• 제목/요약/키워드: Various starting materials

검색결과 197건 처리시간 0.025초

나노입자 혼합 복합슬러리를 이용한 반응소결 SiC 재료의 제조 (Fabrication of Reaction Sintered SiC Materials by Complex Slurry with Nano Size Particles)

  • 이상필
    • 대한기계학회논문집A
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    • 제29권3호
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    • pp.425-431
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    • 2005
  • The efficiency of complex slurry preparation route for developing the high performance SiC matrix of $RS-SiC_{f}/SiC$ composites has been investigated. The green bodies for RS-SiC materials prior to the infiltration of molten silicon were prepared with various C/SiC complex slurries, which associated with both the sizes of starting SiC particles and the blending conditions of starting SiC and C particles. The characterization of Rs-SiC materials was examined by means of SEM, EDS and three point bending test. Based on the mechanical property-microstructure correlation, the process optimization is also discussed. The flexural strength of Rs-SiC materials greatly depended on the content of residual Si. The decrease of starting SiC particle size in the C/SiC complex slurry was effective for improving the flexural strength of RS-SiC materials.

An Environmentally-friendly Precursor, Ferrous Acetate, in preparation for Monodisperse Iron Oxide Nanoparticles

  • Suh, Yong-Jae;Kil, Dae-Sup;Chung, Kang-Sup;Lee, Hyo-Sook;Shao, Huiping
    • Journal of Magnetics
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    • 제13권3호
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    • pp.106-109
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    • 2008
  • Almost monodisperse iron oxide nanoparticles with an average particle size ranging from 5 to 43 nm were fabricated using an environmentally friendly starting material, ferrous acetate. The smallest particles were formed in the presence of a reductant, 1,2-dodecanediol, while the particle size increased with increasing concentration of dispersing agents. The dispersants consisted of various combinations of oleic acid, oleylamine, trioctylphosphine, and polyvinylpyrrolidone. The threshold temperature to form crystalline particles was found to be $240^{\circ}C$. The 43 nm nanoparticles exhibited a room temperature saturation magnetization and coercivity of 57 emu/g and 47 Oe, respectively.

반응소결 SiC 재료의 미세조직 및 강도 특성 (Microstructure and Strength Property of Reaction Sintered SiC Materials)

  • 이상필;신윤석;이진경
    • 한국해양공학회:학술대회논문집
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    • 한국해양공학회 2004년도 학술대회지
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    • pp.380-385
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    • 2004
  • The efficiency of complex slurry preparation route for developing the high performance SiC matrix of RS-SiCf/SiC composites has been investigated. The green bodies for RS-SiC materials prior to the infiltration of nw/ten silicon were prepared with various C/SiC complex matrix slurries, which associated with both different sizes of starting SiC particles and blending ratios of starting SiC and carbon particles. The characterization of RS-SiC materials was examined by means of SEM, TEM, EDS and three point bending test. Based on the mechanical property-microstructure correlation, process optimization methodology is also discussed. The flexural strength of RS-SiC materials greatly depended on the content of residual Si. The decrease of starting SiC particle size in the C/SiC complex slurry was effective for improving the flexural strength of RS-SiC materials.

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Circulating Mechanism of the Oil in Brief Operating for the Oil-impregnated Sintered Bearing

  • Harakawa, Toshiro;Maruyama, Tsuneo;Shimizu, Teruo
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.1006-1007
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    • 2006
  • The oil-impregnated sintered bearings are used for various aplecations and, wide usages without refueling. The oil circulating mechanism operates smoothly the behavior of oil If doing at the time of passing and becoming a stationary state, and there is little thing where trouble is caused. On the other hand, the trouble of such as starting noise might be caused in the unstationary state that repeats operation for a short time. To study the behavior of oil of each parameter, we execute the numerical simulation and various verification experiments. As a result, we developed that the bearings were able to be used enough for various brief operating time in the unstationary state. Finally we have expanded the usage of the oil-impregnated sintered bearings by adding the consideration of the behavior of oil.

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국산자기재료를 이용한 비대칭자속분포 단상유도기구 (A Study On The Performances Of A Single-Phase Motor With Non-Quadrature Stator Windings Using Domestic Magnetic Materials.)

  • 박민호
    • 전기의세계
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    • 제21권3호
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    • pp.41-47
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    • 1972
  • The requirements of a successful design for single phase induction motors with a high efficiency have, in recent years, led to the use of non-quadrature stator windings motors in which a high starting torque is a prime requisite. The capacitor motor is one of above machines in which various possible forms of asymmetry can be occur. These forms of asymmetry in the stator phase windings, encountered in machine designs, are 1) an asymmetrical disposition in space of their magnetic axes, 2) a difference in their effective number of turns, 3) a difference in the distribution of their coil groups per pole and 4) amounts of capacitance of an auxiary winding. In order to apply the effective performance prediction of these form to motors, mading of lower quality-domestic magnetic materials, the analysis and the experimental investigations of its sample motors are described in this paper. The utility of such a motor is demonstrated and it is shown that the effects- a good efficiency, good power factor and high starting torque-of the motor mechanism with non-quadrature stator phase windings can development disadvantages by using the lower quality-domestis magnetic materials.

