• Title/Summary/Keyword: Titanium alloy

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SUPERELASTICITY OF CAST SHAPE MEMORY Ni-Ti ALLOY (주조 형상기억 니켈-티타늄 합금의 초탄성)

  • Choi, Dong-Ik;Choie, Mok-Kyun
    • Journal of the Korean Academy of Esthetic Dentistry
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    • v.3 no.1
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    • pp.32-43
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    • 1995
  • Ni-Ti alloy has excellent corrosion resistance, biocompatibility, shape memory effect and superelasticity, so it has been used widely in biomedical fields. But it has difficulty in casting due to its high melting temperature and oxygen affinity at high temperature. Recently it has been attempted to cast Ni-Ti alloy using new casting machine and investment. The purpose of this study was to examine the superelastic behavior of cast shape memory Ni-Ti alloy and to compare the mechanical properties of the cast shape memory alloy with those of commercial alloys for removable partial denture framework. Ni-Ti alloy(Ni 50.25%, Ti 49.75% : atomic ratio) was cast with dental argon-arc pressure casting machine and Type IV gold alloy, Co-Cr alloy, Ni-Cr alloy, pure titanium were cast as reference. Experimental cast Ni-Ti alloy was treated with heat($500{\pm}2^{\circ}C$) in muffle furnace for 1 hour. Transformation temperature range of cast Ni-Ti alloy was measured with differential scanning calorimetry. The superelastic behavior and mechanical properties of cat Ni-Ti alloy were observed and evaluated by three point bending test, ultimate tensile test, Vickers microhardness test and scanning electron microscope. The results were as follows : 1. Cast Ni-Ti alloy(Ni 50.25%, Ti 49.75% : atomic ratio) was found to have superelastic behavior. 2. Stiffness of cast Ni-Ti alloy was considerably lesser than that of commercial alloys for removable partial denture. 3. Permanent deformation was observed in commercial alloys for removable partial denture framework at three point bending test over proportional limit(1.5mm deflection), but was not nearly observed in cast Ni-Ti alloy. 4. On the mechanical properties of ultimate tensile strength, elongation and Vickers microhardness number, cast Ni-Ti alloy was similiar to Type IV gold alloy, Co-Cr alloy, Ni-Cr alloy and pure titanium. With these results, cast Ni-Ti alloy had superelastic behavior and low stiffness. Therefore, it is suggested that cast Ni-Ti alloy may be applicated to base metal alloy for removable partial denture framework.

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Grindability of Cast Ti-X%Zr(X=10,20,40) Alloys for Dental Applications (치과주조용 Ti-X%Zr(X=10,20,40)합금의 연삭성)

  • Jung, Jong-Hyun;Noh, Hyeong-Rok
    • Journal of Technologic Dentistry
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    • v.33 no.4
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    • pp.263-270
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    • 2011
  • Purpose: The grindability of binary Ti-X%Zr(X=10,20,40) alloys in order to develop a Ti alloy with better machinability than unalloyed titanium has been evaluated. Methods: Experimental Ti-Zr alloys were made in an argon-arc melting furnace. Slabs of experimental alloys were ground using a SiC abrasive wheel on an electric handpiece at circumferential speeds(12000,18000,25000 or 30000rpm) by applying a force(200gr). Grinding rate was evaluated by measuring the amount of metal volume removed after grinding for 1 minute and the volume ratio of metal removed compared to the wheel material lost, which was calculated from the diameter loss (grinding ratio). Experimental datas were compared to those for cp Ti(commercially pure titanium) and Ti-6%Al-4%V alloy were used controls. Results: It was observed that the grindability of Ti-Zr alloys increased with an increase in the Zr concentration. More, they are higher than cp Ti, particularly the Ti-20%Zr alloy exhibited the highest grindability at all circumferential speeds. There was significant difference in the grinding rate and grinding ratio between Ti-20%Zr alloy and cp Ti at any speed(p<0.05). Conclusion: By alloying with Zr, the Ti exhibited better grindability at all circumferential speeds. the Ti-20%Zr alloy has a great potential for use as a dental machining alloy.

Microstructural Analysis of Thermo-Mechanical Processed Ti-6Al-4Fe Alloy (Ti-6Al-4Fe 합금의 가공열처리 미세조직 분석)

  • Choe, Byung Hak;Choi, Won-Youl;Shim, Jong Heon;Park, Chan Hee;Kang, Joo-Hee;Kim, Seung Eon;Hyun, Yong Taek
    • Korean Journal of Materials Research
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    • v.25 no.8
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    • pp.410-416
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    • 2015
  • Microstructural analysis of a (${\alpha}+{\beta}$) Ti alloy was investigated to consider phase transformation in each step of the thermo-mechanical process using by SEM and TEM EDS. The TAF (Ti-6Al-4Fe) alloy was thermo-mechanically treated with solid solution at $880^{\circ}C$, rolling at $880^{\circ}C$ and annealing at $800^{\circ}C$. In the STQ state, the TAF microstructure was composed of a normal hcp ${\alpha}$ and metastable ${\beta}$ phase. In a rolled state, it was composed of fine B2 precipitates in an ${\alpha}$ phase, which had high Fe segregation and a coherent relationship with the ${\beta}$ matrix. Finally, in the annealing state, the fine B2 precipitates had disappeared in the ${\alpha}$ phase and had gone to the boundary of the ${\alpha}$ and ${\beta}$ phase. On the other hand, in a lower rolling temperature of $704^{\circ}C$, the B2 precipitates were more coarse in both the ${\alpha}$ and the boundary of ${\alpha}$ and ${\beta}$ phase. We concluded that microstructural change affects the mechanical properties of formability including rolling defects and cracks.

