• 한국치위생학회지
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• 제12권3호
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• pp.533-541
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• 2012

Objectives : The purpose of this study was to evaluate the effects of tooth bleaching agent contained 35% hydrogen peroxide on the color, microhardness and surface roughness of tooth-colored restorative materials. Methods : Four types of tooth-colored restorative materials, including a composite resin(Filtek Z350 ; Z350), a flowable composite resin(Filtek P60 : P60), a compomer(Dyract$^{(R)}$ AP ; DY), and a glass-ionomer cement(KetacTM Molar Easymix ; KM) were used in the study. The specimens($8mm{\times}5mm$) were made by using a customized acrylic mold. Each material was divided into two groups equally(n=40) : experimental group(35% HP) and control group(distilled water). 35% HP group was treated 30 mim/5 days for 15 days. Each 30 minute treatment session consisted of two 15 minute cycles of gel application with 20 second light exposure. The authors measured the color, microhardness, and roughness of the specimens before and after bleaching. The data were analyzed with ANOVA and T-test. Results : 35% HP group showed an apparent color change(${\Delta}E^*$) than control group. In particular, DY and KM showed a noticeable color change and statistically significant differences(p<0.05). 35% HP group showed a reduction in microhardness. Z350 and P60 does not have a statistically significant difference(p>0.05), DY and KM showed a statistically significant difference(p<0.05). Percentage microhardness loss(PML) of control group was 0.6 to 5.5% in the group, 35% HP group was 6.6 to 34.6%. Roughness was increased in 35% HP group after bleaching. Especially DY and KM were significantly increased(p<0.05). Conclusions : Bleaching agents may affect the surface of existing restorations; therefore, they should not be used indiscriminately when tooth-colored restorations are present.

• 대한소아치과학회지
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• 제33권3호
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• pp.469-481
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• 2006

법랑질 침식의 병인 중에서 식이습관은 많은 관심을 받아왔고 특히 산성음료의 음용이 많은 주의를 끌어왔다. 산성음료의 급속한 소비량 증가는 치아뿐만 아니라 치아색 수복재료의 표면에도 많은 영향을 미칠 것으로 생각된다. 따라서 본 연구는 어린이들이 비교적 일상적으로 접하는 산성음료 중 가장 보편화된 3종을 선택하여 치아색 수복재료의 노출시간에 따른 표면의 변화를 조사할 목적으로 시행되었다. Resin-modified glass-ionomer, polyacid-modified composite resin, composite resin을 0.9% NaCl, 콜라, 오렌지 쥬스, 스포츠 음료의 각 4개 군으로 나누어 저장하였다. 저장 전과 저장 후 1일, 1-,2-,3-,4-주에 표면강도 및 표면조도를 측정하였고 다음과 같은 결론을 얻었다. 1. 산성음료에 저장했을 경우 composite resin을 제외한 치아색 수복재들은 통계학적으로 유의한 표면강도와 표면조도의 변화를 보였다(p<0.05). 2. 표면강도 및 표면조도의 변화는 resin-modified glass-ionomer, polyacid-modified composite resin composite resin 순으로 크게 나타났다. 3. 콜라나 오렌지 쥬스보다 스포츠 음료에서 표면변화는 더 크게 나타났다. 4. 산성음료에 저장한 군의 SEM 촬영에서 resin-modified glass-ionomer, polyacid-modified composite resin의 경우 충전제의 상실이 관찰되었으며 특히 resin-modified glass-ionomer의 경우 심한 균열이 관찰되었다.

• 한국치위생학회지
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• 제13권2호
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• pp.351-360
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• 2013

