• Title/Summary/Keyword: Vacuum condition

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The Effect of Heat Treatment on the Microstructures and Mechanical Properties of Inconel 713C Alloy Vacuum Investment Castings (진공 정밀주조한 Inconel 713C 합금의 조직과 기계적 성질에 미치는 열처리의 영향)

  • Yoo, Byung-Ki;Choi, Hak-Kyu;Park, Heung-Il;Jeong, Hae-Yong
    • Journal of Korea Foundry Society
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    • v.40 no.2
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    • pp.16-24
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    • 2020
  • The effect of a heat treatment on the microstructure and mechanical properties of Inconel 713C alloy vacuum investment castings were investigated. The microstructure of the as-cast state was observed, showing well-developed dendrite structures and distributed carbide particles and solidified massive precipitates in the grain or grain boundary during solidification, in this case the γ′ phase and MC particles. During a heat treatment, the γ phase matrix was reinforced by solid solution elements, carbide particles from the film morphology precipitated along the grain boundary, and many micro-precipitates of second γ′ phases 0.2 ㎛~2 ㎛ in size were newly formed in the γ phase matrix according to SEM-EDS analysis results. The tensile strength at a high temperature (850℃) decreased slightly becoming comparable with the room-temperature result, while the hardness value of the specimen after the vacuum heat treatment increased by approximately 19%, becoming similar to that of the as-cast condition. However, the impact values at room temperature and low temperature (-196℃) were approximated; this alloy was mostly not affected by an impact at a low temperature. In the observations of the fracture surface morphologies of the specimens after the tensile tests, the fractures at room temperature were a mix of brittle and ductile fractures, and an intergranular fracture in the inter-dendrite structure and some dimples in the matrix were observed, whereas the fractures at high temperatures were ductile fractures, with many dimples arising due to precipitation. It was found that a reinforced matrix and precipitates of carbide and the γ′ phase due to the heat treatment had significant effects, contributing greatly to the excellent mechanical properties.

Comparative Study on Microwave Probes for Plasma Density Measurement by FDTD Simulations

  • Kim, D.W.;You, S.J.;Na, B.K.;Kim, J.H.;Chang, H.Y.;Oh, W.Y.
    • Proceedings of the Korean Vacuum Society Conference
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    • 2014.02a
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    • pp.218.1-218.1
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    • 2014
  • In order to measure the absolute plasma density, various probes are proposed and investigated and microwave probes are widely used for its advantages (Insensitivity to thin non-conducting material deposited by processing plasmas, High reliability, Simple process for determination of plasma density, no complicate assumptions and so forth). There are representative microwave probes such as the cutoff probe, the hairpin probe, the impedance probe, the absorption probe and the plasma transmission probe. These probes utilize the microwave interactions with the plasma-sheath and inserted structure (probe), but frequency range used by each probe and specific mechanisms for determining the plasma density for each probe are different. In the recent studies, behaviors of each microwave probe with respect to the plasma parameters of the plasma density, the pressure (the collision frequency), and the sheath width is abundant and reasonably investigated, whereas relative diagnostic characteristics of the probes by a comparative study is insufficient in spite of importance for comprehensive applications of the probes. However, experimental comparative study suffers from spatially different plasma characteristics in the same discharge chamber, a low-reproducibility of ignited plasma for an uncertainty in external discharge parameters (the power, the pressure, the flow rate and so forth), impossibility of independently control of the density, the pressure, and the sheath width as well as expensive and complicate experimental setup. In this paper, various microwave probes are simulated by finite-different time-domain simulation and the error between the input plasma density in FDTD simulations and the measured that by the unique microwave spectrums of each probe is obtained under possible conditions of plasma density, pressure, and sheath width for general low-temperature plasmas. This result shows that the each probe has an optimum applicable plasma condition and reliability of plasma density measurement using the microwave probes can be improved by the complementary use of each probe.

