• Title/Summary/Keyword: Total Ash

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Selection of Herbal Medicines Requiring Quality Control for Loss on Drying, Total Ash, and Acid-insoluble Ash in Korea

  • Kim, Dong-Gyu;Kim, Bog-Soon;Kim, Yeon-Cheon;Hwang, Young-Ok;Chae, Young-Zoo;Park, Seung-Kook
    • Natural Product Sciences
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    • v.17 no.1
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    • pp.38-44
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    • 2011
  • The quality inspections items such as loss on drying, total ash, and acid-insoluble ash contents in herbal medicines, have a correlation with external sources of pollution, but are not themselves hazardous factors. Z-scores for standard normal distribution were used to investigate herbal medicines requiring quality control, which exceeds the regulatory limits of quality inspection. In total, 7,773 samples were analyzed based on plant parts. For the loss on drying, the numbers of items of herbal medicines requiring quality control are like these; 15 items for above-ground parts and 5 items for underground parts. For the total ash, 21 items for above-ground parts and 4 items for underground parts. For the acid-insoluble ash, 8 items for above-ground parts and 1 item for underground parts.

Analysis of Contents and Deviations of Chemical Constituents of flue-cured leaf Tobacco from 1997 to 2001 Crop Years (연산별 황색종 가공엽의 화학성분 함량 및 편차 분석)

  • 김상범;정기택;조수헌;김용규
    • Journal of the Korean Society of Tobacco Science
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    • v.25 no.1
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    • pp.20-26
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    • 2003
  • To investigate the effects of reduction of leaf processing factories on the uniformity of processed leaf quality, the contents and their C.V.(Coefficient of Variation) of chemical constituents of flue-cured leaf tobacco produced from 1997 to 2001 and processed at various factories were analysed. The average leaf chemical contents of 12 grades for 5 years ranged as follows ; nicotine 2.00∼0.85%. total sugar 10.7∼16.9%, total nitrogen 2.36∼2.78%, crude ash 14.6∼15.6% and chlorine 0.50∼0.75%. The variations of chemical contents among crop years was higher in total sugar content while lower in crude ash content. The C.V. of chemical content in same grade leaves was higher in chlorine content while lower in total nitrogen and crude ash contents, and the ratio of C.V. among processing factories/C.V. in total population was higher in total sugar content while lower in crude ash content. When the leaves were processed at one factory, the deviations of chemical contents reduced considerably. Particularly, the decreasing effect of deviation was higher in total sugar content.

A Study on the PCBs-containing Waste Treatment by High Temperature Incineration (고온소각에 의한 PCBs 함유 폐기물처리에 관한 연구)

  • Kim, Seong-Jung;Kim, Dong-Hyuk
    • Journal of the Korea Organic Resources Recycling Association
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    • v.17 no.1
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    • pp.88-95
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    • 2009
  • This study is for understanding the domestic possibilities of the high temperature incineration of waste containing Polychlorinated Biphenyls (PCBs) with the analysis of normal operation case and waste gas, fly ash, dioxin about bottom ash, Total-PCBs, Co-PCBs, and the for analysis the heavy metal leaching feature included by bottom ash and fly ash, heavy metal leaching experiment was implemented. The result shows the dioxin density of the waste gas from waste containing PCBs was $0.00699{\sim}0.00763ng-TEQ/Nm^3$, which is lower than $0.0192ng-TEQ/Nm^3$ from the normal operation case. And each Co-PCBs and total PCBs shows $0.00043{\sim}0.00112ng-TEQ/Nm^3$ and $3.06{\sim}3.87ng/m^3$ respectively. The bottom ash test result shows Dioxin 0.00225~0.00630ng-TEQ/g, Co-PCBs 0.00027~0.00082ng-TEQ/g, Total PCBs 0.9~2.6ng/g, and the fly ash shows Dioxin 0.00164~0.00344ng-TEQ/g, Co-PCBs 0.00053~0.00054ng-EQ/g, Total PCBs 0.64~0.84ng/g. The bottom ash and fly ash experiments for heavy metal leaching did not show any leaching but when it comes to the ingredients of the fly ash, Pb elements shows 31.01~237.7ppm, higher than leaching criterion. The analysis of the density of all air pollution material from the waste gas shows the lower value than permissible criterion.

