• Journal of the Korean Society for Heat Treatment
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• v.4 no.1
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• pp.1-12
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• 1991

This study has been performed to find out the effect of austenitizing temperature, austempering temperature and its holding time, and tempering cycle on the mechanical properties such as impact resistance, hardness etc. of AISI $M_2$ Mo series high speed tool steel austempered or tempered after austempering treatment. The results obtained from the experiment are as follows ; (1) Optical micrograph has revealed that the transformation rate of bainite is delayed as the austenitizing temperature increases and that bainite is most apparently transformed at an austempering temperature of $290^{\circ}C$. (2) The amount of retained austenite during austempering has been analysed to be increased by the X-ray diffraction technique as the transformation product of bainite is increased. It has also been shown that the longer the holding time of austempering, the more the transformation quantity of bainite is formed, exhibiting, however, that the rate of bainitic transformation is considerably retarded after a certain period of holding time elapses. (3) Hardness measurement has shown that hardness values obtained after austempering increase with decreasing the amount of retained austenite. (4) The austempering and then tempering cycle has been formed to give hardness values which are more greatly improved as austenitizing temperature is increased. (5) The mechanical property of the specimen primary-tempered for 1 hour at $550^{\circ}C$ after austempering for 2 hours at $290^{\circ}C$ from the austenitizing temperature range of $1180^{\circ}C$ to $1210^{\circ}C$ have been estimated to be good values.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2001.04a
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• pp.683-686
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• 2001

The thermomechanical characteristics of NITINOL shape memory alloy were evaluated using DSC with small samples and DMA with three-point bending specimens. The shape memory alloy of 54.4Ni/45.5Ti wt.% was used so that the austenite finish temperature was in the range of $50~100^{\circ}C$. Two types of sample were tested in the experiments corresponding to as-received and annealed conditions. Simple beam bending theory was used to calculate the dynamic moduli of the shape memory alloy. According to the results, a large discrepancy in transformation temperatures was found between DSC and DMA techniques. Annealing treatment was found to suppress the R-phase transformation during cooling and the secondary plateau in the austenite transformation. Such a heat treatment was also significantly influenced to raise the transformation temperatures and the moduli of the shape memory alloy.

• Transactions of the Korean Society of Mechanical Engineers
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• v.17 no.6
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• pp.1529-1540
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• 1993

The quenching of steels by water is one of the imprtant problems in the applications of heat treatment, but the fundamental researches by way of theoretical approaches have not been satisfactorily improbed yet. This study aimed at measuring the exact subcooled transient boiling curve for cylindrical specimens and at conducting the analytical researches into the prediction of cooling curves, including the latent heat of phase transformation of steel. Experiments of quenching were made with cylindrical specimens of carbon steel S45C of diameters from 12 to 30 mm and with Cu specimens of 12 mm diameter respectively. The internal temperature of specimens during the quenching process was measured by C-A sheathed thermocouple. The heat fluxes were numerically calculated by the numerical method of inverse heat conduction problem, using the measured inner temperature of specimen as a boundary condition. In case of ${\Delta}T_{sub}=80K$, $q_{s}$ is as follows $q_{s}=2.02{\times}10^{5}{\Delta}T_{set}^{0.05}:{\Delta}T_{set}\le500K.$ And the numerical analysis of unsteady heat conduction during the quenching process was made and the cooling curves were calculated by TDMA method.

• Journal of the Korean Society for Heat Treatment
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• v.22 no.1
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• pp.3-7
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• 2009