The Fabrication and Grindability of Diamond Wheel Bonded with Heat Resistance Aluminum Alloy (내열 Al합금 본드 다이아몬드 휠의 제조 및 연삭성)

  • 최성국
    • Journal of Powder Materials
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    • v.2 no.2
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    • pp.142-148
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    • 1995
  • 2219 aluminum alloy bonded diamond wheels containing intermetallic compounds were fabricated by powder metallurgy method. Nickel and titanium were added in aluminum matrix piece. The hot pressing condition was $600^{\circ}C$ and 20 Mpa in the furnace of the electric resistance type. The mechanical properties and grinding tests were carried out to confirm the wheel performance. Aluminum oxide ceramics were chosen for use in the grinding tests. The test proved that the heat resistance 2219 aluminum bonded diamond wheel containing 15 wt% nickel and 15 wt% titanium respectively showed the best performance.

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The Electrochemical Characteristics of Anodized Ti-29Nb-xZr Alloys

  • Lee, Kang;Choe, Han-Choel;Ko, Yeong-Mu
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2009.05a
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    • pp.219-219
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    • 2009
  • In this study, electrochemical impedance characteristics of anodic oxide layer formed on titanium ternary alloy surface have been investigated, Titanium oxide layers were grown on Ti-29Nb-xZr(x=3, 5, 7, 10 and 15 wt%) alloy substrates using phosphoric acid electrolytes.

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Creep Behaviours of Glasses Rim Material Alloy (안경테소재 합금(Ti-6AI-4V)의 크리프 특성)

  • 황경충;윤종호
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2003.10a
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    • pp.248-253
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    • 2003
  • Titanium alloy has widely been used as glasses rim material because it has high specific strength and also is light, harmless to men. But, we have little design data about the creep behaviors of the alloy. Therefore, in this study, an apparatus has been designed and built for conducting creep tests under constant load conditions. A series of creep tests on them have been performed to get the basic design data and life prediction of titanium products and we have gotten the following results. First, the stress exponents decrease as the test temperatures increase. Secondly, the creep activation energy gradually decreases as the stresses become bigger. Thirdly, the constant of Larson-Miller parameters on this alloy is estimated about 13. And last, the fractographs at the creep rupture show both the ductile and the brittle fracture according to the creep conditions.

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Preparation of $TiB_2$ Dispersed Cu Alloy by Spark Plasma Sintering

  • Kim, Kyong-Ju;Lee, Gil-Geun;Park, Ik-Min
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.523-524
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    • 2006
  • The $TiB_2$ dispersion strengthened copper alloy was attracted as thermal and electrical functional material for the high mechanical strength, high thermal stability and good conductivity of $TiB_2$. In the present study, the focus is on the synthesis of $TiB_2$ dispersed copper alloy by spark plasma sintering process using copper oxide and titanium diboride as raw materials. The mechanical, thermal and electrical properties of sintered bodies were discussed with the sintering parameters, and developed microstructure and phase of sintered bodies.

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Ingot Casting with Ferro-Titanium Pretreatment Process using Ti Scrap (타이타늄 스크랩을 활용한 페로 -타이타늄 전처리 공정 적용 모합금 주조)

  • Lee, Cho-Long;Park, Jong-Bum;Kang, Tae-Woong;Min, Tae-Sik;Jeon, Soo-Hyeok;Ro, Yoon-Gyeong
    • Journal of Korea Foundry Society
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    • v.41 no.2
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    • pp.139-143
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    • 2021
  • A type of titanium alloy, ferro-titanium, is the main material used to manufacture steel and stainless steel. Considering economic aspects, ferro-titanium ingots are intended to be manufactured using low-cost titanium scrap, and the best pretreatment process for removing impurities from recycled titanium scrap surfaces was studied here. Instead of ordinary acid or organic solvents, ecofriendly methods were researched and applied, and chip scrap materials were used. A high-quality ferro-titanium ingot was manufactured from titanium scrap after a pretreatment process was applied, and the impurities and properties were analyzed and compared with commercial material standards through a component analysis.

A Study on the High Temperature Strength of Ferritic Stainless Cast Steels (페라이트계 스테인레스 주강의 고온강도에 관한 연구)

  • Ann, Soo-Jung;Kang, Mi-Ri;Seo, Do-Soo;Kim, Yong-Hyun;Lee, Kwang-Hak;Kim, Heung-Shik
    • Journal of Korea Foundry Society
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    • v.18 no.6
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    • pp.563-569
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    • 1998
  • A Study on microstructure and elevated temperature strength of 18Cr-2Mo ferritic stainless steel castings strengthened by alloying small amounts of titanium and carbon, has been conducted. The morphology of titanium carbides showed spherical in shape and their distribution depended on the amount of alloying elements. Maximum density ($7{\times}10^5/cm^2$) of titanium carbides has been formed in the alloy containing 2.0 wt.% titanium and 0.5 wt.% carbon as alloying elements and the size of carbide particles is in the range of 0.5 to $3.0\;{\mu}m$. High temperature tensile and fatigue strength of this alloy were the highest among the alloys tested in this research. The fracture mode of the alloys containing alloying elements less that 2.0 wt.% titanium and 0.5 wt.% carbon showed intercrystalline fracture at room temperature, while the alloys containing higher amounts of alloying elements showed transcrystalline fracture. All of the alloys showed creep or ductile rupture mode at elevated temperature.

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