• Title/Summary/Keyword: Vacuum Evaporation

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An Experimental Study of Environmental Effects on the Rolling Resistance of Bearing Surfaces Coated by Soft Metallic Films (연금속 박막이 코팅된 베어링 표면의 구름 저항 거동에 미치는 분위기의 영향에 대한 실험적 고찰)

  • 양승호;공호성;윤의성;김대은
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 1998.04a
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    • pp.47-54
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    • 1998
  • An experimental study was performed to discover the effect of environmental conditions on the rolling resistance behavior of pure silver and lead coated 52100 bearing steel. Pure silver and lead coating were produced by a thermal evaporation coating method. Experiments using a thrust ball bearing-typed rolling test-rig were performed under vacuum, dry air and controlled humidity conditions. Results showed that agglomeration of particles were prevented in vacuum environment and as it showed low and stable rolling resistance by shakedown phenomena. Also, humidity relates closely to the agglomeration of particles and increased the rolling resistance after the failure of coated layer.

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A study on the structure and properties of Cr and Cr$_2$O$_3$ films deposited by the vacuum evaporation method (진공 증발법으로 증착한 Cr, Cr$_2$O$_3$ 박막의 조직 및 특성에 관한 연구)

  • 이종민;이정중
    • Journal of the Korean institute of surface engineering
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    • v.27 no.2
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    • pp.74-82
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    • 1994
  • The structure and properties such as adhesion and corrosion resistance of Cr and $Cr_2O_3$ films, deposited on steel plates by the vacuum evaporation method, were investigated. According to the ESCA and AES analy-sis, it could be concluded that chromium oxide with uniform composition could be formed on the steel sub-strate. The deposited Cr and $Cr_2O_3$ films had high adhesion strength, and they did not peeled off by the tape test. The adhesion property, however, was deteriorated as the film thciknes increased. After bending of the deposited specimen many cracks were observed by SEM, and they were assumed to have propagated along co-lumnar boundaries by the bending test. The corrosion resistance of the films was not generally good, which in-dicates that the films had a porous structure with a large number of defects such as pin holes and voids.

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Optical Reactivity Modification of Titanium Oxide coatings on Ceramic filters by Nitrogen ion Implantation

  • Kim, Hyeong-Jin;Park, Jae-Won
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.08a
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    • pp.90-90
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    • 2010
  • We investigated the modification of optical response properties of titanium dioxide (TiO2) coatings on the ceramic water-purification filters by using ultraviolet-visible absorption spectroscopy and X-ray diffraction. The TiO2 coatings were prepared on ceramic substrate by e-beam evaporation method. These amorphous TiO2 were turned into anatase phase by heat treatment at $700^{\circ}C$ for 2 hours. The doping of N atoms into the TiO2 coatings was done by using 70KeV of N+ ion implantation with the dose of $1.0{\times}1017$ ions/cm2, followed by post-irradiation heat treatment at $550^{\circ}C$ for 2 hours. Methylene blue test of TiO2 coatings to solar irradiation showed that the post-evaporation heated TiO2 was photocatalytic and N-doped TiO2 reacted to the visible part of solar irradiation.

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Co-evaporation법으로 성장시킨 CuInxGa1-$xSe_2$ 박막의 Photoreflectance 특성

  • Choe, Sang-Su;Kim, Jeong-Hwa;Jo, Hyeon-Jun;Kim, Dae-Hwan;Bae, In-Ho
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.08a
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    • pp.296-296
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    • 2011
  • 동시 증발법(co-evaporation)에 의해 성장된 $CuIn_xGa_{1-x}Se_2$ (CIGS) 박막의 광학적 특성을 photoreflectance (PR) 분광법으로 연구하였다. 조성비 x는 0~1까지 변화시켰다. 시료의 두께는 약 2.2 ${\mu}m$였다. PR 측정은 변조빔 세기, 변조빔 주파수 및 온도의 함수로 조사하였다. PR 스펙트럼으로부터 조성비 x가 증가함에따라 시료의 띠간격 에너지가 증가하는 것을 관측하였다. 상온 PR 스펙트럼으로부터 시료내에 형성된 내부 전기장을 구하였다. 그리고 변조빔 세기의 증가에 따른 PR 신호의 세기는 점차 증가하는 반면에, 변조 주파수를 증가시킴에 따라 신호의 세기가 점차 감소함을 보였다. PR 신호의 온도 의존성 실험으로부터 띠간격 에너지의 변화 및 Varshni 계수 등을 구하여 CIGS 시료의 특성을 조사하였다.

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Preparation and Reaction Studies of $Pt/Al_2O_3$ Model Catalysts

  • Kim, Chang-Min;Gabor A. Somorjai
    • Journal of the Korean Vacuum Society
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    • v.3 no.4
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    • pp.414-419
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    • 1994
  • Surface of Pt/$Al_2O_3$ model catalyst was produced on an aluminum foil with surface area of 1 $cm^2$ The aluminum surface was oxidized under $10 ^5Torr$Torr oxygen and platinum was deposited on top of the oxide layer using a plasma evaporation source. Conversion of I-butene was performed on the model catalyst surface. Isomerization was the major reaction in I-butene conversion on the aluminum oxide layer. Addition of Pt on the aluminum oxide layer induces hydrogenation of I-butene. Selectivity for the hydrogenation increases as the amount of Pt on alumina increases.

