• Korean Journal of Materials Research
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• v.4 no.8
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• pp.861-869
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• 1994

Chemical vapor deposition using titanium tetra isopropoxide(TTIP) was employed to investigate effects of process parameters on the uniformity of $TiO_{2}$this films deposited on Indium Tin Oxide (ITO)coated glass. Deposition experiments were carried out at temperatures ranging from $300^{\circ}C$ to $400^{\circ}C$ under the pressure of 0.5~2 torrin a cold wall reactor which can handle 200mm substrate. It was found that the growth rate of $TiO_{2}$was closely related to the reaction temperature and the ractant gas compositions. Apparent activation energy for the deposition rate was 62.7lkJ/mol in the absence of $O_{2}$ and 100.4kj/mol in the presence of $O_{2}$, respectively. Homogeneous reactions in the gas phase were promoted when the total pressure of the reactor was increased. Variance in the film thickness was less than a few percent, but at high deposition rates film thickness was less uniform. Effects of reaction temperature on $TiO_{2}$ thin film characteristic was investigated with SEM, XRD and AES.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.7 no.6
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• pp.1040-1046
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• 2006

This paper is aimed to investigate the deformation caused by ununiform contraction of injection molding with highly big differences of thickness by the continuity of various curvature radius. By CAE analysis, the uniform cooling structure and optimum molding conditions are found for Jars made of SAN and PMMA materials and applied to the design of chill. In order toevaluate the molding pressure, resin temperature, molding temperature, cooling conditions, Moldflow program is applied. As results of experiments, the deformation and inferiority phenomena in Jars are analyzed for each factor and proposed the injection molding conditions to minimize the cooling structure and reduce the cycle time.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.05a
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• pp.357-360
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• 2007

The profile ring rolling process of Ti-6Al-4V alloy was designed by finite element(FE) simulation and experimental analysis. The design includes geometry design and optimization of process variables. The geometry design such as initial billet and blank sizes, and final rolled ring shape was carried out with the calculation method based on the uniform deformation concept between the wall thickness and ring height. FEM simulation was used to calculate the state variables such as strain, strain rate and temperature and to predict the formation of forming defects during ring rolling process. Finally, the mechanical properties of profiled Ti-6Al-4V alloy ring product were analyzed with the evolution of microstructures during the ring rolling process.

• Advances in aircraft and spacecraft science
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• v.5 no.1
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• pp.21-49
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• 2018

In this paper, geometric nonlinear bending characteristics of single wall carbon nanotube reinforced composite (SWCNTRC) doubly curved shell panels subjected to uniform transversely loadings are investigated. The nonlinear mathematical model is developed for doubly curved SWCNTRC shell panel on the basis of higher-order shear deformation theory and Green- Lagrange nonlinearity. All nonlinear higher order terms are included in the mathematical model. The effective material properties of SWCNTRC are estimated by using Eshelby-Mori-Tanaka micromechanical approach. The governing equation of the shell panel is obtained using the total potential energy principle and a Newton-Raphson iterative method is employed to compute the nonlinear displacement and stresses. The present results are compared with published literature. The effect of SWCNT volume fraction, width-to-thickness ratio, radius-to-width ratio (R/a), boundary condition, linear and nonlinear deflection, stresses and different types of shell geometry on nonlinear bending response is investigated.

• Proceedings of the SAREK Conference
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• 2009.06a
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• pp.1326-1331
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• 2009

Drying process in the cylindrical thin film layer of sludge with the thickness less than a few millimeters has been investigated. Thin film drying is specially designed and used to dry the viscous materials like sewage sludge. The thin film layer of sludge is dried on the metallic cylindrical surface through which thermal energy is supplied to the layer during drying. The wall temperature is assumed to be constant during drying in the present study for the simplification. In order to solve the equations, the mass transfer rate on the drying surface should be determined. The mass flux of evaporated water vapor on the surface is estimated with the formulation given in the literature. The effect of some physical parameters on drying has been examined to figure out the drying characteristics of the sludge layer.