Monitoring of total ash, acid-insoluble ash and heavy metals content contained in herbal medicines classified by parts used (한약재의 약용부위에 따른 회분, 산불용성회분 및 중금속 함량)

  • Kim, Dong-Gyu;Kim, Kyung-Sik;Lee, Sung-Deuk;Jung, Kweon;Park, Seung-Kook
    • Analytical Science and Technology
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    • v.27 no.2
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    • pp.114-120
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    • 2014
  • The aim of this study was to investigate of total ash, acid-insoluble ash and heavy metals content contained in commercial herbal medicines classified by parts used. A total of 1504 samples (84 species) purchased from markets in Seoul, are classified by five kinds of plant parts. The mean of total ash and acidinsoluble ash content (%) were as follows; Herba 9.0, 1.1, Caulis and cortex 6.1, 1.0, Flos fructus and semen 5.1, 0.8, Radix 4.6, 0.7 and Rhizoma 4.3, 0.4. The total amount of individual heavy metals content (mg/kg) (Pb, As, Cd and Hg) was high in Herba 1.13 and decreased in the order of Caulis and cortex 1.07, Rhizoma 0.91 and Radix 0.91, and was low in Flos fructus and semen 0.73. In addition, acid-insoluble ash contents was correlated with the total amount of individual heavy metals (r=0.314) (p<0.01).

A Study on Ingredient and Bacterial Contamination of Bean Curd on the Market (市販豆腐 成分 및 細菌汚染에 관한 硏究)

  • Hong, Ki-Wha
    • Journal of Environmental Health Sciences
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    • v.9 no.2
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    • pp.1-10
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    • 1983
  • The purpose of this study was to analyze general ingredient of bean cured on the market and to examine its exposure to bacterial contamination. For this study, 17 samples (each 9 samples for general bean curd, soft bean curd, and uncurdled bean curd) were randomly collected from nine areas in Seoul from the beginning of April, 1983 to the beginning of June, 1983. The result of ingredient analysis of moisture, ash, and protein of bean curd was compared with the standard set by the Ministry of Health & Social Affairs. In order to find out exposure of bean curd on the market to bacterial contamination, total biological bacteria and coliform group were examined. Experimental results were shown as follows 1) Results of ingredient analysis of moisture, ash, and protein of general bean curd showed that total samples in both moisture and protein met the standard set by the Ministry of Health & Social Affairs but 44.4% of the samples in ash was below the above standard, indicating average 82.0%, 0.9% and 9.6% in moisture, ash, and protein order. 2) Experimental results of moisture, ash, and protein of soft bean curd demonstrated 90.2%, 0.5% and 4.3% respectively total samples in both moisture and protein satisfied the self-criteria set by the Soft Food Co-operative Association of Seoul City but 11.1% of the samples in ash didn't meet the self-criteria. 3) Total samples of uncurdled bean curd satisfied the self-criteria set by the above association, indicating average 92.0%, 0.4%, and 3.5% in moisture, ash, and protein order. 4) Total biological bacteria and coliform group detected in general bean curd showed that more than 10$^5$/g in total biological bacteria accounted for 88.8% of the samples and that 10$^4$/g or more in coliform group accounted for 77.7% of the samples. The result proves that general bean curd has been exposured to a severe bacterial contamination. 5) Result of total biological bacteria and coliform group detected in such packed bean curd as uncurdled bean curd and soft bean curd showed that 61.6% of the samples exceeded 10$^6$/g in total biological bacteria and 27.7% of the samples exceeded 10$^3$/g in coliform group. 6) According to the change with time and temperatures in total biological bacteria and coliform group of general bean curd, general bean curd began to decay around 72 hours at 4$\circ$C and around 48 hours at 23$\circ$C and around 24 hours at 37$\circ$C and, at that time, total biological bacteria approached 10$^6$/g while coliform group did 10$^6$/g. The result indicates that temperature has a great effect on bacteria counts and decay.

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Acid Blue 92 (Leather Dye) Removal from Wastewater by Adsorption using Biomass Ash and Activated Carbon

  • Purai, Abhiti;Rattan, V.K.
    • Carbon letters
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    • v.11 no.1
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    • pp.1-8
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    • 2010
  • The adsorption of Acid Blue 92 onto three low cost and ecofriendly biosorbents viz., cow dung ash, mango stone ash and parthenium leaves ash and commercial activated carbon have discussed in this work. The ash of all the mentioned bio-wastes was prepared in the muffle furnace at $500^{\circ}C$ and all the adsorbents were stored in an air thermostat. Experiments at total dye concentrations of 10~100 mg/L were carried out with a synthetic effluent prepared in the laboratory. The parameters such as pH and dye concentration were varied. Equilibrium adsorption data followed both Langmuir and Freundlich isotherms. The results indicate that cow dung ash, mango stone ash and parthenium leaves ash could be employed as low-cost alternatives to commercial activated carbon in wastewater treatment for the removal of dye.

