• 대한약학회:학술대회논문집
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• 대한약학회 2003년도 Proceedings of the Convention of the Pharmaceutical Society of Korea Vol.2-2
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• pp.234.2-234.2
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• 2003

Recently, the need for ultra-fine particles, especially nano-sized particles has increased in the fields preparing raw powders such as pharmaceutical additive and high value added products in the Nano-Technology processes. Therefore, the research in ultra-fine grinding is very important, especially, in nanometer grinding. In the previous paper, a series of wet grinding experiments using grinding aids using a stirred ball mill have been performed on grinding rate constant based on grinding kinetics. (omitted)

• 한국공작기계학회논문집
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• 제16권6호
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• pp.1-8
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• 2007

The ultra-fine tungsten carbide(WC) powders have been actively used in the cemented carbides industry, because they have excellent mechanical properties such as high hardness, strength, and toughness. In this study, ultra-fine WC-Co alloys powders have been fabricated by thermochemical and thermomechanical process such as spray conversion process or high energy ball milling. The non-coated end-mill which is made of ultra-fine tungsten carbide is investigated by measuring cutting force, tool wear, tool life, and surface roughness profile according to cutting length. The machining test was conducted with high hardened workpiece and their performances are investigated in high speed cutting conditions. Also, the relationship between the machining characteristics and the Co contents are investigated under various high speed cutting conditions.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2006년도 춘계학술대회 논문집
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• pp.13-14
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• 2006

The quality of tool material is very important factor in machining evaluation. The characteristics of tungsten carbide, such as grain size and hardness, and density are depending on the variation of Co composition and WC size. In this study, the non-coated end mill which is made of ultra-fine tungsten carbide is investigated by measuring tool wear and tool lift test. The machining test is conducted with high hardened workpiece under high-speed cutting condition.

• 한국식품조리과학회지
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• 제29권2호
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• pp.129-135
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• 2013

분쇄방법(핀밀, 초미분쇄)을 달리하여 제분한 찰수수가루의 물리화학적 특성을 조사하였다. 조단백질 함량은 PS와 UFS에서 높았고, 조지방 함량은 핀밀분쇄보다 초미분쇄에서 더 높게 나타났다. 조회분과 총 식이섬유소 함량은 도정하지 않고 핀밀분쇄한 PWS에서 가장 높았다. 겉보기 아밀로오스 함량은 핀밀분쇄한 수수가루가 초미분쇄한 수수가루보다 높았으며 껍질이 없는 경우(PS, UFS) 아밀로오스 함량이 더 낮게 나타났다. 수수가루의 평균입도크기는 도정하지 않은 수수가루에서 컸으며 핀밀분쇄한 것이 초미분쇄보다 평균입도가 큰 것으로 나타났다. 수수가루의 색도는 초미분쇄 수수가루가 핀밀수수가루보다 밝았으며 UFS의 L값이 가장 높았고, 도정한 수수가루(PS, UFS)가 통곡수수(PWS, UFWS)보다 명도가 높았다. 수분결합력은 초미분쇄 시료 UFWS에서 가장 높았으며 핀밀분쇄 PWS보다 높았다. 용해도와 팽윤력은 초미분쇄한 시료가 핀밀분쇄 시료에 비해 모두 높게 나타났으며 도정한 수수가루에서 높게 나타났다. 수수가루의 손상전분 함량은 핀밀분쇄하여 도정한 경우 손상도가 컸다. 수수가루의 호화점도 특성에서 최고점도와 최종점도 PS와 PWS에서 높았고 UFS는 가장 낮은 점도를 나타내었다. 노화도를 나타내는 setback 점도 또한 PS와 PWS에서 높아 초미분쇄보다 노화도가 높게 나타났다. 핀밀분쇄한 통곡 수수가루(PWS)가 전체적으로 높은 호화점도곡선을 보였다. 총 페놀 함량은 핀밀분쇄 수수가루가 초미분쇄 수수가루보다 높았으며 통곡 수수에서 높게 나타났다. 이러한 결과들로 보아 수수는 도정 여부와 분쇄 방법에 따라 가루의 물리화학적 특성이 달라지므로 수수가루를 이용한 제품 개발 시 각 제품의 특성에 따른 적절한 제분방법이 필요하다고 할 수 있다.

• Journal of Applied Biological Chemistry
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• 제50권4호
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• pp.234-238
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• 2007

The effects of ultra-fine pulverization on the physicochemical properties of rice starch (RS) were investigated using a high impact planetary mill. After pulverization, RVA characteristics, peak viscosity, break down, and set back values of RS decreased from 274.75 to 9.42 RVU, 214.46 to 6.17 RVU, and 87.80 to 17.00 RVU, respectively. The pasting properties also changed significantly. X-Ray diffractogram revealed RS had four A-type peaks, which disappeared after pulverization. The peak temperature and gelatinization enthalpy of RS using differential scanning calorimetry (DSC) were 13.99 J/g at $75.14^{\circ}C$, whereas the pulverized RS (PRS) had two peaks, 0.13 J/g at $63.88^{\circ}C$ and 1.23 J/g at $101.24^{\circ}C$. DSC measurement showed the retrogradation degree of PRS was lower than that of RS after storage at 4 and $25^{\circ}C$. The enzymatic (${\alpha}$-amylase) digestibilities of RS and PRS were 72.7 and 77.3%, respectively.