Variation in oxidation behavior with heat treatment temperature is investigated for a Ni-Ti alloy using X-ray diffraction, DSC (differential scanning calorimetry) and Auger electron spectroscopy. And the effect of oxidation on transformation behavior and superelasticity is characterized. A cold-worked 50.6Ni-Ti alloy is oxidized at 300-$700^{\circ}C$ for 1 hr in the air atmosphere. With an increase in heating temperature, the structure of $TiO_2$ changes from amorphous (300 and $400^{\circ}C$) to anatase ($500^{\circ}C$), and to rutile ($700^{\circ}C$). Activation energy of oxidation for NiTi is measured to be 51 Kcal/mol when heating temperature is $500^{\circ}C$ or above. Since Ti reacts preferably with oxygen, Ni content increases between matrix and oxide, forming $Ni_{3}Ti$ compounds. The resultant of oxidation decreases significantly $M_s$ and $A_s$ temperature in the specimen oxidized at $900^{\circ}C$ with $B_2{\rightarrow}M$ transformation path. An extra is found on cooling between two peaks in the specimen with $B_2{\rightarrow}R{\rightarrow}M$ one which is oxidized at $900^{\circ}C$ and aged at $500^{\circ}C$. Oxidation deteriorates superelasticity due to formation of Ni-rich compound.

• Korean Journal of Materials Research
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• v.26 no.5
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• pp.287-291
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• 2016

The effect of heat treatment on the microstructure and mechanical properties of cast Ti-6%Al-4%V alloy was investigated. Heat treatment of cast Ti-6Al-4V alloy was conducted by solution treatment at $950^{\circ}C$ for 30 min; this was followed by water quenching and then aging at $550^{\circ}C$ for 1 to 1440 min. The highest hardness of the heat-treated specimens was obtained by solution treatment and subsequent aging for 5 min due to precipitates of fine ${\alpha}$ that formed from retained ${\beta}$ phase. The tensile strength of this alloy increased without dramatic decrease of the ductility due to microstructural refinement resulting from the decomposition of ${\alpha}^{\prime}$ martensite into fine ${\alpha}$ and ${\beta}$ phases, and also due to the fine ${\alpha}$ phase formed from the retained ${\beta}$ phase by aging treatment for 5 min. In addition, this strengthening might be caused by the transformation induced plasticity (TRIP) effect, which is a strain-induced martensite transformation from the retained ${\beta}$ phase during deformation, and which occurs even after aging treatment at $550^{\circ}C$ for 5 min.

• Journal of the Korean Society for Heat Treatment
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• v.4 no.3
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• pp.54-62
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• 1991

The effect of tempering temperature on the ultrasonic propagation velocity at SCM 440 steel quenched from $870^{\circ}C$ and $1000^{\circ}C$ has been studied by metallurgical and crystallographical observation. The measurements of ultrasonic velocity were made on the specimen by appling an immersion ultrasonic pulse-echo technique with a constant frequency of 10 MHz. The quenched microstructure of this steel was a lath martensite. As the tempering temperature was increased, the martensite was transformed into the tempered martensite composed of cementite and carbide. The ultrasonic velocity increased with increasing the tempering temperature. It was thought that these were resulted from the microstructural transformation. The change of ultrasonic propagation velocity with quenching and tempering heat treatment was resulted from microstrain due to the change of internal stress. Considering these results concerning to the change of ultrasonic propagation velocity. the phenomena of microstructural transformation were estimated. Consequently, it was thought that the degree of quenching and tempered heat treatment of steel could be nondestructively evaluated with the change of ultrasonic propagation velocity.

• Journal of Welding and Joining
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• v.25 no.5
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• pp.36-44
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• 2007

This paper is the first part of the study on the accuracy improvement of numerical analysis of steel welds. The aim of this paper is to raise the accuracy of thermal analysis results, such as the shape and size of the weld cross section and the hardness distribution in HAZ(Heat-Affected Zone). It is known that the factors affecting on the accuracy are thermal properties, metallurgical properties and welding heat source model. It was found that the arbitrary distributed heat source model should be used to predict practical weld cross section shape and size. Also, in order to improve the prediction accuracy of HAZ hardness distribution, it was essential to consider 2 CCT(Continuous Cooling Transformation) diagrams in calculating volume fraction of transformed phases. One is the peak temperature being around melting temperature. The other is the peak temperature being around metallurgical transformation temperature.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2003.05a
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• pp.42-45
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• 2003

