• Title/Summary/Keyword: Trace analysis

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Drinking conditions of adolescents ; Korea Youth Risk Behavior Web-based Survey (청소년의 음주 실태 ; 청소년 건강행태 온라인 조사를 중심으로)

  • Choi, Young-Sil
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.18 no.9
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    • pp.186-192
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    • 2017
  • Thepurpose of this study was to provide a basic data health plan & education program for adolescents by examining the recent 3 year Korea Youth Risk Behavior Web-based Survey data obtained in 2013, 2014 and 2015. The data was analyzed with theSPSS 18.0 statistical program using the t-test and cross-analysis. After confirming the drinking habits of teenagers in Korea, the issue was slightly lower in the issue of problem drinking. However, the first time for drinking alcohol was the 2nd grade of middle school(21.5%) and the average alcohol intake was 20 to 29 days(3.8%) and usually consisted ofmore than two bottles (12.2%)s. Also, the method of buying liquor was found to be mainly at convenience stores(32%), and the adolescents werefound not to have been trained for drinking(52%). As a result of comparing the general characteristics of these items, it was found that there was a significant difference between the coeducation type, the high school type, the trace in the residence type, and the 'middle-high level' in terms of the socio-economic level.When comparing the results of the drinking behavior during these three years, the outcome of the trend is still noteworthy, as health education for drinking alcohol is still important, and attention needs to be paid to this problem.

A Study on Relation of Attached Algae and Odor's Cause in Sedimentation Basin of Water Treatment Plant (정수처리공정 중 침전지 부착조류 특성과 이취발생에 관한 연구)

  • Kim, Young-Ung;Son, Hee-Jong;Yu, Myung-Ho;Lee, Chun-Sik;Cho, In-Cheol;Kim, Eun-Ho;Seung, Nak-Chang
    • Journal of Korean Society of Environmental Engineers
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    • v.22 no.5
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    • pp.887-894
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    • 2000
  • The purposes of this study are investigation of species of attached algae and the relation between attached algae and odor in tap water, Oscillatoria sp. and Mougeotia sp. were colonized at sedimentation basin in water treatment plant. Resulting from analysis, 3.7ppt of geosmin and dimethyl-disulfide with trace were detected in sample of Oscillatoria sp. only, 22 compounds were found in each of sample that had been incubated in room temperature for 5 days, 17 compounds were generated by algal decay. Decayed products were sulfur compounds of 10 species such as dimethyl-sulfide and phenol, p-cresol, indole and scatole. So, it is assumed that attached algae which tolerant to chlorine was the origin of odor in tap water. They usually formed big colonies. Colonies on the bottom were decayed because of anaerobic state. While decaying they were detached from colonies and so, odorous compounds are originated from this decayed algae.

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Material Characteristics of White Wares from Yeongdong Province, Gangwon-do: Gangneung and Donghae Kiln Sites (강원 영동지역 백자의 재료과학적 특성 연구: 강릉 남양리 백자가마터와 동해 발한동2(사문동) 가마터를 중심으로)

  • Lee, Byeong Hoon;So, Myoung-Gi
    • Journal of Conservation Science
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    • v.31 no.3
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    • pp.181-192
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    • 2015
  • This study aims to examine production technique of twelve white wares from the Gangneung Namyang-ri and Donghae Balhan-dong2(Samun-dong) kiln sites, Kangwon Province and characteristics of the used materials, and to find a correlation among materials of the excavated white wares. X-ray fluorescence sequential spectroscopy(XRF), X-ray diffraction(XRD), Dilatometer and Inductively coupled plasma mass spectrometry(ICP-MS), Inductively coupled plasma automic emission spectrometer(ICP-AES) were applied to determine the chemical composition, crystalline phase of samples, firing temperatures, trace elements and rare earth elements. When analyzing body crystalline phases of the white wares using the XRD method, quartz and mullite were extracted from all the samples. Though firing temperature of each sample was different, they were mostly fired at a temperature below $1200^{\circ}C$. Analyzing the excavated white wares using the Seger formula, compositional properties of white wares in Gangneung Namyang-ri kiln showed diffrently from the Donghae Balhan-dong2(Samun-dong) kiln. The body of white wares from Gangneung Namyang-ri kiln have higher raito of $RO_2$ and $RO+R_2O$ than of white wares from Donghae Balhan-dong2(Samun-dong) kiln site. The white wares from Gangneung Namyang-ri kiln and Donghae Balhan-dong2(Samun-dong) kiln were made of host rocks of the different geological origin, according to the result of rare earth elements analysis.