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Design of closed-loop nitrogen Joule-Thomson refrigeration cycle for 67 K with sub-atmospheric device

  • Lee, C.;Lee, J.;Jeong, S.
    • Progress in Superconductivity and Cryogenics
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    • v.15 no.1
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    • pp.45-50
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    • 2013
  • Closed-loop J-T (Joule-Thomson) refrigeration cycle is advantageous compared to common open loop $N_2$ decompression system in terms of nitrogen consumption. In this study, two closed-loop pure $N_2$ J-T refrigeration systems with sub-atmospheric device for cooling High Temperature Superconductor (HTS) power cable are investigated. J-T cooling systems include 2-stage compressor, 2-stage precooling cycle, J-T valve and a cold compressor or an auxiliary vacuum pump at the room temperature. The cold compressor and the vacuum pump are installed after the J-T valve to create sub-atmospheric condition. The temperature of 67 K is possible by lowering the pressure up to 24 kPa at the cold part. The optimized hydrocarbon mixed refrigerant (MR) J-T system is applied for precooling stage. The cold head of precooling MR J-T have the temperature from 120 K to 150 K. The various characteristics of cold compressor are invstigated and applied to design parameter of the cold compressor. The Carnot efficiency of cold compressor system is calculated as 16.7% and that of vacuum pump system as 16.4%. The efficiency difference between the cold compressor system and the vacuum pump system is due to difference of enthalpy change at cryogenic temperature, enthalpy change at room temperature and different work load at the pre-cooling cycle. The efficiency of neon-nitrogen MR J-T system is also presented for comparison with the sub-atmospheric devices. These systems have several pros and cons in comparison to typical MR J-T systems such as vacuum line maintainability, system's COP and etc. In this paper, the detailed design of the subcooled $N_2$ J-T systems are examined and some practical issues of the sub-atmospheric devices are discussed.

Effect of Dietary Processed Sulfur on the Meat Quality in Pork under Aging

  • Hwa, Sung-Hyun;Kim, Ji-Han;Kim, Jung-Ho;Jang, Hyun-Ju;Ju, Min-Gu;Cho, Wonyoung;Lee, Chi-Ho
    • Food Science of Animal Resources
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    • v.36 no.6
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    • pp.760-768
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    • 2016
  • The present study was performed to determine the effect of dietary supplementation with processed sulfur on the quality and stability of vacuum packaged pork during aging time. All groups were designated into two groups; NP, a group fed basal diet and SP, a group fed basal diet and processed sulfur, 3 g/kg feed. Following vacuum packaging, Longissimus dorsi muscles were vacuum-packaged and stored under refrigerated condition ($1-2^{\circ}C$) for 21 d. Weight loss of the SP group was lower (p<0.05) than that of the NP group. Interaction effect of shear force and cooking loss was observed (p<0.05). Redness values of the SP group at 14 and 21 d after storage were higher than those of the NP group (p<0.05). Lipid oxidation and volatile basic nitrogen (VBN) levels in the SP group were retarded (p<0.05) compared to that of the NP group during storage. Aspartic and glutamic acid in SP were higher than in NP (p<0.1). There was no significant (p>0.05) difference in TPC between the both groups during storage. Therefore, vacuum packaged pork from pigs fed processed sulfur had better aging yield and storage stability than pork from pigs fed basal diet.

Study on the deposition rate and vapor distribution of Al films prepared by vacuum evaporation and arc-induced ion plating (증착방법에 따른 Al 피막의 증착율 및 증기분포에 관한 연구)

  • 정재인;정우철;손영호;이득진;박성렬
    • Journal of the Korean Vacuum Society
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    • v.9 no.3
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    • pp.207-215
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    • 2000
  • Al films on cold-rolled steel sheet have been prepared by vacuum evaporation and arc-induced ion plating, respectively, and the evaporation rate and vapor distribution (thickness distribution over the substrate) have been investigated according to deposition conditions. The arc-induced ion plating (AIIP) method have been employed, which makes use of arc-like discharge current induced by ionization electrode located near the evaporation source. The AIIP takes advantage of high ionization rate compared with conventional ion plating, and can be carried out at low pressure of less than $10^{-4}$ torr. Very high evaporation rate of more than 2.0 mu\textrm{m}$/min could be achieved for Al evaporation using alumina liner by electron beam evaporation. The geometry factor n for the $cos^{n/\phi}$ vapor distribution, which affects the thickness distribution of films at the substrate turned out to be around 1 for vacuum evaporation, while it features around 2 or higher for ion plating. For the ion plated films, it has been found that the ionization condition and substrate bias are the main parameters to affect the thickness distribution of the films.

