• The Journal of Korean Academy of Prosthodontics
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• v.59 no.2
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• pp.190-200
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• 2021

Purpose. The aim of this study was to evaluate biaxial flexural strength and hardness of colored monolithic zirconia after dipping in different time intervals of coloring solution. Materials and Methods. Disk shaped specimens were prepared from monolithic zirconia (Eclipse V2.0, AMS, Gimpo, Korea). Four experimental groups were categorized (n = 12) due to coloring time (PU (0s); ST (8s); OV (1 min); PS (preshade)), to evaluate biaxial flexural strength and Vickers hardness. After fracture, X-ray diffraction analysis was performed using fractured specimens. Results were analyzed with one-way ANOVA test. Results. There was no significant difference between groups in the biaxial flexural strength test. However, in the Vickers hardness test, the group with standard dipping time (ST) showed significantly higher value than the group without dipping in coloring liquid (PU)(P=.038). Also, there was no significant difference in the rest of the groups (P>.05). As a result of X-ray diffraction analysis, specific peaks of tetragonal phase were shown and the volume of monoclinic phase fraction was lower than 25%. Conclusion. Although this study has several limitations, coloring liquids had no significant effect on biaxial flexural strength. Vickers hardness was significantly different between the group to which the coloring liquid was applied and the group to which the coloring solution was not applied, but there was no significant difference between the other groups. Also, the flexural strength of monolithic zirconia corresponds to Class 5 of the minimal flexural strength standard according to the use of dental ceramics.

• Journal of Power System Engineering
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• v.21 no.3
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• pp.37-44
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• 2017

In this study, failure analysis of the angular pin for molding machines to aluminum component molding was carried out. SM45C steel was used for the angular pin, it was surface hardened by the induction surface hardening heat treatment. The cross section of damaged angular pin was observed, and micro Vickers hardness value from the fractured part was measured. Brittle fracture was occurred from the fracture surface of angular pin, therefore, impact toughness value was evaluated by V-notch Charpy impact test. It was confirmed that the impact absorption energy was high when was tempered at a high temperature for a long time, and the toughness was slightly increased. Also, 2-parameter Weibull statistical analysis was investigated in order to evaluate the reliability of the measured micro Vickers hardness values and absorbed energy. The micro Vickers hardness and absorbed energy well followed a two-parameter Weibull probability distribution, respectively. The reverse design against angular pin was proposed as possible by using test results.

• Korean Journal of Materials Research
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• v.18 no.11
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• pp.604-609
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• 2008

The sintering behavior of zircon with silica was investigated. Zircon with 5 vol% of sedimentation $SiO_2$ resulted in the apparent density of $4.45\;g/cm^3$, the diametral tensile strength of $12.125\;kgf/cm^2$, and the micro Vickers hardness of 1283 HV. The dissociation temperature and mechanical characteristics of the $ZrSiO_4$ were changed with different kinds of $SiO_2$. $SiO_2$ addition prevented dissociation of $ZrSiO_4$. Zircon with 5 vol% of sedimentation $SiO_2$ and with 5 vol% of fused $SiO_2$ resulted in increased diametral tensile strength and increased micro Vickers hardness by suppression of $ZrSiO_4$ dissociation and low temperature liquid $SiO_2$ formation. Zircon with fumed $SiO_2$ and quartz $SiO_2$ resulted in decreased diametral tensile strength and decreased micro Vickers hardness because of cristobalite and quartz phase formation and high temperature liquid $SiO_2$ formation. Zircon with 10 vol% of $SiO_2$ resulted in decreased diametral tensile strength and decreased micro Vickers hardness because of weak particle coupling due to excess formation of liquid $SiO_2$.

• Journal of the Korean Society for Precision Engineering
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• v.12 no.2
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• pp.5-13
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• 1995

Various techniques to measure fracture toughness which is an important parameter to predict fracture behavious of structural materials have been reported. Among these mathods, this paper describes the micro-Vickers indentation crack method to estimate the fracture toughness of some WC-Co composites. Two indentation crack patterns (such as radial-median cracks (orhalf-penny cracks) and Palmqvist cracks generated during indentation) are referred precisely. The fracture toughness of WC-4.7wt%Co, WC-6wr%Co and WE-9wr%Co composites were estimated by using some equations given by Shetty et al., Nihara et al. in this study. We show the reliability of indentation method by comparing the results with those from literatures. The appropriate equation to estimate the fracture toughness in the case of WC-Co composite is given. In addition, some technical informations in terms of the crack length by indentation in estimating the existence of the surface residual stress that prevents to obtain an accurate fracture toughness are presented.

• Journal of Technologic Dentistry
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• v.27 no.1
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• pp.73-78
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• 2005

The surface-reacted layer of titanium castings greatly affects their mechanical properties. This study analyzed the interfacial zone of Ti-20%Zr-5%Cr alloy castings obtained from phosphate bonded investment and examined the relationship between the surface-reacted layer and hardness. The Vickers hardness of cast disks were tested at 20$\mu m$ intervals from the surface to 120$\mu m$ in depth. The cross-section was observed metallurgically, and line profile of the reacted layer was conducted under the EDX. The surface-reacted layer of Ti-20%Zr-5%Cr alloy is showed a similar tendency to Ti-6%Al-4%V alloy in thickness, and also Si diffusion in multiple reacted layer of Ti-20%Zr-5%Cr alloy is less than cp Ti and similar to Ti-6%Al-4%V alloy. The Vickers hardness in the surface layer was greater than in the inner part, and the Vickers hardness of Ti-20%Zr-5%Cr alloy ranged 650 to 390 and cp Ti ranged 810 to 160, Ti-6%Al-4%V alloy ranged 710 to 530 respectively.