An Experimental Study on the Properties of Concrete using High Volume of Coal Ash

  • Kim, Moo Han;Choi, Se Jin
    • Architectural research
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    • v.4 no.1
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    • pp.39-44
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    • 2002
  • Recently, the coal-ash production has been increased by increase of consumption of electric power. So it is important to secure a reclaimed land from pollution and develop practical application of coal ash. This is an experimental study to compare and analyze the properties of concrete using high volume of coal ash (including fly ash and bottom ash) as a part of fine aggregate. For this purpose, the mix proportions of concrete according to replacement ratio of coal ash (10, 20, 35, 50%) were selected. And then air content, slump, setting time, bleeding content, chloride content, compressive strength and carbonation test were performed. According to test results, it was found that the bleeding content of concrete using the coal ash decreased according to increase of replacement ratio. And the chloride content of concrete using the bottom ash as a part of fine aggregate increased as the replacement ratio of bottom ash increased, but it is satisfied with the total chloride content of concrete recommended by KCI - $0.3kg/m^3$ below. Also, the compressive strength of concrete using the bottom ash was similar to that of plain concrete(BA 0) after 28days of curing and the carbonation depth of concrete increased as the replacement ratio increased. However, the carbonation depth of concrete using the fly ash decreased as the replacement ratio of fly ash increased.

Characteristics of phosphorus leaching from sewage sludge ash by acid and alkali (산과 알카리에 의한 슬러지 소각재의 인 침출 특성)

  • Battsooj, Munkhjargal;Lee, Minsu;Kim, Dong-Jin
    • Journal of Korean Society of Water and Wastewater
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    • v.30 no.5
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    • pp.571-577
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    • 2016
  • Phosphorus is an essential and irreplaceable element for all living organisms and its resource is limited. Significant amount of used phosphorus is collected in sewage treatment plant as sludge. Sludge ash after incineration contains about 10% of phosphorus in dry mass basis, which is comparable to phosphate rocks, and it is an important source of phosphorus recovery. Acid and alkali were used to leach phosphorus from sludge ash and compared for their leaching kinetics and performance. Phosphorus leaching by NaOH was fast and 0.2 N and 2 N NaOH leached 49% and 56% of the total phosphorus in the sludge ash at the L/S ratio of 100. Phosphorus leaching by sulphuric acid and hydrochloric were very fast and most of the phosphorus was leached in 5 minutes. In case of sulphuric acid 95% of the total phosphorus in the sludge ash was leached by 0.2 N at the L/S ratio of 100 and 93% was leached by 1 N at the L/S ratio of 10. 1 N hydrochloric acid leached 99% of the total phosphorus at the L/S ratio of 10. The results showed acids were more effective than alkali for phosphorus leaching from sludge ash and hydrochloric acid leached more phosphorus than sulphuric acid.

An Experimental Study on Thermal Property of Porous Concrete Containing Bottom Ash (바텀애시를 활용하는 다공성 콘크리트의 열전도 특성에 관한 실험 연구)

  • Jeong, Seung-Tae;Kim, Bum-Soo;Park, Ji-Hun;Yang, In-Hwan
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.9 no.4
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    • pp.625-632
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    • 2021
  • In this paper, the applicability of bottom ash to insulation concrete was investigated to increase the utilization of bottom ash. Bottom ash was used as the aggregates in porous concrete and extensive experiments were conducted to investigate the characteristics of porous concrete using two types of bottom ash aggregates. The water-binder ratios of 0.25 and 0.35 were chosen and concrete specimens was produced with the compaction of 0.5, 1.5, and 3.0MPa to analyze the material properties at different compaction conditions. After concrete specimens were cured for 28 days at water tanks, unit weight, total void ratio, and thermal conductivity were measured. Based on the measured experimental results, the relationships between the unit weight, total void ratio, and thermal conductivity of porous concrete containing bottom ash was presented.

The Analysis of Slope Stability on Clay-Fly Ash Mixtures Embankment (점토-Fly Ash 혼합물로 된 제체의 사면안정 해석(지반공학))

  • 권무남;정성욱;김현기
    • Proceedings of the Korean Society of Agricultural Engineers Conference
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    • 2000.10a
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    • pp.477-483
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    • 2000
  • Fly ash is the unburned residue resulting from the combustion of coal in utility and industrial boilers such as thermal power plants. Annually about 5 million tons of fly ash is being produced in korea. Less than 25 percent of total volume of fly ash is currently being used effectively for some ways. In the future, the volume of fly ash discharge from thermal power stations will be increasing more and more, and the development of the utilization of high volume fly ash is required. Fly ash has a lower compacted density and specific gravity than coarse grained natural aggregates but equivalent strength properties indicating that the fly ash could be used as a structural fill materials. So, clay-fly ash mixtures can be used as a fill material in the construction of embankments. Laboratory tests have been carried out to determine the physical, chemical, and geotechnical characteristics of the clay and fly ash. The fly ash is mixed with the clay in different proportions and the geotechnical characteristics of the mixtures have been studied also. In this study describes the results of the experimental study. The implications of the use of clay and clay-fly ash mixtures on the stability of embankments are discussed.

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