• 한국분말재료학회지
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• 제20권2호
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• pp.100-106
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• 2013

Ultra-fine zirconium carbide (ZrC) powder with nano-sized primary particles was synthesized by the carbothermal reduction method by using nano-sized $ZrO_2$ and nano-sized graphite powders mixture. The synthesized ZrC powder was well dispersed after simple milling process. After heat-treatment at $1500^{\circ}C$ for 2 h under vacuum, ultra-fine ZrC powder agglomerates (average size, $4.2{\mu}m$) were facilely obtained with rounded particle shape and particle size of ~200 nm. Ultra-fine ZrC powder with an average particle size of 316 nm was obtained after ball milling process in a planetary mill for 30 minutes from the agglomerated ZrC powder.

• 소성∙가공
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• 제11권1호
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• pp.24-35
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• 2002

Recent trend and future prospect of flat rolling of steel has been summarized based on the earlier reports. Key technology in the plate rolling is to have ultra fine microstructure having high resistance against crack propagation during application. Heavy accelerated cooling facility and high power rolling mill will be helpful to develope the high toughness steel. Precise modeling of properly prediction based on deformation and transformation imposed on microstructure of steel during processing is highly anticipated. For the hot strip rolling process, new trend is lies on the production of ultra-thin gauged hot strip to substitute cold rolled strip. For the substitution of cold rolled strip into hot rolled strip widely, high formable property of hot strip is highly required. For the formabilit, the ferritic rolling of extra low carbon steel under high lubricated condition is essential. Recently introduced semi-continuous thin slab and rolling mill line is very plausible to develope those kinds of products easily In the view groin facility combination. New idea to modify the existing continuous hot strip mill line to produce the ultra thin-gauged hot strip in an economic way is suggested in this report.

• 한국잠사곤충학회지
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• 제43권1호
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• pp.41-48
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• 2001

The purification, dissolution and powdering of stained waste silk obtained from weaving and dyeing process were studied for the surface modification of textile fabric and plastic materials. The whiteness of stained waste silk could be improved through degumming and bleaching with sodium hydrosulfite. The water-soluble fibroin solution can be obtained by dissoving the degummed waste silk in a boiling solution of 50% calcium chloride for 60 minutes. The salts and heavy metals contained in fibroin solution were removed by electric dialysis, wool fiber filtration and gel filtration chromatography. The fibroin powder was prepared by using a fine grinder after the alkali treatment for weakening the silk fiber. The fine fibroin powder of particle size around 30 ㎛ was obtained with a ultra fine-mill, while it was finer below 10 ㎛ with a ball-mill. The dissolved or powdered silk was applied to the surface of fabric with addition of the binder (a urethane resin). The moisture content of polyester and nylon fabrics treated with the silk solution was improved due to hygroscopic property of silk. The fine fibroin powder mixed with the binder ws coated on the surface of synthetic film by use of the air pressed sprayer. It was revealed that the hygroscopicity as well as the softness of fibroin powder coated film was much improved. Therefore, it is thought that the fine silk fibroin powder is applicable as an coating agent for the surface modification of plastic and synthetic leather.

• Agricultural and Biosystems Engineering
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• 제6권2호
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• pp.70-76
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• 2005

Seed, stem and sprout of F. tataricum were separately milled using the ultra fine mill under the same condition to investigate the effect of roasting or extruding on the particle size, microstructure and water solubility of dietary fiber. The mean particle size of MR (roasting) is increased in stem and sprout, and that of ME (extruding) is increased in seed, compared to that of control. The microscopic views of seed show that control has the spherical shape but ME the larger and irregular shape, and those of stem and sprout show that control has the needle like shape but ME more rounded shape. Water solubility index of ME is much higher than that of control or MR in seed, stem and sprout. It shows that seed, stem and sprout are damaged more in extruding than in roasting, and the starch and cell wall structure must be destroyed to change the water insoluble dietary fiber into the water soluble dietary fiber.

• Applied Biological Chemistry
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• 제50권3호
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• pp.160-166
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• 2007

본 연구는 초미세 분체기술을 이용하여 쌀 전분의 입자구조 파괴가 이루어졌을 때 분자구조적, 물리적 변화가 어떻게 이루어지는지를 구명하고자 하였다. 분쇄 후 쌀 전분의 평균직경은 약 20% 감소가 이루어졌으며 비표면적은 25% 증가하였다. 분쇄 전후의 쌀 전분에 대한 분자량분포를 GPC(gel permeation chromatography)로 측정한 결과 Peak II의 면적이 36.5%에서 59.5%로 상승하였다. 분쇄 전후 손상전분 정도는 각각 16.40%와 99.2%로 나타났다. 분쇄 전에 비하여 분쇄 후 쌀 전분의 물결합능력, 용해도와 광 투과도에서도 월등히 높았다. $30^{\circ}C$에서 20 rpm을 기준으로 분쇄후의 쌀 전분의 겉보기점도는 상대적으로 분쇄 전의 7% 수준에 불과하였으며 측정온도가 높아짐에 따라서 차이는 더욱 커졌다.