High Resolution for Shallow Seismic Reflection (Applied to the Underground Cavity) (천부층 지진파 반사에 대한 해상도 (지하 공동에 응용))

  • 김소구
    • The Journal of Engineering Geology
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    • v.3 no.2
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    • pp.167-176
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    • 1993
  • The high resolution studies for shallow seismic reflection are carried out using 24-channel seismograph and the high sensitivity geophone(50-500Hz). In order to study the underground structures such as small faults, fractures, cracks and cavities, it is of great importance to enhance high resolution of the seisrnic records for the targets vertically and laterally. In analysis of high resolution seismic reflection, Nyquist frequency($F_N$) should be lager than the highest frequency in the records and the highest wave number should not be exceed the Nyquist wave number($1/2{\Delta}x$). The highest frequency above the Nyquist will be removed using low pass filter or antialias filter. The trace interval Ax should be taken into account so that the highest wave number(f/v) can be less than $1/2{\Delta}x$. The Fraunhofer diffraction of a hyperbola seismic section above the tunnel appeares on the common offset method, and little first arrivals of direct wave on the single-end shooting, delayed strong impulsive reflections are also shown above the tunnel. Ray Method(Cherveney and Psencik, 1983) also represents the same results that the reflected waves from the tunnel are delayed and single impulsive with little first arrivals, while transrnitted waves through the tunnel are delayed with low frequency.

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Characteristics of Fracture Systems in Southern Korea (우리나라 단열구조의 특성)

  • 김천수;배대석;장태우
    • The Journal of Engineering Geology
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    • v.13 no.2
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    • pp.207-225
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    • 2003
  • According to the data analysis of the regional fracture systems in southern Korea, the fracture orientations show three dominant sets : NNE, NW and WNW. A NNE set is the most abundant and includes most of the largest fractures. The highest fracture density is shown in the Taebaegsan mineralized area corresponding to Ogchon nonmetamorphic belt and the lowest one in the southwestern area of southern Korea. In addition, the density is higher in nonmetamorphic sedimentary rocks such as Choseon Supergroup. Pyeongan Supergroup, Daedong Supergroup and Kyeongsang Supergroup than in Precambrian basements and Jurassic granites. The regional fractures in southern Korea can be classified into four orders designated $F_1,{\;}F_2,{\;}F_3{\;}and{\;}F_4${\;}and{\;}F_4$ on the basis of their trace length. It is quite significant that fractures of each order are self-similar with respect to orientation and the combined fracture length distribution indicates a power-law distribution with an exponent of -2.04. As fractures were analyzed based on the tectonic provinces, Gyeonggj Massif and Kyeongsang Basin have all orders of fractures from $F_1$ to $F_4$. Most of the large scale faults may be ascribed to the products of slip accumulation through multiple deformation. Others besides $F_1$ fractures are thought to be evenly distributed through the whole area of southern Korea.

Principles and Applications of Multi-Level H2O/CO2 Profile Measurement System (다중 수증기/이산화탄소 프로파일 관측 시스템의 원리와 활용)

  • Yoo, Jae-Ill;Lee, Dong-Ho;Hong, Jin-Kyu;Kim, Joon
    • Korean Journal of Agricultural and Forest Meteorology
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    • v.11 no.1
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    • pp.27-38
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    • 2009
  • The multi-level profile system is designed to measure the vertical profile of $H_2O$ and $CO_2$ concentrations in the surface layer to estimate the storage effects within the plant canopy. It is suitable for long-term experiments and can be used also in advection studies for estimating the spatial variability and vertical gradients in concentration. It enables the user to calculate vertical fluxes of water vapor, $CO_2$ and other trace gases using the surface layer similarity theory and to infer their sources or sinks. The profile system described in this report includes the following components: sampling system, calibration and flow control system, closed path infrared gas analyzer(IRGA), vacuum pump and a datalogger. The sampling system draws air from 8 inlets into the IRGA in a sequence, so that for 80 seconds air from all levels is measured. The calibration system, controlled by the datalogger, compensates for any deviations in the calibration of the IRGA by using gas sources with known concentrations. The datalogger switches the corresponding valves, measures the linearized voltages from the IRGA, calculates the concentrations for each monitoring level, performs statistical analysis and stores the final data. All critical components are mounted in an environmental enclosure and can operate with little maintenance over long periods of time. This report, as a practical manual, is designed to provide helpful information for those who are interested in using profile system to measure evapotranspiration and net ecosystem exchanges in complex terrain.

Monitoring of norovirus and indicator microorganisms from agricultural products and environmental samples in Korea (한국에서의 농산물 및 환경시료에서 노로바이러스와 위생지표세균의 모니터링)

  • Kang, Ji Hyun;Shim, Hye Mee;Kim, Kwang Yup
    • Korean Journal of Food Science and Technology
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    • v.49 no.2
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    • pp.123-131
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    • 2017
  • Norovirus causes frequent epidemic viral gastroenteritis in Korea. The team for the control of noroviral foodborne outbreaks (NOROTECL) executed a project to trace the cause of norovirus contamination in agricultural products and environmental samples to reduce norovirus outbreaks in Korea. Between January and November in 2015, the contaminations by norovirus and indicator microorganisms such as coliforms, Escherichia coil and male specific coliphage (MSC) were examined in 80 agricultural products, 80 soil samples, 78 human feces samples, 3 animal feces samples, 80 agricultural water samples and 80 river water samples. Semi-nested PCR and DNA sequencing revealed 18 genogroup I and 3 genogroup II noroviruses in a total of 18 samples. These noroviruses were validated by real-time (RT)-PCR analysis. For indicator microorganisms, coliform and E. coli were respectively detected in agricultural products (68, 1%), soils (88, 7%), human feces (44, 12.8%), animal feces (67, 67%), agricultural waters (74, 30%) and river waters (96, 51%). The MSC results revealed 14 positive samples.