Objectives : The purpose of this study was to evaluate the effects of tooth bleaching agent contained 15% carbamide peroxide on the color, microhardness and surface roughness of tooth-colored restorative materials by using pH cycling model. Methods : Four types of tooth-colored restorative materials, including a composite resin(Filtek Z350 ; Z350), a flowable composite resin(Filtek P60 : P60), a compomer(Dyract$^{(R)}$ AP ; DY), and a glass-ionomer cement(KetacTM Molar Easymix ; KM). were used in the study. Eighty-eight specimens of each material were fabricated, randomly divided into two groups(n=44): experimental group(15% carbamide peroxide) and control group(distilled water). These groups were then divided into four subgroups(n=11). All groups were bleached 4 hours per day for 14 days using pH cycling model. The authors measured the color, microhardness, and roughness of the specimens before and after bleaching. The data were analyzed with ANOVA and T-test. Results : Z350 and P60 showed a slight color change(${\Delta}E^*$), whereas DY and KM showed significantly color change(p<0.05). Among them, the greatest color change was observed in DY. Percentage microhardness loss(PML) of the distilled water group was 1.8 to 5.1%, and 15% peroxide peroxide group was 5.0 to 25.2%. Microhardness of DY and KM showed a statistically significant decrease(p<0.05). Roughness was increased in all groups after bleaching. Z350 and P60 does not have a significant difference(p>0.05), however DY and KM significantly increased more than the 0.2 ${\mu}m$(p<0.05). Conclusions : The effects of bleaching on restorative materials were material dependent. It is necessary to consider the type of the material before starting the treatment.

• 치위생과학회지
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• 제21권3호
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• pp.178-184
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• 2021

Background: As the importance of the esthetic function of teeth increases, the use of esthetic restoration materials and whitening treatment are increasing. The purpose of this study was to investigate the color change of esthetic restoration materials upon using staining and whitening toothpaste. Methods: Light curing (LC) packable composite resin, LC flowable resin, LC glass ionomer (GI), and self-curing GI specimens were colored in coffee or curry for three hours a day for seven days. After that, regular toothpaste, whitening toothpaste containing hydrogen peroxide, and whitening toothpaste containing activated charcoal were applied for three minutes three times a day for two weeks. Luminosity (L), chromaticity a (a), and chromaticity b (b) were measured using a spectrophotometer once a week. Results: In the coffee-colored group, the change in L^2*a^2*b² (E²) with time was significant (p=0.004), there was no difference for different toothpaste types (p=0.646), and there was significant difference (p<0.001) for different esthetic restorative materials. The change of E² in the curry-colored group was significant only for different esthetic restorative materials (p<0.001). In the coffee-colored group, the L, a, and b values of the light-curing GI showed greater change than other materials after staining and one week after whitening, turning dark, red, and yellow. In the curry-colored group, L did not differ for different materials and times, and a and b showed the greatest difference in light-curing GI after staining and one and two weeks after whitening. Conclusion: The use of whitening toothpaste for two weeks was not different from the use of general toothpaste in the removal of staining or whitening. Since light-curing GI is the most vulnerable to coloration, it is recommended that coloring by food chromogen should be explained in advance, before using light-curing GI for teeth restoration.

• Restorative Dentistry and Endodontics
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• 제25권3호
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• pp.313-320
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• 2000

The purpose of this study was to evaluate on the interfacial morphology between dentin and restorative materials. In this in vitro study, the cavity wall restorated with 3 different kinds of tooth colored restorative materials [resin-modified Glass Ionomer cement (Fuji II LC), composite resin (Z-100), compomer (Dyract)]. The thirty extracted human molar teeth without caries and/or restorations are used. The experimental teeth were randomly divided into three groups of ten teeth each. In each group, Wedge shaped cavities (width: 3mm, length: 2mm, depth: 1.5mm) were prepared at the cementoenamel junction on buccal and lingual surfaces. The adhesive of composite resin were mixed with rhodamine B. Primer of composite resin, Prime & Bond 2.1 of Dyract and liquid of Fuji II LC were mixed with fluorescein. In group 1, the cavity wall was treatment with dentin conditioner, and then restorated with Fuji II LC. In group 2, the cavity wall was treatment with Prime & Bond 2.1 and then restorated with Dyract. In group 3, the cavity wall was etching with 10% maleic acid, applied with primer and bonding agent and then restorated with Z-100. The interface between dentin and restorative materials was observed by fluoresence imaging with a confocal laser scanning microscope. The results were as follows : 1. In Glass ionomer group, adaptation of resin modified Glass-ionomer restoration against cavity wall is tight, but the crack formed inside of restoration were observed. 2. In Dyract group, the penetration of resin tag is shorter and the width of hybrid layer is narrower than composite resin group. 3. In Z-100 group, primer penetrated deeply through dentinal tubule. Also bonding agent was penetrated along the primer, but the penetration length is shorter than primer part, and in 3-D image, the resin tag is conical shape and lateral branch is observed.

