• Title/Summary/Keyword: UV150

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A Quantitative Analysis of Dissolved Starch in White Water by UV Spectroscopy (분광분석법을 이용한 공정백수에서의 전분 정량분석)

  • Jung So-Hyun;Ryu Jeong-Yong;Kim Hyoung-Jin
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.37 no.4 s.112
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    • pp.38-43
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    • 2005
  • Natural Com Starch(NCS) spray system has been widely used In multiply board mill for the better bonding strength between board layers. However the unsuitable NCS spray system could lead to a drop in plybond efficiency of multiply board. It could also result in the accumulation of unretained-starch in the white water system, which could not only rise in BOD and COD level but also reduce the effects of rosin-alum sizing system and other additives. In this study, the simple and rapid method by UV-spectroscopy for measuring the starch contents in the white water was proposed, and the quantitative analysis for dissolved starch content in white water was carried out in two kinds of board production process. It could be confirmed that about 150 ppm of oxidized starch was retained in white water dewatered from undertop ply of multiply board process, and about 470 ppm of natural starch was dissolved in white water originated from unsuitable spraying system in the multiply board production lines for cup base paper.

Analysis of Alizarin Dye in Accelerated Degradation Conditions

  • Ahn, Cheunsoon
    • The International Journal of Costume Culture
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    • v.7 no.1
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    • pp.40-47
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    • 2004
  • The purpose of this research was to examine the degradation rate of alizarin in accelerated degradation conditions using the GC-MS quantitative analysis. Alizarin dye solution (2.5 x 10/sup -3/ M conc.) were kept in 150℃ oven for total of 7 days and the degradation rate was examined each day. 2.5 × 10/sup -4/M conc. alizarin dye solution was mixed with H₂O₂ according to [H₂O₂]/[dye] ratio 40 and were kept under 365㎚ UV for 2 hours, analyzed after 0, 30, 60, 90, 120min using the GC-MS. Gas chromatogram showed alizarin peak at 9.96 - 10.13 min. retention time range and residual peaks in the wide range from 9.6 to 11.1 min. Oven degradation exhibited an initial decrease in the amount of alizarin, which was followed by increasing amount in 4/sup th/ day. The decrease in the alizarin was significantly shown by the 7/sup th/ day. Same pattern was also observed in the H₂O₂/UV/O₂ degradation samples and was verified ed by the UV-VIS spectra. The differences in the amount of alizarin between 1/sup st/ day and 4/sup th/ day samples, 4/sup th/ day and 7/sup th/ day samples, and Control and 7/sup th/ day samples of the oven degradation were significant at alpha .20.

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Fabrication and Characterization of Nano-Sized ZnSe Powders by Hydrothermal Process (수열합성법에 의한 Zinc Selenide 나노 분말 합성 및 미세구조 특성 연구)

  • Kim, Mi-So;Hong, Hyun-Seon
    • Korean Journal of Materials Research
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    • v.27 no.9
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    • pp.459-465
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    • 2017
  • Nano-sized Zinc selenide (ZnSe) powder was successfully synthesized using Zn and Se precursors in a hydrothermal process. Temperature for the synthesis was varied from $95^{\circ}C$ to $180^{\circ}C$ to evaluate its influence on the microstructural properties of the synthetic particles. ZnSe powder thus fabricated was characterized using various analytical tools such as SEM, XRD, TEM and UV-Vis methods. Two types of ZnSe particles, that is, the precipitated particle and the colloidal particles, were identified in the analysis. The precipitated particles were around 100 nm in average size, whereas the average size of the colloidal particles was around 20 nm. The precipitated particles made at $150^{\circ}C$ and $180^{\circ}C$ were found to be a single phase of ZnSe; however, an inhomogeneous phase was obtained at the lower synthesis temperature of $95^{\circ}C$, suggesting that the temperature for the synthesis should be over $100^{\circ}C$. The precipitated particles were inactive in the UV-Vis absorption investigation, whereas the colloidal particles showed that absorptions occurred at 380 nm in the UV-Vis spectrum.