• Journal of Power System Engineering
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• v.20 no.5
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• pp.5-13
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• 2016

This study is on wear damage of the material for a molding machine that be used at finally cutting of metal beam made in roll forming process of vehicle bump beam process line. SKD11 steel was used with the material for cutting mold jig. In the cutting mold jig, Ti diffusion heat treatment after vacuum heat treatment was carried out for upgrade of surface hardness and anti-wear. Also, the heat treatments by various methods were performed to compare the wear damage degree against above the existing heat treatment. Wear loss and friction coefficient were obtained from wear test. And, micro Vickers hardness values were compared with damaged parts or not of cutting mold jig. Micro Vickers hardness value appeared higher at the undamaged part by Ti diffusion heat treatment. The micro Vickers hardness well followed a two-parameter Weibull probability distribution.

• Journal of the Korean institute of surface engineering
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• v.46 no.1
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• pp.48-53
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• 2013

In the present work, it was investigated a behavior of hydrogen embrittlement at the subsurface zones of 590 DP steels by using the micro-Vickers hardness test. The micro-Vickers hardnessess of DP steels were measured to evaluate the degree of embrittlement as the effective hardening depths of subsurface zones with hydrogen charging conditions. The results showed that the distributions of micro-Vickers hardness in width varied from maximum hardness 239.5 Hv to minimum hardness 174 Hv, while the depth of effective hardening layer at the subsurface zones of DP steels was from $320{\mu}m$ to $460{\mu}m$ with hydrogen charging conditions, respectively. It was proposed that the distribution of microhardness be used as the evaluation index of the degree of embrittlement. But the variations of martensite volume fractions were not affected along depth of hardening at the same changing time, hydrogen charging times were appeared as an effective factor of the degree of embrittlement. Therefore, the micro-Vickers hardness test is an attractive tool for evaluation of hydrogen embrittlement at the subsurface zones of these DP steels.

• Journal of the korean academy of Pediatric Dentistry
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• v.51 no.2
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• pp.165-175
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• 2024

This study aimed to investigate the effects of blood contamination on the Vickers hardness and the surface morphology of premixed MTA and compare them with the effects on conventional MTA. The Vickers microhardness of Endocem MTA Premixed Regular (EP) and ProRoot MTA (PM) was assessed after immersion in fetal bovine serum (FBS) and saline. Stem cells from human exfoliated deciduous teeth (SHED) were seeded on MTA after immersion in FBS, saline, and deionized water (DW). Cell adhesion patterns and surface morphology were visualized via scanning electron microscopy (SEM). The surface microhardness of EP and PM in FBS was lower than in saline. However, short-term exposure of PM to FBS did not reduce the microhardness compared to saline. Angular crystals formed in water, while rounded crystals with more air voids appeared in FBS. Favorable SHED attachment occurred in all groups. Overall, the surface hardness of EP and PM decreased after FBS exposure, although PM was less influenced. We suggest minimizing the amount of bleeding when using MTA clinically; nevertheless, PM remains an option with more expected blood contamination than EP. In summary, exposure to FBS decreased mechanical performance but allowed cell adhesion for both MTAs, with PM being more resistant to these changes.

• Journal of the Korean Magnetics Society
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• v.8 no.5
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• pp.249-254
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• 1998

In relation to the application of magnetic method to the evaluation of irradiation damage (embrittlement) changes in the magnetic parameters(hysteresis loop and Barkhausen noise) and Vickers microhardness due to neutron irradiation and heat treatment were measured and compared. In the case of irradiation $(2.3{\times}10^{19}\;n/cm^2,\; E{\ge}1\;Mev,\; 288{\circ}C)$ hysteresis loop measurements show that susceptibility decreases as coercivity increase. Saturation magnetization do not show any change. Barkhausen noise amplitude and Barkhausen noise energy have decreased while Vickers microhardness has increased. For isothermally heat treated condition of irradiated specimen at 470 $^{\circ}C$ and 540 $^{\circ}C$, Barkhausen noise energy has increased while Vickers microhardness has decreased. Results of BNE and Vickers microhardness are reversed to the results on irradiated condition. All these consistent changes in magnetic parameter and Vickers microhardness measurement, which are thought to be resulted from the interaction between irradiation-induced defects and dislocation, and magnetic domain, respectively, show a possibility that magnetic measurement may be used to the evaluation of material degradation and recovery due to neutron irradiation and heat treatment, respectively, if a relevant large database in prepared.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.40 no.12
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• pp.987-995
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• 2016

In this study, the effects of shot peening (SP) on the Vickers hardness of $ZrO_2$ were studied. The size of the shot balls were ${\phi}180{\mu}m$ and ${\phi}300{\mu}m$. The Vickers hardness was measured using an indentation load of 98 N and 294 N. The Vickers hardness was evaluated using Weibull statistical analysis. The scale parameters were significantly evident from the indentation load of 98 N and the shot ball of ${\phi}180 {\mu}m$. Generally, the shape parameters were also evident from the small short ball (180sp). Thus, it is shown that the introduction of a compressive residual stress by SP is an effective technique for increasing the mechanical properties of $ZrO_2$.