• Title/Summary/Keyword: Ultrasonic Cavitation

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A Study on the Alkali Hydrolysis of PET fabrics with Ultrasonic Application(II)- Surface Porosity and Oligomer Analysis - (초음파를 적용한 PET 직물의 알칼리 가수분해에 관한 연구(II) - 기공특성과 올리고머 분석 -)

  • 김삼수;서말용;박성우;윤태희;이승구;허만우
    • Textile Coloration and Finishing
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    • v.14 no.6
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    • pp.305-312
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    • 2002
  • In order to give a silk-like touch to PET fabrics, the PET fabrics were treated with NaOH alkaline solution in various conditions. In alkaline treatment, the liquor flow type pilot weight reduction apparatus with magnetostrictive ultrasonic transducer was used for the study. The effects of ultrasonic application, treatment time and temperature at NaOH 4% and 6"A solution on the decomposition rate of PET fabrics. From the results of the decomposition rate of PET fabrics, the qualitative and quantitative analysis of oligomer after decomposition of PET fabrics carried out by the HPLC. On the other hand, the surface pore characteristics of decomposition PET fabrics measured by porosimetery. The pore characteristics on the surface of treated PET fiber depended on the decomposition rate and did not depend on the ultrasonic cavitation. The pore diameter of alkaline untreated PET fiber were 15A and those of treated PET fibers were 5~6$\AA$ at the maximum pore volume. The average pore sizes of fiber before and after treatment were 141 h and 160h, respectively. Total amount of oligomer of the untreated PET fibers were 1.70wt% and 67.7% of total oligomer occupied with PET cyclic trimer and PET cyclic tetramer. Total amount of oligomer of fiber with 26.9% and 48.0% of weight loss without ultrasonic application were 1.78wt% and 1.79wt%, respectively. Also total amount oligomer of fibers which were reduced 27.7% and 48.2% of weight loss with ultrasonic application were 1.74wt%. This result showed that the removal rate of oligomer in the process of alkaline hydrolysis with ultrasonic higher than that of without ultrasonic application.tion.

Atomization Characteristics Experiment of Pintle Type Nozzle by the PDPA (PDPA에 의한 Pintle형 노즐의 미립화 특성실험 -식물유를 중심으로-)

  • 나우정;유병구;정진도
    • Journal of Energy Engineering
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    • v.7 no.1
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    • pp.17-23
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    • 1998
  • A simplified experiment was performed to figure out the atomization characteristics of highly viscous liquid of rice-bran oil by applying ultrasonic energy to improve the atomization of spray droplets. A spray system, an ultrasonic system, and three kinds of pintle-type nozzles(pin-edge angle: 5 , 10 , 15 ) were manufactured. To investigate the effects of ultrasonic energy on the atomization of a highly viscous liquid, a phase doppler particle analyzer was used for the measurement and calculation of spray droplets data. Nozzle opening pressures were chosen of 3 levels, i.e, 10, 13, 16 MPa. As a result, it could be concluded that the ultrasonic energy was effective to improve the spray atomization when applied to the fuel by means of 3 different nozzles because of the effects of the liquid fuel cavitation and relaxation between molecules caused by ultrasonic energy. The improvement rate of the spray atomization by the ultrasonic spray atomization by the ultrasonic spray compared with the conventional spray was about 10% increase in the case of pintle type nozzles. With the increase of pin-edge angles the distribution lines by nozzle opening pressures are declined for both conventional and ultrasonic sprays. This means that the increase of the pin-edge angle improves the atomization of sprays.