An Integrated Sensor Module for Diagnosis of Closed Switchboards (수배전반 진단을 위한 통합형 센서모듈)

  • Cha, Sang-Wook;Cha, Hyeon-Kyu;Park, Dae-Won;Park, Hee-Chul;Kil, Gyung-Suk
    • Proceedings of the KSR Conference
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    • 2011.10a
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    • pp.2043-2048
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    • 2011
  • According to the statistical report from National Emergency Management Agency (NEMA) in Korea, the accident rate of closed switchboards in power systems occupies over 40%. In this paper, an integrated sensor module for monitoring the condition of closed switchboards is described. The sensor module monitors electro-magnetic (EM) wave, ultra-violet (UV) ray, heat and smoke generated by electrical discharges or insulation breakdown. The effective detection ranges were decided from experiment results; 100 kHz~10 MHz for EM wave, 220 nm~395 nm for UV ray and 0~$150^{\circ}C$ for heat, respectively. The prototype sensor module includes all functions above-mentioned in one device.

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A Study on Liquid Crystal Alignment Effect on a Photopolymer Layer Based N-(phenyl)maleim ids Containing Three Kind of the Substituent (3가지 종류의 치환기를 함유한 N-(phenyl)maleimide계 광폴리머 표면을 이용한 액정 배향 효과에 관한 연구)

  • 황정연;이윤건;서대식;김준영;김태호
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.15 no.3
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    • pp.264-268
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    • 2002
  • Three types of polymer, a photoalignment material based N- (phenol)maleimide were synthesized and the liquid crystal (LC) aligning capabilities on the photopolymer layer were studied. A good LC alignment with UV exposure on the PMI5CA(N-(phenol)maleimide with 5-carbon chain cinnamoyl group) can be obtained. However, the LC alignment defects were observed on the PM13CA (N-(phenol)maleimide with 3-carbon chain cinnamoyl group) and PMIF (N-(phenyl)maleimide including fluoro cinnamoyl group). Also, the good LC alignment with UV exposure on the PM15CA surface was observed at until $150^{\circ}C$ of annealing temperature. The LC aligning ability on the photopolymer layer based N-(phenol)maleimide depends on the side chain length of photopolymer.

HPLC Determination of Loratadine in Human Plasma with UV Detection and Pharmacokinetics of Loratadine Following Oral Administration of Tablet Formulation in Human

  • Cho, Eun-Sook;Chun, In-Koo
    • Proceedings of the PSK Conference
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    • 2002.10a
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    • pp.420.2-421
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    • 2002
  • A validated UV determination of loratadine in human plasma was developed and the pharmacokinetic profiles of single dose of loratadine were determined in 8 healthy volunteers. Human serum samples (1.0 mL) spiked with known concentration of loratadine and 50 ng diazepam as an internal standard were alkalinized with 500 ${\mu}\ell$ ${\mu}\ell$ of 10% $Na_{2}CO_{3}$ and extracted with 7 mL of mixture of isopentane and hexane (2 : 1. v/v) for 5 min. Extracts were centrifuged and 6 mL of organic layer was back-extracted with 150 ${\mu}\ell$ of 12.5% $Na_{2}PO_{4}$ for 1 min. (omitted)

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Conductivity of copper(II)-phthalocyanine thin films due to a grain growth (결정 성장 조건에 따른 copper(II)-phthalocyanine 박막의 전기전도도 특성)