The phase transformation of $REBa_2Cu_3O_{7-x}$ (RE=Nd, Gd, Dy) was investigated using isothermal heat-treatment and continuous cooling in air. During continuous cooling, the $REBa_2Cu_3O_{7-x}$ (RE=123) superconducting phase with well-distributed $REBa_2Cu_3O_{7-x}$ (RE-211) was obtainde at a cooling rate of $0.001^{\circ}C$/s. Single phase RE-123 (Nd, Gd, Dy) was stable at $1050^{\circ}C$, $1050^{\circ}C$, and $950^{\circ}C$ during isothermal heat-treatment, respectively. Above these temperatures the RE-211 phase existed within the RE-123 grains. The RE-123, RE-211, $BaCu_2Od_2$, and CuO phases coexisted at $50^{\circ}C$ below the partial melting temperature for each respective rare-earth RE-123.

• Journal of Korean Medical classics
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• v.32 no.4
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• pp.67-90
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• 2019

Objectives : This study aims to summarize Tang Zong-hai's Qi transformation theory of the Six meridians through his book "Shanghanlun Qianzhubuzheng傷寒論淺注補正" where he integrated Western anatomy with the Qi transformation theory of East Asian Medicine to interpret Zhang Zhong Jing's "Shanghanlun(傷寒論)". The objective is to assist clinical application. Methods : Focusing on the contents of disease of the six meridians in the "傷寒論淺注補正", Tang's theories on the function of Zangfu(臟腑), Opening-Closing-Pivot(關闔樞), Inter-communication of Zangfu(臟腑相通), the Twelve Meridians(十二經脈) from his other publication "中西匯通醫經精義" were examined and related to in the process of explaining Qi transformation theory in detail. Results : 1. The Qi transformation function of the Taiyang meridian is related to "膀胱者, 氣化則能出" where the Small Intestine and Bladder inter-communicate. 2. The Qi transformation function of the Yangming meridian is related to the control of dryness and dampness through the Qi transformation of "陽明不從標本, 從乎中." 3. The Qi transformation function of the Shaoyang meridian is related to the Life-Fire function of the Triple Energizer-Gallbladder-Pericardium coalition through "少陽屬腎." 4. The Qi transformation function of the Taiyang meridian refers to the Heart Fire nurturing the Spleen Earth by creating 膏油 through veins. 5. The Qi transformation function of the Shaoyin meridian is related to the controlling of the Nutrient Qi(營氣) and Defense Qi(衛氣) through '心主血脈, 腎主元氣.' 6. The Qi transformation function of the Jueyin meridian is related to the ability of 和風 which results from '陰盡陽生' to harmonize and control the balance of Water Coldness(水冷) and Fire Heat(火熱). Conclusions : Tang's Qi Transformation Theory of the Six Meridians is his key theory explained from the perspective of Qi transformation of disease in the six meridians of "Shanghanlun", closely related to basic theories such as theory of Zang form(臟象學說), Opening-Closing-Pivot(關闔樞), Inter-communication of Zangfu(臟腑相通), the Twelve Meridians(十二經脈) of East Asian Medicine.

• Journal of the Korean Society for Heat Treatment
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• v.37 no.2
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• pp.79-85
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• 2024

The effects of annealing heat treatment and the addition of Cu element on the shape memory effect of the NiTi-based alloy were investigated by analyzing differential scanning calorimeter results and characterizing recovery rate through 3D scanning after Vickers hardness test. Through 3D scanning of impressions after Vickers hardness test, the strain recovery rates for specimens without annealing treatment and annealed specimens at 400, 450, and 500℃ were measured as 45.96%, 46.76%, 52.37%, and 43.57%, respectively. This is because as the annealing temperature increases, both B19' and NiTi₂ phases, which can impede martensitic transformation, are incorporated within the NiTi matrix. Particularly, additional phase transformation from R-phase to B19' observed in specimens annealed at 400 and 450℃ significantly contributes to the improvement in strain recovery rates. Additionally, the results regarding the Cu element content indicate that when the total content of Ni and Cu is below 49.6 at.%, the precipitation of fine B19' and NiTi₂ phases within the matrix can greatly influence the transformation enthalpy and temperature range, resulting in relatively lower strain recovery rates in NiTi alloys with a small amount of Cu element produced in this study.