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Evaluation of Durability for Al Alloy with Anodizing Condition (알루미늄 합금의 양극산화 조건에 따른 내구성 평가)

  • Lee, Seung-Jun;Han, Min-Su;Kim, Seong-Jong
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2016.11a
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    • pp.152-152
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    • 2016
  • Anodizing is a technology to generate thicker and high-quality films than natural oxide films by treating metals via electrochemical methods. It is a technique to develop metals for various uses, and extensive research on the commercial use has been performed for a long time. Aluminum anodic oxide (AAO) is generate oxide films, whose sizes and characteristics depending on the types of electrolytes, voltages, temperatures and time. Electrochemical manufacturing method of nano structure is an efficient technology in terms of cost reduction, high productivity and complicated shapes, which receives the spotlight in diverse areas. The sulfuric acid was used as an anodizing electrolyte, controlling its temperature to $10^{\circ}C$. The anode was 5083 Al alloy with dimension of $5(t){\times}20{\times}20mm$ while the cathode was the platinum. The distance between the anode and the cathode was maintained at 3 cm. Agitation was introduced by magnetic stirrer at 300 rpm to prevent localized temperature rise that hinders stable growth of oxide layer. In order to observe surface characteristics with applied current density, the electrolyte temperature, concentration was maintained at constant condition for $10^{\circ}C$, 10 vol.%, respectively. To prevent hindrance of stable growth of oxide layer due to local temperature increase during the experiment, stirring was maintained at constant rate. In addition, using galvanostatic method, it was maintained at current density of $10{\sim}30mA/cm^2$ for 40 minutes. The cavitation experiment was carried out with an ultrasonic vibratory apparatus using piezo-electric effect with modified ASTM-G32. The peak-to-peak amplitude was $30{\mu}m$ and the distance between the horn tip and specimen was 1 mm. The specimen after the experiment was cleaned in an ultrasonic, dried in a vacuum oven for more than 24 hours, and weighed with an electric balance. The surface damage morphology was observed with 3D analysis microscope. As a result of the investigation, differences were observed surface hardness and anti-cavitation characteristics depending on the development of oxide film with applied current density.

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Image enhancement in ultrasound passive cavitation imaging using centroid and flatness of received channel data (수신 채널 신호의 무게중심과 평탄도를 이용한 초음파 수동 공동 영상의 화질 개선)

  • Jeong, Mok Kun;Kwon, Sung Jae;Choi, Min Joo
    • The Journal of the Acoustical Society of Korea
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    • v.38 no.4
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    • pp.450-458
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    • 2019
  • Passive cavitation imaging method is used to observe the ultrasonic waves generated when a group of bubbles collapses. A problem with passive cavitation imaging is a low resolution and large side lobe levels. Since ultrasound signals generated by passive cavitation take the form of a pulse, the amplitude distribution of signals received across the receive channels varies depending on the direction of incidence. Both the centroid and flatness were calculated to determine weights at imaging points in order to discriminate between the main and side lobe signals from the signal amplitude distribution of the received channel data and to reduce the side lobe levels. The centroid quantifies how the channel data are distributed across the receive channel, and the flatness measures the variance of the channel data. We applied the centroid weight and the flatness to the passive cavitation image constructed using the delay-and-sum focusing and minimum variance beamforming methods to improve the image quality. Using computer simulation and experiment, we show that the application of weighting in delay-and-sum and minimum variance beamforming reduces side lobe levels.

Evaluation of Creep-Fatigue Damage in 304 Stainless Steel using Ultrasonic Non-Destructive Test (초음파 비파괴 검사를 이용한 AISI 304 스테인리스강의 크리프-피로 손상의 평가)

  • Lee, Sung Sik;Oh, Yong Jun;Nam, Soo Woo
    • Korean Journal of Metals and Materials
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    • v.49 no.12
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    • pp.924-929
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    • 2011
  • It is well known that grain boundary cavitation is the main failure mechanism in austenitic stainless steel under tensile hold creep-fatigue interaction conditions. The cavities are nucleated at the grain boundary during cyclic loading and grow to become grain boundary cracks. The attenuation of ultrasound depends on scattering and absorption in polycrystalline materials. Scattering occurs when a propagation wave encounters microstructural discontinuities, such as internal voids or cavities. Since the density of the creep-fatigue cavities increases with the fatigue cycles, the attenuation of ultrasound will also be increased with the fatigue cycles and this attenuation can be detected nondestructively. In this study, it is found that individual grain boundary cavities are formed and grow up to about 100 cycles and then, these cavities coalesce to become cracks. The measured ultrasonic attenuation increased with the cycles up to cycle 100, where it reached a maximum value and then decreased with further cycles. These experimental measurements strongly indicate that the open pores of cavities contribute to the attenuation of ultrasonic waves. However, when the cavities develop, at the grain boundary cracks whose crack surfaces are in contact with each other, there is no longer any open space and the ultrasonic wave may propagate across the cracks. Therefore, the attenuation of ultrasonic waves will be decreased. This phenomenon of maximum attenuation is very important to judge the stage of grain boundary crack development, which is the indication of the dangerous stage of the structures.

