• Proceedings of the Korean Society for Agricultural Machinery Conference
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• 2002.02a
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• pp.471-478
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• 2002

초음파를 사과의 비파괴 품질판정에 이용하기 위한 기초연구로서 계측된 저장기간에 따른 사과의 초음파 특성과 본 연구에서 계측된 사과의 기계적 특성을 이용하여 초음파에 의한 사과의 탄성계수 및 생물체항복강도 예측모델을 개발하고자 하였으며, 결론은 다음과 같다. 1. UTM을 이용하여 사과의 기계적 특성치를 분석하여 생물체항복점, 생물체항복변형량, 생물체항복강도, 파괴점, 극한변형량, 극한강도 및 탄성계수 등을 구하였다. 2. 사과의 기본 물성, 초음파 특성과 기계적 특성값 들을 분석한 결과 사과의 질량, 체적, 시간영역의 진폭(PTP), 제3영역 에너지 스펙트럼 밀도함수가 기계적 특성 중 생물체항복강도, 탄성계수와 높은 상관성이 있는 것으로 나타났다. 3. 사과의 저장 기간, 질량, 체적, Peak-to-peak, 제3영역의 에너지값 등 5개의 독립변수를 가지는 다중선형회귀모형으로 사과의 탄성계수 및 생물체 항복강도 예측모형을 개발하였다.

• Journal of the Korean Society of Industry Convergence
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• v.5 no.4
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• pp.361-366
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• 2002

The change of mechanical properties of drawn PP filaments which was treated by isothermally annealed after elevated heating. Measurements were carried out with UTM for mechanical properties. Isothermally heat treatment were carried out $100^{\circ}C$, $120^{\circ}C$, $140^{\circ}C$ for 10min., 30min., 60min, in silicon oil bath. And isothermally heat treatment after elevated heating from $20^{\circ}C$ were carried out $100^{\circ}C$, $120^{\circ}C$, $140^{\circ}C$ for 10min., 30min., 60min., with heating rate of $1^{\circ}C/min$., $5^{\circ}C/min$., $10^{\circ}C/min$. From the results of this study, it found the following facts. Initial modulus and tensile strength were increased with increasing of annealed temperature and time. Also initial modulus of tensile strength of samples which were isothermally annealed after elevated heating from $20^{\circ}C$ were higher than those of isothermally annealed samples.

• Applied Chemistry for Engineering
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• v.31 no.3
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• pp.284-290
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• 2020

Energetic thermoplastic elastomers (ETPEs) based on glycidyl azide polymer (GAP) and carboxylated GA copolymers [GAP-ETPE and poly(GA-carboxylate)-ETPEs] were synthesized using isophorone diisocyanate (IPDI), dibutyltin dilaurate (DBTDL), 1,4-butanediol (1,4-BD), and soft segment oligomers such as GAP and poly(GA-carboxylate). The synthesized GAP-ETPE and poly(GA-carboxylate)-ETPEs were characterized by Fourier transform infrared (FT-IR), gel permeation chromatography (GPC), thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), universal testing machine (UTM), calorimetry and sensitivity towards friction and impact. DSC and TGA results showed that the introduction of carboxylate group in GAP helped to have better thermal properties. Glass transition temperatures of poly(GA-carboxylate)-ETPEs decreased from -31 ℃ to -33 ℃ compared to that of GAP-ETPE (-29 ℃). The first thermal decomposition temperature in poly(GA_0.8-octanoate_0.2)-ETPE (242 ℃) increased in comparison to that of GAP-ETPE (227 ℃). Furthermore, from calorimetry data, poly(GA-carboxylate)-ETPEs exhibited negative formation enthalpies (-6.94 and -7.21 kJ/g) and higher heats of combustion (46713 and 46587 kJ/mol) compared to that of GAP-ETPE (42,262 kJ/mol). Overall, poly(GA-carboxylate)-ETPEs could be good candidates for a polymeric binder in solid propellant due to better energetic, mechanical and thermal properties in comparison to those of GAP-ETPE. Such properties are beneficial to application and processing of ETPE.