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수열합성법으로 제조된 PZT 분말의 특성에 미치는 광화제 농도와 출발물질의 영향 (Effect of Mineralizer Concentration and Starting Materials on the Characteristics of PZT Powders by Hydrothermal Process)

  • 양범석;윤기석;박영철;원창환
    • 한국세라믹학회지
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    • 제42권11호
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    • pp.743-748
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    • 2005
  • The effect of reaction parameters in the characteristic of $Pb(Zr_{0.52} Ti_{0.48})O_3$ powders by hydrothermal process was investigated in this study. In the preparation of PZT, the types of starting material and concentration of mineralizer on phase fraction and morphology was investigated respectively. Regardless the types of Pb precursor, PZT was able to synthesize ranging from 7 to 20 on KOH concentration and from 13.01 to 13.55 on pH of solution. The particle size of the PZT powders can be controlled by the mineralizer concentration and various types of precursor.

Synthesis of Cobalt Oxide Film by Thermal Decomposition for Potential Various Applications

  • Han, Seong Ho;Park, Bo Keun;Son, Seong Uk;Kim, Chang Gyoun;Chung, Taek-Mo
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2014년도 제46회 동계 정기학술대회 초록집
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    • pp.365.1-365.1
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    • 2014
  • Cobalt oxide has excellent various properties such as high catalytic activity, antiferromagnetism, and electrochromism. So cobalt oxides offer a great potential for their applications in the various areas such as optical gas sensor, catalysts for oxidation reaction, electrochromic devices, high temperature solar selective absorbers, magnetic materials, pigment for glasses and ceramics, and negative electrodes for lithium-ion batteries. We have synthesized novel cobalt complexes by simple reaction of cobalt bistrimethylsilylamide as a starting material with a lot of conventional ligands as potential cobalt oxide precursors. The studies include the facile preparation, structural characterization, and spectroscopic analysis of the new precursors. We are making efforts to grow cobalt oxide thin films using cobalt complexes newly synthesized in this study using deposition techniques.

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Fe-TiC 복합재료분말의 방전플라즈마소결 (Spark Plasma Sintering of Fe-TiC Composite Powders)

  • 이용희;;김지순
    • 한국분말재료학회지
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    • 제21권5호
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    • pp.382-388
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    • 2014
  • Fe-TiC composite powder was fabricated by high-energy milling of powder mixture of (Fe, TiC) and (FeO, $TiH_2$, C) as starting materials, respectively. The latter one was heat-treated for reaction synthesis of TiC phase after milling. Both powders were spark-plasma sintered at various temperatures of $680-1070^{\circ}C$ for 10 min. with sintering pressure of 70 MPa and the heating rate of $50^{\circ}C/min$. under vacuum of 0.133 Pa. Density and hardness of the sintered compact was investigated. Fe-TiC composite fabricated from (FeO, $TiH_2$, C) as starting materials showed better sintered properties. It seems to be resulted from ultra-fine TiC particle size and its uniform distribution in Fe-matrix compared to the simply mixed (Fe, TiC) powder.

반응소결 SiC 재료의 제조 및 특성 (Fabrication and Characterization of Reaction Sintered SiC Based Materials)

  • 진준옥;이상필;박이현;황희진;윤한기
    • 한국해양공학회:학술대회논문집
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    • 한국해양공학회 2003년도 춘계학술대회 논문집
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    • pp.294-299
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    • 2003
  • The efficiency of complex slurry preparation route for the development of high performance RS-SiCf/SiC composites has been investigated. The green bodies for RS-SiC and RS-SiCf/SiC composite materials prior to the infiltration of molten silicon were prepared with various C/SiC complex matrix slurries, which associated with both different sizes of starting SiC particles and blending ratios of starting SiC and carbon particles. The reinforcing materials in the composite system were uncoated and C coated Tyranno SA SiC fiber. The characterization of RS-SiC and RS-SiCf/SiC composite materials was examined by means of SEM, EDS and three point bending test. Based on the mechanical property-microstructure correlation, process optimization methodology is discussed.

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현대 패션디자인의 금속소재 연구 -모드사적 분석과 조형성를 중심으로- (Study on Metal material in Contemporary Fashion -Focus on analysis of mode history and the normativeness-)

  • 이영재
    • 한국의류학회지
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    • 제26권5호
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    • pp.582-593
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    • 2002
  • Metal materials have been used in the clothing design on the spirit of ingenious experiment by fashion designers, and they have been put to practical use by several designers who work out a scheme of popular fashion merchandise. This current starting from the 1960s was weakened in the 1980s, but it was appeared with various shapes of metal materials in the 1990s due to a popularity of techno/cyber fashion. Recently, textile engineering technology causes to develop new-materials which are practical and sanitary. The development of fashionable metal materials brings about the popularization of fashion with metal materials, and it induces that mainstream of modem fashion has been changed into designers of pursuing the spirit of ingenious experiment. This study examines the formative characteristics of metal materials that are based on the spirit of ingenious experiment. As a result, it is evaluated that the formative of metal materials shown in modern fashion is futurism, visual concentration, avast-garde, resistance, precious.