Acoustically-enhanced particle dispersion in polystyrene/alumina nanocomposites

  • Philip, Mercy A.;Natarajan, Upendra;Nagarajan, Ramamurthy
    • Advances in nano research
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    • v.2 no.2
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    • pp.121-133
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    • 2014
  • Polymer nanocomposites are advanced nanomaterials which exhibit dramatic improvements in various mechanical, thermal and barrier properties as compared with the neat polymer. Polystyrene/ alumina nanocomposites were prepared by an ultrasound-assisted solution casting method at filler loadings ranging from 0.2 to 2% and also at different ultrasonic frequencies, viz. 58 kHz, 192/58 kHz, 430 kHz, 470 kHz and 1 MHz. The composites were subjected to mechanical property tests (tensile and impact tests) and cavitation erosion tests to study the enhancement in functional properties. Filler dispersion in the polymer matrix was observed by SEM analysis. The effect of frequency on filler dispersion in the matrix was studied by SEM analysis and functional property enhancement of the composite material. The composites prepared at dual (high/ low) frequency (192/58 kHz) were found to show better property enhancement at low filler loadings as compared with neat polymer and also with composites prepared without ultrasound, thus reinforcing the finding that ultrasound-assisted synthesis is a promising method for the synthesis of nanocomposites.

A Study on the Cleaning Efficiency using the d-Limonene Oil Extracted in Wasted Mandarin Peels (폐감률피에서 추출한 limonene 오일의 세정성에 관한 연구)

  • Song, Min-Kyung;Oh, Eun-Ha;Im, Ho-Sub;Kim, Yoon-Shin
    • Journal of the Korean Applied Science and Technology
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    • v.27 no.2
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    • pp.107-113
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    • 2010
  • The object of this research is to conform of practicable possibility and recycling of producing junk after citrus fruits is processed. With extracting d-limonene oil that have 70~90% a component of oil out of junk citrus peel, making certain the about 12000ppm concentration of it. Limonene derived from citrus in jeju using conventional synthetic detergents can be replaced with the development of environmentally friendly natural detergent investigated the possibility. Mostly due to ocean dumping, disposal and cause environmental problems by recycling natural citrus cleaner alternative to the research conducted on the possibility. Cleaning efficiency with temperature did not affect the largest concentrations were able to identify the difference between cleaning efficiency. At least 10% of the d-limonene oil could be from the cleaning performance, increasing the concentration of the cleaning efficiency was increased in size. Ultrasonic is very high removal efficiency under the conditions shown in the cause of pure self-generated ultrasonic cleaning power as co-effects of d-limonene oil appears to chemical cleaning effect of ultrasonic cavitation occurs in the physical cleaning effect due to a combination of synergistic stability is maximized by low concentrations of d-limonene oil in a short time showed an excellent cleaning ability. Having the ability of cleaning at the same time, considering the side recycling in the junk citrus peels reflects possibility of basic materials utility eco-friendly in the skin soap, bath soap, cosmetics etc, through ability of exclusion a contaminant in based cleaning effect(EC) it can prospect substitution effect environmentally in the pre existence synthetic detergents.

