• 제목/요약/키워드: Vacuum Sintering

검색결과 203건 처리시간 0.033초

농도기울기를 갖는 초경합금/철 혼합분말 성형체의 진공소결시의 미세조직 변화 (Microstructure Evolution in the Layered (WC-Co)/Fe Powder Compacts with a Composition Gradient during Vacuum Sintering)

  • 양성철
    • 한국분말재료학회지
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    • 제3권4호
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    • pp.266-270
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    • 1996
  • The microstructure evolution during sintering of a compact being composed of three layers of (WC-15%Co)/Fe powder mixture with different Fe contents has been observed. The Fe contents in the respective (WC-15%Co)/Fe layers were varied by 20%. 50%, and 90% in sequence by volume from a top layer to a bot- tom layer. The sintering temperatures and times were varied from 110$0^{\circ}C$ to 125$0^{\circ}C$ and from 1 h to 4 h, The compact layer was not densified below 120$0^{\circ}C$ in 4 h. Appropriate sintering temperature and time conditions for making a multi-layered hard metal compact were determined as 125$0^{\circ}C$ and 3 h, respectively.

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Cu25Cr 접점재료의 성형압력에 따른 소결 및 전기적 특성에 관한 연구 (A study on the effects of compacting pressure on the electrical & sintering characteristics of Cu25Cr contact material)

  • 연영명;박홍태;오일성;이경행
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2001년도 하계학술대회 논문집
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    • pp.1065-1068
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    • 2001
  • Effects of compacting pressure on the electrical and sintering characteristics of Cu25Cr contact material have been investigated. Cu25Cr contact materials were prepared by solid and liquid-phase sintering methods varying compacting pressure. Influence of compacting pressure on electrical characteristics were investigated in the cylindrical stainless-steel vessel using L-C resonant circuit. The physical and electrical properties of solid-phase sintered Cu25Cr material were found to be improved by increased compacting pressure. On the other hand, it was found that compacting pressure had little influence in case of liquid-phase sintered Cu25Cr material. After conditioning, contact resistance of Cu25Cr material was decreased regardless of compacting pressure. With increased compacting pressure, interrupting ability was shown to be increased.

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방전플라즈마소결법을 이용한 WC-3 wt%Co 소결체 제조 및 평가 (Fabrication and Evaluation of WC-3 wt%Co Compacts Fabricated by Spark Plasma Sintering)

  • 최정철;장세훈;차용훈;오익현
    • 한국재료학회지
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    • 제18권7호
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    • pp.357-361
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    • 2008
  • Microstructure and mechanical properties of WC-3 wt% Co cemented carbides, fabricated by a spark plasma sintering (SPS) process, were investigated in this study. The WC-3 wt%Co powders were sintered at $900{\sim}1100^{\circ}C$ for 5min under 40MPa in high vacuum. The density and hardness were increased as the sintering temperature increased. WC-3 wt%Co compacts with a relative density of 97.1% were successfully fabricated at $1100^{\circ}C$. The fracture toughness and hardness of a compact sintered at $1100^{\circ}C$ were $21.6 MPa{\cdot}m^{1/2}$ and 4279 Hv, respectively.

Graphite mould의 사용에 의한 2단소성법의 개선에 관한 연구(투명 PLZT를 제작함에 있어서) (Improvement of two stage sintering method by using graphite mould)

  • 박일규;이재열;백동수;이개명;박창엽
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1988년도 춘계학술대회 논문집
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    • pp.88-91
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    • 1988
  • In this paper, PLZT Ceramics were fabricated by two stage sintering method whose first stage vacuum hot pressing and second stage PbO atmosphere sintering. Using Graphite Mould instead of Alumina Mould in first stage prevented the adhision between PLZT substrate and the mould. The grain sizes of PLZT Ceramics were controlled by varying the hot pressing time and second sintering time.

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Effect of Residual Carbon on the Microstructure Evolution during the Sintering of M2 HSS Parts Shaping by Metal Injection Moulding Process

  • Herranz, G.;Levenfeld, B.;Varez, A.
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.225-226
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    • 2006
  • In this present investigation, Metal Injection Moulding (MIM) of M2 High Speed Steel (HSS) parts using a wax-High Density Polyethylene (HDPE) binder is shown. The elimination of organic binder was carried out by thermal debinding under inert atmosphere. In order to keep carbon in the sample that could improve the sintering process, incomplete debinding was performed between 450 and $600^{\circ}C$. The specimens were sintered at temperatures between 1210 and $1280^{\circ}C$ in high vacuum atmosphere, obtaining the 98% of the theoretical density. In the samples with higher residual carbon content, the sintering window was extended up to 20 degrees and the optimum temperature was lower.