• Journal of Sensor Science and Technology
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• v.27 no.4
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• pp.264-268
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• 2018

Vertically-aligned $TiO_2$ nanotube electrodes have attracted considerable attention for applications in solar cells, catalysts, and sensors, because of their ideal structure for electron transport and electrolyte diffusion. Here, we prepare vertically-aligned $TiO_2$ nanotube electrodes using a two-step anodization process. The prepared $TiO_2$ nanotube electrodes exhibit uniform pore structures with an inner diameter of ~80-90 nm and wall thickness of ~20-25 nm. In addition, they exhibit an anatase crystal phase after a high-temperature annealing. The annealed $TiO_2$ nanotube electrodes are applied in dye-sensitized solar cells (DSSCs) as photoanodes. The fabricated DSSC exhibits conversion efficiencies of 3.46 and 2.15% with liquid- and gel-type electrolytes, respectively.

• Steel and Composite Structures
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• v.26 no.1
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• pp.1-15
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• 2018

This study reported, the effect of random variation in system properties on bending response of single wall carbon nanotube reinforced composite (SWCNTRC) plates subjected to transverse uniform loading is examined. System parameters such as the SWCNT armchair, material properties, plate thickness and volume fraction of SWCNT are modelled as basic random variables. The basic formulation is based on higher order shear deformation theory to model the system behaviour of the SWCNTRC composite plate. A C0 finite element method in conjunction with the first order perturbation technique procedure developed earlier by the authors for the plate subjected to lateral loading is employed to obtain the mean and variance of the transverse deflection of the plate. The performance of the stochastic SWCNTRC composite model is demonstrated through a comparison of mean transverse central deflection with those results available in the literature and standard deviation of the deflection with an independent First Order perturbation Technique (FOPT), Second Order perturbation Technique (SOPT) and Monte Carlo simulation.

• Transactions of Materials Processing
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• v.16 no.4 s.94
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• pp.223-228
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• 2007

The profile ring rolling process of Ti-6Al-4V alloy was investigated by finite element(FE) simulation and experimental analysis. The process design of the profile ring rolling includes geometry design and optimization of process variables. The geometry design such as initial billet and blank sizes, and final rolled ring shape was carried out with the calculation method based on the uniform deformation concept between the wall thickness and ring height. FEM simulation was used to calculate the state variables such as strain, strain rate and temperature and to predict the formation of forming defects during ring rolling process. Finally, the mechanical properties of profiled Ti-6Al-4V alloy ring product were analyzed with the evolution of microstructures during the ring rolling process.

• Bulletin of the Korean Chemical Society
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• v.35 no.1
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• pp.173-176
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• 2014

The hollow $SiO_2$ spheres with uniform size were synthesized by a modified Stober method under the control of polyelectrolytes (PSS and PAA) as templates. This synthetic route includes the formation of spherical colloid micelle in ethanol solution, hydrolysis of TEOS under control of ammonia, and the removal of polyelectrolyte by washing or calcination. Hollow silica spheres with controllable core diameters between 100 and 270 nm and wall thickness between 15 and 50 nm have been synthesized. The influence of template solution concentration and solvent and dispersant on the formation of silica hollow spheres is studied and reported in detail.

• Journal of Energy Engineering
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• v.28 no.3
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• pp.1-9
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• 2019

A major stress determining the remaining life of the tube in feedwater heater of fossil fuel power plant is hoop stress by the internal pressure. However, thermal stress due to temperature difference across the wall thickness also contributed to reduce the remaining life of the tube. Therefore, thermal loading must be considered even though the contribution of internal pressure loading to the stresses of the tube was known to be much higher than that of the thermal loading. In this study, thermal stress of the tubes in the de-superheating zone was estimated, which was generated due to the temperature difference across the tube thickness. Analytic equations were shown for determining the hoop stress and the radial stress of the tube with uniform thinning and for the temperature across the tube thickness. Accuracy and effectiveness of the analytic equations for the stresses were verified by comparing the results obtained by the analytic equations with those obtained from finite element analysis. Using finite element analysis, the stresses for eccentric thinning were also determined. The effect of heat transfer coefficient on thermal stress was investigated using series of finite element analyses with various values of heat transfer coefficient for both inner and outer surface of the tube. It was shown that the effect of heat transfer coefficient at outer surface was larger than that of heat transfer coefficient at inner surface on the thermal stress of the tube. Also, the hoop stress was larger than the radial stress for both cases of uniformly and eccentrically thinned tubes when the thermal loading was only considered without internal pressure loading.