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Characteristics of Vacuum Consolidation by Comparing with Surcharge Loading Consolidation (성토재하공법과 비교한 진공압밀공법의 압밀특성 분석)

  • Sim, Dong-Hyun;Lee, Jae-Hwan;Jeong, Sang-Seom
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.30 no.5C
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    • pp.201-208
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    • 2010
  • In this study, the ground settlement was investigated by using monitoring data of the test sites where vacuum consolidation method and surcharge method were applied for improving deep soft soil. The monitoring data are chosen in ${\bigcirc}{\bigcirc}$ area port construction site reclaimed with very soft dredged clay. These data are analyzed to compare the consolidation characteristics between the different loading methods for soil improvement. Through analysis of the loading time, it is shown that the ground settlement reaches its allowable value under vacuum consolidation loading by about 45% faster than that of the surcharge loading consolidation. This could be explained that vacuum consolidation method makes the isotropic consolidation condition so that the time for reaching a certain final preloading without soil failure can be shortened.

Storage condition that induce black heart of potato (Solanum tuberosom L.)

  • Jin, Yong-Ik;Chang, Dong-Chil;Cho, Ji-Hong;Yu, Dong-Lim;Nam, Jeong-Hwan;Yu, Hong-Seob;Koo, Bon-Choel;Choi, Jong-Kun;Lee, Soon-Ae
    • Proceedings of the Korean Society of Crop Science Conference
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    • 2017.06a
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    • pp.193-193
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    • 2017
  • The black heart in potato is a physiological disorder that occurs when potatoes suffer from breathing problems. When storing potatoes at a low temperature around $0^{\circ}C$, there is a high possibility that the respiration rate of potato will rise and black heart will occur. Also, respiration can occur easily and briefly in a state where high temperature and ventilation is insufficient. Recently, as black heart has been occurred continuously and severely in South Korea, here we tried to identify the causes of black heart in potato and to develop the control strategy of this disorder. Firstly, we analyzed the influence on the black heart on the basis of preservation containers (breathable plastic box, burlap bag, paper box, sealed plastic box). After harvesting the potato which is cv. Superior, it preserved for 6 months under conditions of temperature $3.5^{\circ}C{\pm}0.2$ and humidity 85%, after then we surveyed the incidence of emergence rate, rate of weight loss and occurrence rate of black heart. Secondly, in order to investigate the time point of black heart initiation under the oxygen concentration condition of 1% or less, The potatoes were used for this experiment stored for 6 months in a aerated plastic box under conditions of temperature $3.5^{\circ}C{\pm}0.2$ and humidity 85% under sufficient oxygen condition. After stored for 6 month, those were stored at $15^{\circ}C$ and below 1% of oxygen for 25 days, and then the incidence of black heart was surveyed. Thirdly, to investigate the effects of the number of days after harvest on the occurrence of black heart, it was examined the occurrence of black heart stored on 40 days and 100 days after harvesting under sealed condition and vacuum condition. The temperature condition of potato storage was stored was at $4^{\circ}C$ and $25^{\circ}C$ in humidity 85%. As a result of investigating the occurrence of black heart depending on the storage containers, all of the potatoes stored in the sealed plastic box had been occurred black heart. However, black heart of the potatoes in the other treatments did not. Potato preserved under the condition of below 1% of oxygen was found to occur 32% black heart after 25 days of storage. The potatoes corresponding to the required number of days after harvesting were stored for 31 days and the black heart was examined on the occurred. As a result, the potatoes which were 40 days after the harvest did not have black heart under sealed condition and vacuum condition. But potatoes harvested 100 days after harvesting had a black heart incidence of 95.7% under sealed condition at $4^{\circ}C$. The potato placed in the vacuum condition and a sealed state at $25^{\circ}C$ was transformed into anaerobic respiration, the inner tissue of tuber collapsed. Therefore, it is considered that black heart is caused by the breathing trouble in the central part when the oxygen is almost consumed after the aerobic respiration which gradually consumes the oxygen. We conclude that the black heart occurred in the central part where exchange of oxygen and carbon dioxide is the slowest is sensitive to respiration disorder. It is thought that research to investigate black heart generation time according to storage conditions and post-harvest state of potatoes is further necessary.