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A study on the optical characteristics of selenium thin film (Selenium박막의 광학적 특성연구)

  • 허창수;오영주
    • Electrical & Electronic Materials
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    • v.9 no.1
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    • pp.44-50
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    • 1996
  • In this study, Selenium device was fabricated by vacuum evaporation method with the substrate temperature at room temperature and its electrical and optical properties were investigated to be used in optical device. The film properties largely depended on the transmittance and annealing time, and improved with aging owing to stress release. We found that the photocurrent of the films increase linearly with light illumination. As a result, Selenium device made by this method yielded a short circuit current density of 10.5mA/$\textrm{cm}^2$, an open circuit voltage of 39OmV.

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Optical properties of the polycrystalline CdSe thin films grown by the electron-beam evaporation technique (전자선 증착기술에 의해 성장된 다결정 CdSe 박막의 광학적 특성)

  • 김화민
    • Journal of the Korean Vacuum Society
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    • v.9 no.1
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    • pp.60-68
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    • 2000
  • The optical constants ($E_g^d$, n, K) of the polycrystalline CdSe thin films deposited on the glass substrate by the electron-beam evaporation technique are determined over 400~2,500 nm photon wavelengths. In order to explain the variation of the optical contents with film thickness and substrate temperatures, the surface microstructural parameter are investigated by AFM (atomic forced microscope( images for the films deposited by different growth conditions. It is shown that the variations of optical constants are close related to changes of the surface morphology of the CdSe thin films. The decrease in the band gap with film thickness is connected with quantum size effects due to increase of the grain size. The refractive index of CdSe films decrease with increasing the grain size of the films, and the dispersion of the refractive index followed a single oscillator model according to the Sellmeier formulation.

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Defect Formation in Epitaxially Grown Silver Films (배향 성장시킨 은박막중의 결함생성)

  • Lee Ki-Seon;Kim Key-Soo
    • Applied Microscopy
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    • v.6 no.1
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    • pp.33-38
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    • 1976
  • Formation of crystal defects which may occur during and after the vacuum deposition of silver films on rocksalt substrates were studied by electron microscopy. To obtain defect free films, various evaporation conditions, such as evaporation rate, substrate temperature, substrate treatments and annealing of films were examined. Stacking faults and micro-twins are dominant defects in silver films.

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A Study on the Precool Characteristics of Agricultural Products Using the Water-driven Ejector (수구동 액체이젝터를 이용한 농산물의 예냉특성에 관한 연구)

  • 박영승;이정혜;김호영;김경근
    • Proceedings of the Korean Society of Marine Engineers Conference
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    • 2001.11a
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    • pp.45-49
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    • 2001
  • To maintain the freshness of produce, because of stand away between produced and consumer, we need refrigeration system that can supply to consumer at cold chain as soon as gathering. General refrigeration system consist of refrigeration chamber or low temperature store. But the vacuum technology can rapidly refrigeration without refrigerator. This precool system possible to get low precooled temperature, suitable for the fishes, the meat, the vegetables, the fruit etc. Especially get advantage that quality maintain through rapid refrigeration of ferment directly generate heat. Vacuum precool system's principle is that water saturated temperature reduce according to pressure is get to vacuum area, so product temperature reduce as water evaporation at product. In vacuum suction, unit, on early experiment period run the rotary type vacuum pump at purpose pressure, then maintain pressure by water-diven ejector. As the results, cabbage took about 60 minutes to reach from $23.2^{\circ}C$ to $4.5^{\circ}C$at 5mgHg abs.

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Combustion Synthesis of $LiMn_2$$O_4$with Citric Acid and the Effect of Post-heat Treatment

  • Han, Yi-Sup;Son, Jong-Tea;Kim, Ho-Gi;Jung, Hun-Teak
    • Journal of the Korean Ceramic Society
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    • v.38 no.4
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    • pp.307-307
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    • 2001
  • Combustion process with citrate was used to produce the LiMn$_2$O$_4$powder. Precursors are pre-ignited in open air followed by post-heating in the range from $600^{\circ}C$ to 80$0^{\circ}C$ for 4h. With varying the molar ratio (R) of ethylene glycol (EG) to citric acid (CA) from 0 to 4, the effect of EG content on powder characteristics is evaluated. Vacuum drying promote the auto-ignition at room temperature. With small addition of EG metal ion was selectively segregated with organic substances and undesired lithium evaporation occurred during post-heating. LiMn$_2$O$_4$phase which is produced by combustion reaction was decomposed back to Mn$_3$O$_4$because the reaction temperature was higher than 95$0^{\circ}C$. With increasing EG content, the homogeneity of LiMn$_2$O$_4$powder increased and specific surface area increased. And lithium evaporation during vacuum drying and/or ignition also increased.

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