• 대한치과보존학회:학술대회논문집
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• 대한치과보존학회 2001년도 추계학술대회(제116회) 및 13회 Workshop 제3회 한ㆍ일 치과보존학회 공동학술대회 초록집
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• pp.594-594
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• 2001

Increased demand for esthetic restorations has promoted a growing interest in tooth-colored restorations even in the posterior regions. Preparation for specific types of indirect inlay and onlays may vary because of differences in fabrication steps for each commercial system and variations in the physical properties of the restorative materials. Preparations for indirect inlay/onlay basically are meant to provide adequate thickness for restorative material and at the same time a passive insertion pattern with rounded internal angles and well defined margins after deciding what type of restoration is indicated.(omitted)

• 대한치과의사협회지
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• 제51권1호
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• pp.12-17
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• 2013

Curing methods for denial resin-based materials are limited because of the need to polymerize quickly in the oral cavity at an ambient temperature. At present, most dental restorative composites use a camphorquinone-amine complex initiation, visible light-cure, one-component systems. Clinically, it is important to try to optimize the degree of conversion of res in composites using proper manipulation and adequate light-curing techniques to ensure the best outcome.

• 대한치과보존학회:학술대회논문집
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• 대한치과보존학회 2001년도 추계학술대회(제116회) 및 13회 Workshop 제3회 한ㆍ일 치과보존학회 공동학술대회 초록집
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• pp.579-579
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• 2001

One of the most important factors for the clinical success of adhesive posterior restorations is marginal adaptation. This property is very closely related to mechanical properties and to the shrinkage behavior of composite materials. Most of modem composite materials are light-cured. This is why the first part of this lecture will be confined to our recent research on light curing, such as plasma polymerization, LED polymerization and the power of modem halogen lamps. In the second part of the lecture the shrinkage properties such as dimensional shrinkage and shrinkage forces of different light curing materials and during different curing procedures will be discussed. Finally, in the third part of the lecture, marginal adaptation before and after loading in different cavity classes and by using different restorative techniques and curing procedures will be presented. Data will also be given on wear resistance, abrasiveness against opposing cusps and postcuring of composite materials.(omitted)

• Restorative Dentistry and Endodontics
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• 제17권1호
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• pp.126-133
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• 1992

Tooth colored resin restorative materials are widely used in anterior teeth restorations. The color instability of resin was the main cause of failure in resin restorations. The purpose of this study was to investigate color stability and microhardness of serval visible light curing resins. Colorimetric measurements(Tokyo Denshoku Co., Japan) and microhardness tests(Matusuzawa, MXT 70, Japan) were made on six composite resins before and after controlled immersion treatments. The six composite resins were BIS - FILM(BISCO, USA), Durafill(Kulzer, Germany), Helioprogess(VIVADENT, Germany), Palfique(TOKUYAMA SODA, Japan), Silux(3M, USA), Photoclearfil(KURARAY, Japen). Six light curing resins showed significant color change after 2 weeks. Palfique exhibited the hightest $dE^*$ values and Helio progress presented the lowest $dE^*$ values. Photoclearfil showed the highest microhardness value. Durafill and Helio progress showed lower microhardness values. Microhardness values were decreased after 8 weeks in Bisfil, Palfique light, and Photoclearfil.

• Restorative Dentistry and Endodontics
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• 제25권1호
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• pp.71-77
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• 2000

The color of an esthetic restorative material is controlled primarily by thickness of the material and background color. Although the effects of the two factors on the color coordinates of esthetic dental materials have been reported, the mechanism has not been clarified well enough to explain the effects quantitatively. The purpose of this study was to evaluate the effect of thickness and background color on the color of tooth colored restorative materials quantitatively. One hundred sixty samples were fabricated from two commercial light-cured composite resins and two commercial compomers. The color characteristics and changes in the color coordinates were measured by a tristimulus colorimeter (Model TC-6FX, Tokyo Denshoku Co. Japan) using the CIELAB system. The results were as follows: 1. As thickness increased from 1.0 to 4.0mm, values of $L^*$ $a^*$ $b^*$ changed irregulary for white and dentin color background, but showed no obvious difference in color for black background. 2. The colors of composite resins and compomers were significantly influenced by background color. 3. The color difference was recognized even the same shade name in four representative kinds of composite resins and compomers. 4. As thickness changed, values of color difference for same products and same background color showed constancy, but showed difference for different background color.