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Manufacturing Process Improvement of Electrode for PEMFC (공정 효율 향상을 위한 연료전지전극 개발)

  • PARK, SEOK JUNG;LEE, JAE SEUNG;LEE, KI SUB;ROH, BUM WOOK
    • Journal of Hydrogen and New Energy
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    • v.26 no.6
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    • pp.547-553
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    • 2015
  • For commercialization of fuel cell electric vehicles, one of the key objectives is to reduce cost of full stack assembly. Regarding Membrane Electrode Assembly, the major issue is to improve fuel cell activation process in the initial Hydrogen Oxidation Reaction and Oxygen Reduction Reaction. In this research, the VD (Vacuum Drying) process has been developed for improvement of activation process. The VD condition is developed by controlling the temperature and degree of vacuum to remove the remaining solvent of electrode. Consequently, the electrode applied to VD process showed the low characteristics such as 3.5% of remaining solvent content and the improved efficiency such as 15% of activation process speed.

Investigation of new in the Oil-Hydraulic Pump Consisting of Swing Twin-Cylinder (요동형 쌍원통 유압펌프내의 유동장 해석에 관한 연구)

  • Sim Woo Gun;Kim Gi Son
    • Journal of the Korean Vacuum Society
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    • v.14 no.1
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    • pp.7-16
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    • 2005
  • Oil-Hydraulic pump consisting of swing twin-cylinder becomes to be used as a next generation of low vacuum pump. However, there is no enough flow-analysis for design improvement. It is essential to develope a numerical method for flow-analysis before manufacturing, in economic sense. Using a commercial code (Fluent), developed for flow-analysis, useful informations for design of pump were provided. Two-dimensional analysis has been performed to investigate the flow parameters such as pressure and velocity distributions between the swing twin-cylinder and the fixed cylinder. This numerical method will be used to design a better performance of pump consisting of swing twin-cylinder.

Sound Absorption Property of Heat-Treated Wood at A Low Temperature and Vacuum Conditions

  • Byeon, Hee-Seop;Park, Jung-Hwan;Hwang, Kyo-Kil;Park, Han-Min;Park, Beyung-Soo;Chong, Song-Ho
    • Journal of the Korean Wood Science and Technology
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    • v.38 no.2
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    • pp.101-107
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    • 2010
  • Heat treatment was performed to improve sound absorption properties for four tree species; Tulip tree, Korean Paulownia, Red pine and Costata birch, at temperature of $175^{\circ}C$ and $200^{\circ}C$under vacuum condition. Sound absorption properties of two kinds of boards, which were in radial and tangential sections, were measured under a frequency range of 100 to 3200 Hz by the two microphone transfer function method. It was found that sound absorption properties were increased by heat treatment and the efficiency was higher at $200^{\circ}C$ than that at $175^{\circ}C$. Even Costata birch had a little effect on low temperature of $175^{\circ}C$, $200^{\circ}C$ heat treatment for sound absorption property, the efficiencies of sound absorption were 14, 19%, respectively. The efficiencies of sound absorption ranged 22 to 120% for heat-treated Tulip tree, Korean Paulownia.