• Applied Chemistry for Engineering
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• v.23 no.3
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• pp.339-343
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• 2012

Poly(olefin ketone) terpolymer having excellent mechanical properties was synthesized and composite materials of poly(olefin ketone) containing polyurethane/amino silane functionalized glass fibers were prepared. The compatibilities between the functionalized glass fiber and the polymer were characterized by observing the fracture surfaces of the composites using scanning electron microscopy (SEM). Mechanical properties of composites with different contents, diameters, lengths, and binders of glass fibers were also studied using universal testing machine (UTM). The introduction of suitably functionalized glass fiber into the poly(olefin ketone) produces composite materials having excellent mechanical properties and they are very promising alternative materials for the engineering plastic applications.

• Korean Journal of Materials Research
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• v.27 no.1
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• pp.43-47
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• 2017

E (Electric) -glass fibers are the most widely used glass fibers, taking up 90 % of the long glass fiber market. However, very few papers have appeared on the physical characteristics of E-glass fibers and how they depend on the fiberizing temperature of fiber spinning. Glass fiber was fabricated via continuous spinning process using bulk E-glass. In order to fabricate the E-glass specimen, raw materials were put into a Pt crucible and melted at $1550^{\circ}C$ for 2hrs; mixture was then annealed at $621{\pm}10^{\circ}C$ for 2hrs. The transmittance and adaptable temperature for spinning of the bulk marble glass were characterized using a UV-visible spectrometer and a viscometer. Continuous spinning was carried out using direct melting spinning equipment as a function of the fiberizing temperature in the range of $1175{\sim}1250^{\circ}C$, while the winder speed was fixed at 500 rpm. Subsequently we investigated the physical properties of the E-glass fiber. The average diameter of the synthesized glass fiber was measured by optical microscope. The mechanical properties of the fiber were confirmed using a UTM (universal materials testing machine); the maximum tensile strength was measured and found to be $1843{\pm}449MPa$ at $1225^{\circ}C$.

• Carbon letters
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• v.24
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• pp.82-89
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• 2017

In this study, composite PAN-based ACNFs embedded with MgO and $MnO_2$ were prepared by the electrospinning method. The resultant pristine ACNFs, ACNF/MgO and $ACNF/MnO_2$ were characterized in terms of their morphological changes, SSA, crystallinity and functional group with FESEM-EDX, the BET method, XRD and FTIR analysis, respectively. Results from this study showed that the SSA of the ACNF/MgO composite ($1893m^2g^{-1}$) is significantly higher than that of the pristine ACNFs and $ACNF/MnO_2$ which is 478 and $430m^2g^{-1}$, respectively. FTIR analysis showed peaks of 476 and $547cm^{-1}$, indicating the presence of MgO and $MnO_2$, respectively. The FESEM micrographs analysis showed a smooth but coarser structure in all the ACNFs. Meanwhile, the ACNF/MgO has the smallest fiber diameter ($314.38{\pm}62.42nm$) compared to other ACNFs. The presence of MgO and $MnO_2$ inside the ACNFs was also confirmed with EDX analysis as well as XRD. The adsorption capacities of each ACNF toward $CH_4$ were tested with the volumetric adsorption method in which the ACNF/MgO exhibited the highest $CH_4$ adsorption up to $2.39mmol\;g^{-1}$. Meanwhile, all the ACNF samples followed the pseudo-second order kinetic model with a $R^2$ up to 0.9996.