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Thermoelectric Properties of N-type 90% $Bi_2Te_3+10%Bi_2Se_3$ Thermoelectric Materials Produced by Melt Spinning Method and Sintering

  • Kim, Taek-Soo;Chun, Byong-Sun
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.459-460
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    • 2006
  • N-type $Bi_2Te_3-Sb_2Te_3$ solid solutions doped with 1$CdCl_2$ was prepared by melt spinning, crushing and vacuum sintering processes. Microstructure, bending strength and thermoelectric property were investigated as a function of the doping quantity from 0.03wt.% to 0.10wt.% and sintering temperature from $400^{\circ}C$ to $500^{\circ}C$, and finally compared with those of conventionally fabricated alloys. The alloy showed a good structural homogeneity as well as bending strength of $3.88Kgf/mm^2$. The highest thermoelectric figure of merit was obtained by doping 0.03wt.% and sintering at $500^{\circ}C$.

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SPS에 의한 $SiC-ZrB_2$ 복합체의 특성에 미치는 분위기 영향

  • 김철호;신용덕;주진영;이정훈;박진형;조성만;김인용
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2009년도 추계학술대회 논문집
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    • pp.105-105
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    • 2009
  • The composites were fabricated by adding 30, 35, 40, 45[vol.%] Zirconium Diboride(hereafter, $ZrB_2$) powders as a second phase to Silicon Carbide(hereafter, SiC) matrix. $SiC-ZrB_2$ composites were sintered by Spark Plasma Sintering(hereafter, SPS) in vacuum or argon gas atmosphere. The relative density of SiC+40[vol.%]$ZrB_2$ composites reveal high 99.57[%] in argon gas atmosphere and pressure 50MPa.

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Novel Fabrication of Platinum Counter Electrode in Dye-sensitized Solar Cells Using Nano-second Pulsed Laser Sintering

  • Lee, Jin Ah;Yoo, Kicheon;Kim, Woong;Ko, Min Jae
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
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    • pp.234-234
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    • 2013
  • The counter electrodes in dye-sensitized solar cells (DSSCs) play roles in not only collecting electrons from external circuit but also reducing I3- to I- in electrolytes. Generally, conventional counter electrodes for DSSCs are prepared from the high temperature treatment of the H2PtCl6 precursor solution at $400^{\circ}C$ However, the more simplified fabrication process of counter electrodes is required for the commercialization of DSSCs. In this work, we developed novel fabrication process of counter electrodes using nano-second pulsed laser. DSSCs employing counter electrodes prepared by laser process showed conversion efficiency of 6.75% with short-circuit current of 12.73 mA/cm2, open-circuit voltage of 0.74 V and fill factor of 0.72. Closer investigating of photovoltaic properties will be reported.

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전기선폭발법으로 제조된 텅스텐 분말의 산소 조성이 방전플라즈마소결 거동에 미치는 영향 (Effect of Oxygen Content in the Tungsten Powder Fabricated by Electrical Explosion of Wire Method on the Behavior of Spark-Plasma Sintering)

  • 김철희;이성;김병기;김지순
    • 한국분말재료학회지
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    • 제21권6호
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    • pp.447-453
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    • 2014
  • Effect of oxygen content in the ultrafine tungsten powder fabricated by electrical explosion of wire method on the behvior of spark plasma sintering was investigated. The initial oxygen content of 6.5 wt% of as-fabricated tungsten powder was reduced to 2.3 and 0.7 wt% for the powders which were reduction-treated at $400^{\circ}C$ for 2 hour and at $500^{\circ}C$ for 1h in hydrogen atmosphere, respectively. The reduction-treated tungsten powders were spark-plasma sintered at $1200-1600^{\circ}C$ for 100-3600 sec. with applied pressure of 50 MPa under vacuum of 0.133 Pa. Maximun sindered density of 97% relative density was obtained under the condition of $1600^{\circ}C$ for 1h from the tungsten powder with 0.7 wt% oxygen. Sintering activation energy of $95.85kJ/mol^{-1}$ was obtained, which is remarkably smaller than the reported ones of $380{\sim}460kJ/mol^{-1}$ for pressureless sintering of micron-scale tungsten powders.