A Non-Invasive Ultrasonic Urinary Bladder Internal Pressure Monitoring Technique: Its Theoretical Foundation and Feasibility Test (비침습적 초음파 방광 내압 측정 기술: 이론적 기초 및 실현 가능성 평가)

  • Choi, Min Joo;Kang, Gwan Suk;Lee, Kang Il
    • Journal of the Korean Society for Nondestructive Testing
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    • v.32 no.5
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    • pp.526-539
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    • 2012
  • A new approach was proposed in this article, named, a non-invasive ultrasonic method to monitor the urinary bladder internal pressure which can resolve the shortcomings of the existing methods. The proposed method makes use of acoustic cavitation. It is based on a physical phenomenon that an extracorporeal high intensity focused ultrasonic pulse generates bubbles inside the urinary bladder and the dynamic properties of the bubbles are related to the urinary bladder internal pressure. The article presents the theoretical foundation for the proposed technique and verifies its feasibility with preliminary experimental data. The suggested ultrasonic urinary bladder internal pressure monitoring method is non-invasive and can be used any time regardless of sex and age, so that it will be of a great benefit to the diagnosis and therapy of urination related diseases.

Development of Inspection Methodology for a Nuclear Piping Wall Thinning Caused by Erosion Using Ultrasonic B-Scan Measurement Device (B-Scan 초음파 측정장비를 이용한 원전 배관 침식손상 검사법 개발)

  • Lee, Dae Young;Suh, Heok Ki;Hwang, Kyeong Mo
    • Corrosion Science and Technology
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    • v.11 no.3
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    • pp.89-95
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    • 2012
  • U.S. Electric Power Research Institute (EPRI) has developed CHECWORKS program and applied it to power plant piping lines since some lines were ruptured by flow-accelerated corrosion (FAC) in 1978. Nowadays the CHECWORKS program has been used to manage pipe wall thinning phenomena caused by FAC. However, various erosion mechanisms can occur in carbon-steel piping. Most common forms of erosion are cavitation, flashing, liquid droplet impingement erosion (LDIE), and Solid Particle Erosion (SPE). Those erosion mechanisms cause pipe wall thinning, leaking, rupturing, and even result in unplanned shutdowns of utilities. Especially, in two phase condition, LDIE damages a wide scope of plant pipelines. Furthermore, LDIE is the major culprit to cause such as power runback by pipe leaking. This paper describes the methodologies that manage wall thinning and also predict LDIE wall thinning area. For this study, current properties of two-phase condition are investigated and LDIE areas are selected. The areas are checked by B-Scan method to detect the effect of wall thinning phenomena.

Synthesis of Nano-Scale Photocatalyic TiO2 Powder Doped with Ag by Sonochemistry Reaction (초음파화학 반응에 의한 Ag 도핑 광촉매용 나노 TiO2 분말의 합성)

  • Cho, Sung-Hun;Lee, Soo-Whon
    • Korean Journal of Materials Research
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    • v.19 no.3
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    • pp.169-173
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    • 2009
  • In chemistry, the study of sonochemistry is concerned with understanding the effect of sonic waves and wave properties on chemical systems. In the area of chemical kinetics, it has been observed that ultrasound can greatly enhance chemical reactivity in a number of systems by as much as a million-fold. Nano-technology is a super microscopic technology in which structures of 100 nanometers or smaller can be investigated. This technology has been used to develop $TiO_2$ materials and $TiO_2$ devices of that size. Thus far, electrochemistry methods and photochemistry methods have generally been used to create $TiO_2$ nano-size particles. However, these methods are complicated and create pollutants as a by-product. In the present study, nano-scale silver particles (5 nm) were prepared in a sonochemistry method. Sonochemistry deals with mechanical energy that is provided by the collapse of cavitation bubbles that form in solutions during exposure to ultrasound. $TiO_2$ powders 25 nm in size doped with Ag were formed using an ultrasonic sound technique. The experimental results showed the high possibility of removing pollution through the action of a photocatalyst. This powder synthesis technique can be considered as an environmentally friendly powder-forming processing owing to its energy saving characteristics.