• Korean Journal of Agricultural Science
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• v.43 no.3
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• pp.432-440
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• 2016

The consumption of pre-treated vegetables (including fresh-cut vegetables) that are washed, peeled, and trimmed has been significantly increased because of their easy use for cooking. Vegetable cutting machines have been widely utilized for producing fresh-cut vegetables or agricultural products of different sizes; however, the design standard is not established for specific types of agricultural products. Therefore, this study was conducted to determine mechanical properties (compressive and shear forces) of targeted agricultural products (radish, carrot, squash, cucumber, shiitake mushroom, and sweet potato) for developing a multipurpose vegetable cutting machine. According to ASAE standard (s368.3), compressive and shear forces of targeted agricultural products were measured by using a custom built UTM (universal testing machine). Shape type of samples and speed ranges (5 - 15 mm/min) of loading rate on bioyield and shear points varied depending on the targeted agricultural product. The range of averaged bioyield points of targeted agricultural products were between 7.89 and 146.98 N. On the other hand, their averaged shear points ranged from 22.50 to 53.47 N. Results clearly showed that the bioyield and shear points of targeted agricultural products were thoroughly affected by their components. As measuring compressive and shear forces of a variety of agricultural products, it will be feasible to calculate blade cutting force for designing multipurpose vegetable cutting machine.

• Journal of Environmental Science International
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• v.24 no.8
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• pp.1037-1043
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• 2015

Since single-use disposable plastic usage has steadily been increasing, recent trends in polymeric research point to increasing demand for eco-friend materials which reduce plastic waste. A huge amount of non-degradable polypropylene (PP)-based pots for seedling culture are discarded for transplantation. The purpose of this study is to investigate an eco-friendly biodegradable material as a possible substitute for PP pot. The blend of poly(lactic acid) (PLA) with poly(butylene adipate-co-terephthalate) (PBAT) was used because of its good mechanical and flexible properties as well as biodegradation. After landfill, various properties of the blend pot were investigated by UTM, SEM, NMR and TGA. The results showed the tensile strength of the blend film rapidly decreased after 5 weeks of landfill due to degradation. From NMR data after landfill, the composition of PLA in the blend was decreased. These results indicate that the biodegradation of the blend preferentially occurs in PLA component. To investigate the effect of holes in pot bottom and side on root growth, a plant in the pot was grown. Some roots came out through holes as landfill period increases. These results indicate that the eco-friendly pot can be directly planted without the removal of pot.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.11 no.3
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• pp.1027-1034
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• 2010

Effects of inorganic nano-powders on the polymerization and thermal degradation kinetics as well as the mechanical properties of polyurethane nano-composites were studied by both the measurement of polymerization temperature as a function of time and non-isothermal thermogravimetric analysis (TGA) as well as the Instron test. As the results from polymerization studies, the reaction rates of MMT-filled PU composites were faster than those of Ce500-filled ones, and moreover, the activation energies using Kissinger method for the thermal degradation of composites were calculated as 139.34 kJ/mol for the Ce500-filled PU composites and 91.12 kJ/mol for MMT-filled one, respectivel, exhibiting that MMT nano-powder seemed to be acting as the catalyst for both polymerization and degradation of PU composites. UTM result, however, showed that tensile strength at break of MMT-filled composites was much higher than that of Ce500-filled ones above the concentrations range of 5 phr in the composites.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.12 no.5
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• pp.2451-2456
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• 2011

Inorganic micropowder(Ce500)-filled polyurethane composite foams were fabricated and the effects of postcure on the mechanical properties were studied by the measurement of polymerization temperature, TGA, and UTM test. Temperature for the maximum reaction rate of 20wt% Ce500-filled sample reached upto ca. $100^{\circ}$ within 10min. and, for the same sample, double mode thermal decomposition was observed around two distinguished temperatures of $250^{\circ}$ and $350^{\circ}C$. The activation energies for the decomposition were calculated using Kissinger method as 117.4 and 139.4 kJ/mol, respectively. While break strength and hardness of the sample seemed nearly affected by postcure time at $160^{\circ}C$, elongation, however, was significantly changed upto 1.72 times after 7hrs treatment. As the results, the condition of 7hrs at $160^{\circ}$ was considered as the optimum postcure condition for the Ce500-filled PU composite foam samples.