  • Park, Mie-Hwa;Yoo, Hyun-Jun;Lee, Kie-Jin
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.05a
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    • pp.132-136
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    • 2004
  • 열 증착 방법을 이용하여 copper(II)-phthalocyanine(CuPc) 박막을 glass 기판 위에 제작하였다. 열처리 조건은 $150^{\circ}C$에서 후열(annealing) 처리 하는 방식과 예열하는 두 가지 방식으로 달리하였다. 제작된 박막의 전기전도도를 평가하기 위해 마이크로웨이브 근접장 효과를 이용한 근접장 현미경(near-field scanning microwave microscope)을 이용하여 비파괴적인 방식으로 CuPc 박막의 반사계수(reflection coefficient)를 측정하였다. CuPc 박막의 전기전도도 특성을 UV 흡수도를 통한 에너지 밴드갭의 shift 현상과 관련지어 설명하고 또한 x-ray diffraction(XRD) data를 통해 박막의 결정 특성과 비교하였다. 박막 표면 특성은 SEM(scanning microscope microscopy)을 통해 관측하였다. 열처리 조건에 따른 CuPc 박막의 전기전도도 특성은 후열 처리한 박막의 경우 예열 처리한 박막보다 전기 전도 특성이 향상되었음을 관측할 수 있었다.

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Study of the breathable film processing techniques for microwave oven using a laser (레이저를 이용한 전자렌지용 숨쉬는 필름 가공 기술 연구)

  • Sohn, Ik-Bu;Choi, Hun-Kook;Yoo, Dong-Yoon;Noh, Young-Chul;Kim, Joung-Nyon;Kang, Ho-Min
    • Laser Solutions
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    • v.16 no.2
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    • pp.16-18
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    • 2013
  • In this paper, we fabricated breathable films on the use of microwave oven by using UV nanosecond laser micromachining, and the number of micro-grooves on the film is controlled for different oxygen transfer rate(OTR). As different number of micro-groove, the breath films of 100,000cc, 120,000cc, and 150,000cc can be fabricated. The breath film package of 120,000cc is used for the experiment of steaming a sweet potato. At the result, the sweet potato is well-cooked with enough moisture in the package not bursted.

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Deposition condition and Confirmation of Organic Charge Transfer complex Langmuir-Blodgett Film (유기전하 이동착물 Langmuir-Blodgett막의 누적조건 및 누적확인에 관한 연구)

  • Jeong, Soon-Wook
    • Journal of the Korean Applied Science and Technology
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    • v.14 no.1
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    • pp.89-93
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    • 1997
  • In this research, ultra-thin films of organic charge transfer complex were deposited on to ordinary microscope slide-glass subtrates with a Langmuir-Blodgett technique. ${\pi}$-A isotherm characteristics of these complex were studied in order to find optimum conditions of deposition by varying temperature of subphase, compression speed, and spreading amount. Transfer ratio of these films were studied during the process of deposition. The UV-visible absorbance spectra of LB films were measured to find state of deposition by varing layer number. The observed optimum conditions of surface, pressure, spreading amount, and dipping speed for depositing LB films(Y-type) were 38m/Nm, $150{\mu}l$ and 5mm/min, respectively. Since the tansfer ratio is close to 100%, the monolayer on the subphase seems to be well transferred to the solid substrate. The thickness of the film was well-controlled as the UV-vis absorbance of films were changed linear according to the number of layers.

Study on synthesis of CuPc derivative and preparation of its Langmuir- Blodgett Films. (($NO_{2}$가스센서용 phthalocyanine 유도체의 합성과 LB막의 제작 및 특성에 관한 연구)

  • Sohn, Byoung-Chung
    • Journal of the Korean Applied Science and Technology
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    • v.11 no.2
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    • pp.147-150
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    • 1994
  • Ultra thin films of HDSM-CuPc(Tetra-3-hexadecylsulphamoylcopperphthalocya-nine) were formed on various substrates by Langmuir-Blodgett method, where HDSM-CuPc was synthesized by attaching long-chain alkylamine(hexa-decylamine) to CuPc. The reaction product was identified with FT- IR, UV-visible absorption spectroscopies, elemental analysis and thin layer chromatography. The formation of ultrathin films of HDSM-CuPc was confirmed by FT-IR and UV-visible spectroscpies.