• Title/Summary/Keyword: Under the microscope

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Microstructure of Precipitation Strengthened Ll2-type Co3Ti Intermetallic Compound

  • Han, Chang-Suk;Chun, Chang-Hwan;Han, Seung-Oh
    • Korean Journal of Metals and Materials
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    • v.47 no.11
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    • pp.694-698
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    • 2009
  • The $Co_{3}Ti$ phase hardens appreciably by the fine precipitation of disordered fcc Co-rich phase upon aging after quenching from solution annealing temperature. Transmission electron microscope (TEM) observations revealed that the precipitates are platelet in shape, lying nearly parallel to the {100} planes of the $Ll_{2}$-ordered matrix, and perfectly coherent with the matrix lattice at the beginning of aging. The high temperature strength increases appreciably with the fine precipitation of disordered Co-rich phase over the whole temperature range investigated. TEM observations of the under-aged and deformed alloys revealed that superdislocations are pinned by precipitates indicating an attractive interaction between dislocations and precipitates. In the over-aged state, thin twins are introduced in the fcc Co-rich precipitates during deformation.

Fabrication and Linear & Nonlinear Optical Characterization of Photonic Crystals (포토닉 밴드갭 광결정의 제작과 선형 및 비선형 광학 특성 연구)

  • Ha Na Yeong;U Yeon Gyeong;Hwang Ji-Su;Jang Hye-Jeong;Park Byeong-Ju;U Jeong-Won
    • Proceedings of the Optical Society of Korea Conference
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    • 2002.07a
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    • pp.162-163
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    • 2002
  • 1-D photonic band-gap structure is identified in a cholesteric liquid crystal system. The optical transmission spectrum is measured and compared with the theoretical analysis. Nonlinear transmission is measured near the band edge. Also 3-D photonic band-gap structures are fabricated from dielectric colloidal polystyrene beads through a centrifuge method. The fabricated photonic crystals exhibit opalescent colors under white light and show a clear diffraction peak dependent on the incident angle of the light beam. Also the scanning electron microscope image was taken to verify the face-centered cubic crystal structure. Bragg's law and Snell's law are employed to describe the position of angle resolved diffraction peaks. It was shown that the optically deduced effective refractive index and lattice constants were in good agreement with the crystal structure identified by scanning electron microscope.

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Management of a permanent maxillary first molar with unusual crown and root anatomy: a case report

  • Chowdhry, Prateeksha;Reddy, Pallavi;Kaushik, Mamta
    • Restorative Dentistry and Endodontics
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    • v.43 no.3
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    • pp.35.1-35.7
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    • 2018
  • The aim of this article was to showcase the endodontic management of a maxillary first molar with an unusual crown and root anatomy. Clinical diagnosis of the roots and root canal configuration was confirmed by a cone-beam computed tomography (CBCT) and the detection of the canals was made using a dental operating microscope. CBCT images revealed the presence of 5 roots with Vertucci type I canal configuration in all, except, in the middle root which had 2 canals with type IV configuration. The 6 canal orifices were clinically visualized under the dental operating microscope. Clinicians should familiarize themselves with the latest technologies to get additional information in endodontic practice in order to enhance the outcomes of endodontic therapy.

Friction and Wear of Nano-Sized Silica Filled Epoxy Composites

  • Kim, Jae-Dong;Kim, Yeong-Sik;Kim, Hyung-Jin
    • Journal of Power System Engineering
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    • v.18 no.6
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    • pp.174-179
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    • 2014
  • The wear behavior of epoxy matrix composites filled with nano sized silica particles is discussed in this paper. Especially, the variation of the coefficient of friction and the specific wear rate under the various applied load and sliding velocity were investigated for these materials. Wear tests of pin-on-disc mode were carried out and followed by scanning electron microscope observations. The presence of silica filler in epoxy composites was demonstrated significant influence on the friction and wear behavior of epoxy nanocomposites. With the incorporation of silica filler into the epoxy matrix, reduction of the coefficient of friction and specific wear rate were identified. Wear mechanism was discussed by analyzing the worn surface by scanning electron microscope as well.

Evaluation of Microstructure and Mechanical Property of Inconel 600 Degraded under High Temperature (고온 열화된 Inconel 600강의 미세조직 및 기계적 특성 평가)

  • Jung, Kwang-Hu;Kim, Seong-Jong
    • Journal of the Korean institute of surface engineering
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    • v.50 no.6
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    • pp.492-497
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    • 2017
  • In this study, we investigated the effect of thermal aging on mechanical characteristics of Inconel 600 nickel-based alloy. The thermal aging was conducted up to 1000 hours at an atmosphere of $650^{\circ}C$. The microstructure of thermally aged specimens was investigated by an optical microscope (OM), scanning electron microscope (SEM) and energy dispersive spectrometer (EDS). In addition, tensile test (strain rate: 2 mm/min) and micro Vickers hardness test were conducted to evaluate mechanical properties with time. As a result of the experiment, Cr-rich carbide continuously precipitated during thermal aging, leading to the change of the mechanical characteristics and fracture mode. With the increase of aging time, tensile strength, yield strength, and hardness gradually decreased. The fracture mode changed from ductile to brittle with the increase of grain boundary carbide.