Micro-Determination of D-Amino Acids in Food by Using Achirai/Chiral Coupled Column Method (Achiral/Chiral Coupled Column법에 의한 식품 중의 D-아미노산의 정량분석)

  • Lee, Sun-Haing;Chang, Youn-Hee;Lee, Kwang-Pill
    • Analytical Science and Technology
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    • v.9 no.1
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    • pp.52-61
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    • 1996
  • Detectable levels of several free D-amino acids were found in some food. This was accomplished by using a column switching method. The determination of total amount of D- and L-amino acids was based on an achiral separation with a $C_{18}$ column. The level of D-amino acids to L-amino acids was determined by the column switching system including the postcolumn reaction detection of the amino acids derivatized with O-phthalaldehyde. The chiral separation of the postcolumn detection system was carried out with chiral crown ether column. This system was applied for the micro-determination of D-amino acids in food such as soy sauce, fermented soy bean and beans. It turned out that the sampling process is critical for the trace analysis of D-amino acids under this achiral / chiral coupled-column system. It was found that commercial soy sauce contained 42ppm, conventional soy sauce 102ppm, fermented soy bean 8.34mg per 1g and bean 2.87mg per 1g sample for phenylalanine. D-phenylalanine was found 0.67% in commercial soy sauce, 0.34% in conventional soy sauce, less than 1.81% in fermented soy bean, and Jess than 2.82% in bean.

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A Study on the Gas Chromatographic Analysis of Alcohols and Organic Acids during Takju Fermentation (가스 크로마토그래피에 의한 재래주 발효중 알코올과 유기산 분석)

  • Choi, Sun-Hee;Kim, Ok-Kyung;Lee, Myung-Whan
    • Korean Journal of Food Science and Technology
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    • v.24 no.3
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    • pp.272-278
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    • 1992
  • Takju, a Korean traditional wine, was prepared by using nuruk and Koji which were inoculated with Aspergillus kawachii and Aspergillus shirousamii. Those chemical composition such as alcohols and organic acids were determined with gas chromatography to investigate the variation of its content by the fermentation. Alcohol such as methyl, ethyl, n-propyl, i-butyl, i-amyl alcohol were detected in the most takju mash samples. Alcohol contents in the groups fermented with KNR and SNR were slightly higher than KKR, SKR groups. Lactic acid were concentrated and organic acids such as pyruvic, oxalic, malonic, succinic, maleic, malic, ${\alpha}-keto$ glutaric acid were also detected in the most samples. The pH was lowest in the KKR group. The total acid content was slightly decreased at the later fermentation and was highest in KKR. The content of minerals were highest in the WNR and BNR groups. Throughout fermentation the content of potassium and magnesium varied greatly with the tested groups.

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Comparative Analysis of the Bufonis Venenum by Using TLC, HPLC, and LC-MS for Different Extraction Methods

  • Lee, Hyo-Jae;Koung, Fan-Pei;Kwon, Ki-Rok;Kang, Dae-In;Cohen, Lorenzo;Yang, Pei-Ying;Yoo, Hwa-Seung
    • Journal of Pharmacopuncture
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    • v.15 no.4
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    • pp.52-65
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    • 2012
  • Objectives: Toad venom, called Chan-Su, is a traditional Oriental medicine secreted from the auricular and the skin glands of the Bufo bufo gargarizanz Cantor or B. melanosticus Schneider and has been widely used in China, Korea and other parts of Asia for the treatment of pain, heart conditions, and cancer. We examined the concentrations of the main chemical constituents within a commercially available toad venom product and compared the levels for different extraction methods. Methods: Toad venom was extracted using either cold or hot water, ethanol (EtOH), methanol (MeOH), or ethyl acetate (EtOAc), was fractionated using precipitation or reflux, and was then analyzed using thin layer chromatography (TLC), high-performance liquid chromatography (HTLC), and liquid chroma-tography - mass spectrometry (LC-MS). Individual components were identified by comparisons of the retention times, the ultraviolet spectra, and mass spectras and differences in chemical constituents for different solvents and extraction methods are presented. Results: Components with authentic standards, including serotonin and bufodienolides (cinobufagen, bufalin, cinobufalin, and resibufogenin), were detected. The water extract of toad venom contained the greatest amount of serotonin ($75.7{\pm}0.1$ mg/g), but very small amounts of bufodienolides ($3.8{\pm}0.0$ mg/g). In contrast, the use of MeOH or EtOH extraction solutions resulted in 5-26 times higher concentrations of bufodienolides, with only trace amounts of serotonin. The relative and the absolute concentrations of the component also varied based on the extraction method; i.e., EtOH extracts yielded the greatest total amounts of bufodienolides, and EtOAc precipitation had the lowest amounts of bufodienolides. Conclusions: Toad venom consists of serotonin and several bufodienolides, and the choice of solvent to extract chemical the constituents is important as a way to enrich the purported active components for treating different conditions.