus carica L.) by Maturation Stage (무화과의 성숙도에 따른 유기산, 유리당 및 향기 성분의 변화에 관한 연구)

  • Shin, Tai-Sun;Park, Jin-A;Jung, Bok-Mi
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.44 no.7
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    • pp.1016-1027
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    • 2015
  • This study collected 120 figs, classified them into six degrees of maturity according to hardness values, and analyzed contents of organic acids and free sugars. Volatile compounds in figs were investigated using the solid-phase microextraction method of gas chromatography/mass spectrometry. For measurement of texture, elasticity increased up to stage 4 and decreased again. Cohesiveness and brittleness increased with maturation. Organic acids in figs were mainly composed of citric acid, malic acid, and tartaric acid in the final stage. Fructose and glucose were the major sugar components of figs. Fructose content decreased from stage 1 to stage 4 and then increased significantly. One hundred and nineteen volatile compounds were identified in figs, and classes were 14 acids, 15 alcohols, 23 aldehydes, 10 esters, 33 hydrocarbons, 11 ketones, four aromatics, six miscellaneous, and five terpenes. The dominant volatile components in figs were hexadecanoic acid, hexane, dodecanal, DL-limonene, 2-hexanal, nonanal, and 6-methyl-5-hepten-2-one.