Fabrication and Optical Characterization of Colloidal 3-D Photonic Crystals

  • N. Y. Ha;Y. Woo;Park, Byungchoo;J. W. Wu
    • Journal of the Korean Vacuum Society
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    • v.12 no.S1
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    • pp.15-16
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    • 2003
  • 3-D photonic band-gap structures are fabricated from dielectric colloidal polystyrene beads through a centrifuge method. The fabricated photonic crystals exhibit opalescent colors under white light and show a clear diffraction peak dependent on the incident angle of the light beam. Also the scanning electron microscope image was taken to verify the face-centered cubic crystal structure. Bragg's law and Snell's law are employed to describe the position of angle resolved diffraction peaks. It was shown that the optically deduced effective refractive index and lattice constants were in good agreement with the crystal structure identified by scanning electron microscope.

Fabrication of PDMS Mold by AFM Based Mechanical TNL Patterning (AFM기반 기계적 TNL 패터닝을 통한 PDMS 몰드제작)

  • Jung, Y.J.;Park, J.W.
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.22 no.5
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    • pp.831-836
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    • 2013
  • This study demonstrates the process of fabricating patterns using tribonanolithography (TNL),with laboratory-made micro polycrystalline diamond (PCD) tools that are attached to an atomic force microscope (AFM). The various patterns are easily fabricated using mechanical scratching, under various normal loads, using the PCD tool on single crystal silicon, which is the master mold for replication in this study. Then, polydimethylsiloxane (PDMS) replica molds are fabricated using precise pattern transfer processes. The transferred patterns show high dimensional accuracy as compared with those of TNL-processed silicon micro molds. TNL can reduce the need for high cost and complicated apparatuses required for conventional lithography methods. TNL shows great potential in that it allows for the rapid fabrication of duplicated patterns through simple mechanical micromachining on brittle sample surfaces.

Characterization of nano-fiber web structures using a morphological image processing

  • Kim, Jooyong;Lee, Jung-Hae
    • Proceedings of the Korean Fiber Society Conference
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    • 2003.10a
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    • pp.100-100
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    • 2003
  • An image processing algorithm has been developed in order to analyze the nanofiber web images obtained from a high magnification microscope. It has been known that precise pore detection on thick webs is extremely difficult mainly due to lack of light uniformity, difficulty of fine focusing and translucency of nanofiber web. The pore detection algorithm developed has been found to show excellent performance in characterizing the porous structure, thus being a promising tool for on-line quality control system under mass production. Since the images obtained from an optical microscope represent only web surface, a scale factor has been introduced to estimate the web structure as a whole. Resulting web structures have been compared to those by mercury porosimetry, especially in pore size distribution. It has been shown that those two structures have a strong correlation, indicating that scaling of a single layer web structure can be an effective way of estimating the structure of thick fiber webs.

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Mass production of carbon nanotubes using Vapor Phase Growth (기상합성법을 이용한 탄소나노튜브의 대량합성)

  • 류승철;이태재;이철진
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.07a
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    • pp.123-126
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    • 2001
  • Multiwalled carbon nanotubes were massively produced by the catalytic reaction of C$_2$H$_2$ - Fe(CO)$\sub$5/ mixture at 750 - 950$^{\circ}C$ in a quartz tube reactor and over quartz substrates. Well-aligned MWNT array grows perpendicular to the quartz tube reactor and the quartz substrates at an average of 60 nm in diameter and up to several thousands of micrometers in length. This method does not require any pretreatment of substrates and CNTs are grown at atmospheric pressure. It could be suitable for mass production of multiwalled nanotubes. Scanning electron microscope and transmission electron microscope images of the nanotubes deposited on the substrates allowed us to monitor the quality of MWNTs grown under different operating conditions.

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Surface Damage Characteristics of Self-Assembled Monolayer and Its Application in Metal Nano-Structure Fabrication (자기 조립 분자막의 표면파손특성 및 미세 금속 구조물 제작에의 응용)

  • Sung, In-Ha;Kim, Dae-Eun
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2002.05a
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    • pp.40-44
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    • 2002
  • The motivation of this work is to use SAM(Self-Assembled Monolayer) for developing a rapid and flexible non-photolithographic nano-structure fabrication technique which can be utilized in micro-machining of metals as well as silicon-based materials. The fabrication technique implemented in this work consists of a two-step process, namely, mechanical scribing followed by chemical etching. From the experimental results, it was found that thiol on copper surface could be removed even under a few nN normal load. The nano-tribological characteristics of thiol-SAM on various metals were largely dependent on the native oxide layer of metals. Based on these findings, nano-patterns with sub-micrometer width and depth on metal surfaces such as Cu, Au and Ag could be obtained using a diamond-coated tip.

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