• Journal of Biomedical Engineering Research
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• v.42 no.6
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• pp.251-258
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• 2021

Hyaluronic acid (HA) microspheres (MSs) crosslinked with polyethylene glycol diglycidyl ether (PEGDE) are prepared using a simple fluidic device (SFD) to investigate the optimized parameters. A solution mixture of PEGDE in 2-methyl-1-propanol was prepared as a continuous phase in SFD. HA solutions of 1 wt% concentration were introduced into SFD as a discontinuous phase. The HA solution prepared by stirring for more than 48 h exhibited spherical MSs at the needle tip inside the ring cap. As the flow rate of the continuous phase increased from 0.7 to 1.9 mL/min, the diameter of the MS decreased from 173±36 ㎛ to 129±13 ㎛. Although the PEGDE concentration in the range of 0.2 to 1.8 vol% did not affect the diameter of the MS, the microstructure of MS, consisting of inner hollow void and wall, was changed. The inner void and wall size decreased and increased from 79.5 ㎛ to 57.2 ㎛ and from 10.3 ㎛ to 21.4 ㎛, respectively, with increasing PEGDE concentration from 0.2 vol% to 1.8 vol%. FT-IR peaks located around 2867 cm^-1 and 1088 cm^-1 indicated that the HA MS prepared at different PEGDE concentrations were chemically crosslinked. The HA MSs containing different PEGDE concentrations exhibited quantitative cell viability of more than 98%. L-929 cells adhered well to the HA MSs and proliferated continuously with increasing culture time to 48 h regardless of PEGDE concentration, implying that the HA MSs are clinically safe and effective.

• Restorative Dentistry and Endodontics
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• v.46 no.2
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• pp.25.1-25.12
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• 2021

Objectives: This study used micro-computed tomography (µCT) to compare voids and interfaces in single-cone obturation among AH Plus, EndoSequence BC, and prototype surface pre-reacted glass ionomer (S-PRG) sealers and to determine the percentage of sealer contact at the dentin and gutta-percha (GP) interfaces. Materials and Methods: Fifteen single-rooted human teeth were shaped using ProTaper NEXT size X5 rotary files using 2.5% NaOCl irrigation. Roots were obturated with a single-cone ProTaper NEXT GP point X5 with AH Plus, EndoSequence BC, or prototype S-PRG sealer (n = 5/group). Results: The volumes of GP, sealer, and voids were measured in the region of 0-2, 2-4, 4-6, and 6-8 mm from the apex, using image analysis of sagittal µCT scans. GP volume percentages were: AH Plus (75.5%), EndoSequence BC (87.3%), and prototype S-PRG (94.4%). Sealer volume percentages were less: AH Plus (14.3%), EndoSequence BC (6.8%), and prototype S-PRG (4.6%). Void percentages were AH Plus (10.1%), EndoSequence BC (5.9%), and prototype S-PRG (1.0%). Dentin-sealer contact ratios of AH Plus, EndoSequence BC, and prototype S-PRG groups were 82.4% ± 6.8%, 71.6% ± 25.3%, and 70.2% ± 9.4%, respectively. GP-sealer contact ratios of AH Plus, EndoSequence BC, and prototype S-PRG groups were 65.6% ± 29.1%, 80.7% ± 25.8%, and 87.0% ± 8.6%, respectively. Conclusions: Prototype S-PRG sealer created a low-void obturation, similar to EndoSequence BC sealer with similar dentin-sealer contact (> 70%) and GP-sealer contact (> 80%). Prototype S-PRG sealer presented comparable filling quality to EndoSequence BC sealer.

• Proceedings of the KSME Conference
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• 2004.11a
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• pp.1158-1161
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• 2004

Shell shaped hollow carbon nanoparticles are synthesized in the oxygen-hydrogen diffusion flame with $C_{2}H_{2}$ as precursor when it is irradiated with $CO_{2}$ laser of certain power. Below this power of laser, we couldn't get any other but amorphous soot. This shell shaped hollow carbon nanoparticles shows outer wall of high degree of crystallinity with void space inside of itself. And size distribution of these nanoparticles is measured with TEM image analysis. Also the structural comparison between this carbon nanoparticle and soot is done by Raman and XRD measurement. These results show this carbon nanoparticles are of grapheme structure, which means it has good crystallinity when compared with soot.

• Transactions of the Korean Society of Mechanical Engineers
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• v.10 no.4
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• pp.477-486
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• 1986

본 연구에서는 SM20C를 모재로 하여 입경의 크기가 다른 3종의 복합조직강을 제작 동일한 분위기에서 저 및 고사이클 전영역에 걸쳐 피로특성을 검토하고져 한다. 제일보는 그 중 저사이클특성에 대한 보고이다. 일반적으로 저사이클 피로현상은 재 료가 탄소성 상태하에서 전위, 미소크랙, 보이드(void) 등의 인자가 복합적으로 작용 하여 발생함으로 변형률속도, 제어파형, 온도, 시험방법 및 분위기에 따라 많은 영향 을 받는다. 따라서 본 연구에서는 두가지 실험방법을 사용, 응력-변형율거동을 검토 복합조직강의 피로특성과 입경크기가 피로거동 및 강도에 미치는 영향을 비교 고찰하 였다.

• Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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• 2001.06a
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• pp.1011-1011
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• 2001

In general, NIR reflectance spectra (whether recorded using log(1/R) or the Kubelka-Munk function) are not linear functions of the concentration of the absorbers which we are measuring. There are several causes for this non-linearity, the most commonly cited one being front surface reflection. However, non-linearity also arises from the effects of particle size, sample thickness, void fraction, and experimental arrangement. In this talk, we will attempt to isolate the effects of the various causes, and show the effects of each, using both theoretical calculations and actual data. The listener should then be able to assess where we stand in our quest to produce “linear” data through pre-processing and/or alternate collection schemes.

• Proceedings of the Korean Society of Agricultural Engineers Conference
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• 2002.10a
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• pp.201-204
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• 2002

This study is performed to develop of planting block using rice straw ash for Protection of Inclined plane. For the planting, porous concrete block is demanded ability to passing water and air through void of block. In this paper, material used for porous concrete block is cement, rice straw ash, and coarse aggregate(5-10, 10-20, 5-20mm). Planting block size is 23*23*4cm and kinds of planting are Tall fescue, Lespedeza cyrtobotrya and Lespedeza cuneata. The results measured for three months show that possible planting of various kinds for porous concrete block.

• Advances in environmental research
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• v.1 no.4
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• pp.305-321
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• 2012

This study entails establishing reference standard sand in Nigeria for engineering and geoenvironmental research work. Sands from four geographical locations in southwestern Nigeria were examined for baseline geotechnical and mineralogical properties. A total of sixteen sand samples were collected. The samples were air dried and subjected to tests in accordance with standard specifications. The tests carried out were: specific gravity, grain size analysis, moisture content, bulk density, porosity, void ratio, chemical analysis, X-ray diffraction and Differential Thermal Analysis. The properties of the samples were compared with a standard (Ottawa sand in Illinois of the United States) in order to find out which of the four samples selected from southwestern Nigeria could serve as standard baseline sand. The results show that Igbokoda sand has geotechnical and mineralogical characteristics closest to Ottawa sand. It was therefore concluded that Igbokoda sand could be used as a standard baseline sand for research work in southwestern Nigeria and other parts of Nigeria since it needs little processing to bring it to the same level as standard baseline sand, like the Ottawa sand.

• Proceedings of the Korean Society of Agricultural Engineers Conference
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• 2001.10a
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• pp.375-378
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• 2001

This study was peformed to understand permeability characteristic of clays with various pH values. A serious of physical properties and permeability tests, consolidation tests was performed on a clay and a marine clay. Results of the study are as follows. As pH values were decreased, coefficient of permeability was increased because of increase in effective void caused by decrease in thickness of diffuse double layer besides change in soil structures and effective grain size. As pH values were increased, coefficient of permeability of marine clay was increased. Variation of coefficient of permeability of marine clay was increased. Variation of coefficient of permeability of marine clay was largely related because of higher clay contents.

• Transactions of Materials Processing
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• v.9 no.5
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• pp.533-538
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• 2000

This study has been carried out to develop a CRT die using hot forging. The conventional CRT die made by casting has defects such as void and inclusion. These defects of the cast die make micro-spots on the surface of the CRT which affect the quality of the final product. So, a hot forging process is developed to avoid these defects of CRT die by the model material test and the rigid-plastic FEM. Firstly, model material tests are carried out with plasticine billets in order to investigate the material flow pattern in the die cavity and to get the reasonable initial values for designing the preform in the FE simulation. And then a finite element analysis has been performed to Predict the preform and the forging load of a CRT die. We also suggest an integrated die-set which combines two die-sets into one die-set to save manufacturing time and cost in case of similar die-size.

• Proceedings of the Korean Geotechical Society Conference
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• 2010.03a
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• pp.717-721
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• 2010

Soil volume conversion factors are used for estimation of an excavated the soil volume which will be removed or added in levelling the ground surface of a construction site. An accurate evaluation method will help us reduce a construction cost and time consuming. In this study, we performed the laboratory tests, including grain size measurement, water content, specific gravity, porosity, density and XRD tests, to suggest reliable soil volume conversion factors and weathering indices in field using nondestructive methods. The weathering index and soil volume conversion factor L are obtained for different types of soils. At results, the CIW index is the best method measuring the weathering index and the factor L is relative to natural porosity, void ratio, density and dry density.