• 약학회지
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• 제23권1호
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• pp.7-10
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• 1979

A gas chromatographic determination of dienestrol in dienestrol cream has been studied. Dienestrol cream was dissolved in pyridine and silylation was done by using N, O-bis (trimethylsilyl) trifluoroacetamide. The derivative was injected into 3% silicone OV-17 column for chromatographic estimation. The dienestrol peak was found to be well separated from the other components of the cream. The detection limit was obtained to be $5.6{\times}10^{11}$ mol of dienestrol for this method. As there is no need for prior separation procedure, this experiment is extremely simple and less time consuming as compared to the conventional methods for estimation of dienestrol in cream.

• 대한전기학회논문지
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• 제32권11호
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• pp.387-393
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• 1983

This paper descrives the computational algorithm for determination of system characteristic constants using diakoptic method. When the system charateristic contants of large scale power system are calculated by using sensitivity matrix method which requires the inversion of Jacobian matrix, the necessary computing time and memory requirements increase very largely. Diakoptic mothods is benefit to get around these problems, and it is applied to a model system compared with the integrated method to discuss the efficiency of the algorithm.

• Bulletin of the Korean Chemical Society
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• 제16권7호
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• pp.578-582
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• 1995

The resonance ionization mass spectrometry (RIMS) system with angular reflectron type time-of-flight mass spectrometer (AREF-TOFMS) has been developed and characterized. The system is applied for the ultratrace determination of Pb element. The 2-color 3-photon laser ionization scheme is adopted for the study and the mass resolution of the system is determined as T/ΔT=1680. The calibration curve for Pb is obtained in the range of 100 ppb to 0.01 ppb by using standard solutions. The minimal amount of detection for the present RIMS system is determined as less than 100 femtograms (10-13 gram).

• 한국정밀공학회지
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• 제19권5호
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• pp.95-102
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• 2002

The grinding operation is an important machining process for machining of final surface. However, grinding process has inevitable troubles such as loading and glazing for grinding wheel. It is, therefore, an essential research theme to determine the wheel life and the dressing time for efficient grinding. In this study, AE signals (AEavg) generated in the grinding operation were measured and the dressing time was determined from the analysis of the AEavg value. To verify the propriety of the obtained result, the AE signals measured on the grinding and the dressing operation were compared with the grinding force signals and the dressing force which were measured at same time. From the obtained result, it was confirmed that the determination of the wheel life and the dressing tilde by the AE measurement technique proposed in this study can be practically used.

• Smart Structures and Systems
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• 제22권1호
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• pp.41-55
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• 2018

Damping ratio and frequency have influence on dynamic serviceability or instability such as vortex-induced vibration and displacement amplification due to earthquake and critical flutter velocity, and it is thus important to make determination of damping ratio and frequency accurate. As bridges are getting longer, small scale model test considering similitude law must be conducted to evaluate damping ratio and frequency. Analysis conditions modified by similitude law are applied to experimental test considering different scale ratios. Generally, Nyquist frequency condition based on natural frequency modified by similitude law has been used to determine sampling rate for different scale ratios, and total time length has been determined by users arbitrarily or by considering similitude law with respect to time for different scale ratios. However, Nyquist frequency condition is not suitable for multimode system with noisy signals. In addition, there is no specified criteria for determination of total time length. Those analysis conditions severely affect accuracy of damping ratio. The focus of this study is made on the determination of minimum analysis conditions for different scale ratios. Influence of signal to noise ratio is studied according to the level of noise level. Free initial value problem is proposed to resolve the condition that is difficult to know original initial value for free vibration. Ambient and free vibration tests were used to analyze the dynamic properties of a system using data collected from tests with a two degree-of-freedom section model and performed on full bridge 3D models of cable stayed bridges. The free decay is estimated with the stochastic subspace identification method that uses displacement data to measure damping ratios under noisy conditions, and the iterative least squares method that adopts low pass filtering and fourth order central differencing. Reasonable results were yielded in numerical and experimental tests.

• Journal of Radiation Protection and Research
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• 제29권2호
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• pp.91-96
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• 2004

원자력시설의 사고로 인한 방사성물질의 환경 누출후 주민의 이주를 위한 유도개입주위 산정의 실용적 방법론을 지표면 선량율에 근거하여 고안하였다. 이주를 요하는 기간에 따라 잠정 이주와 영주이주로 구분하여 환경특성 변수 값에 따른 유도개입준위의 영향을 고찰하였다. 이주를 위한 유도개입준위는 방사성물질의 지표 침적후 핵종의 유효 제거 반감기, 측정 지연시간 피폭자의 거주특성 등에 따라 뚜렷이 다르게 나타났다. 특히 지표면 선량율이 지수함수 형태가 아닌 멱함수 형태의 감소를 가정하는 경우 측정 지연시간은 유도개입준위 설정에 있어 중요한 요소로 작용한다는 것을 알 수 있다. 핵종의 유효 제거반감기가 길수록 측정 지연시간이 늦을수록 그리고 피폭자가 오염원에 노출되는 시간이 길수록 유도개입준위는 보다 낮은 값을 나타냈다.

• 한국항공우주학회지
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• 제44권9호
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• pp.781-788
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• 2016

본 논문에서는 실시간 On-board 궤도 결정 성능을 향상시키기 위해 고정밀 우주 섭동 모델을 구현하였고, 구현된 우주 섭동모델을 GNSS 수신기의 궤도 결정 로직에 적용하여 그 결과를 분석하였다. 궤도 결정 로직은 확장 칼만 필터(Extended Kalman Filter)로 구현되었고, 의사거리로 계산한 궤도(Standard Position Service)를 관측정보로 이용하였다. 궤도 결정 로직 성능 검증은 GPS 인공위성의 신호를 모사하는 GNSS 시뮬레이터를 이용하여 수행하였다. 고정밀 섭동모델의 궤도 결정 성능을 $J_2$ 항만 고려한 섭동모델의 궤도 결정 성능과 비교하여 분석한 결과, GPS 항행해의 위치 정밀도는 43.61 m($3{\sigma}$)에서 23.86 m($3{\sigma}$)로 46 % 개선되었으며 속도 정밀도는 0.159 m/s($3{\sigma}$)에서 0.044 m/s($3{\sigma}$)로 72 % 개선되어 정밀도가 향상된 것을 확인할 수 있었다.

• 한국우주과학회:학술대회논문집(한국우주과학회보)
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• 한국우주과학회 2002년도 한국우주과학회보 제11권2호
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• pp.32.2-32
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• 2002

• 대한기계학회논문집
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• 제6권4호
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• pp.315-322
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• 1982

The slab analogy method was introduced in the 1920's for the first time as a new experimental stress analysis method. Notwithstanding its theoretical propriety, this method has not been recognized as efficient one because of its difficulty in practical measurement of the slab curvature. In this paper, aiming at experimental determination of two-dimensional stress intensity factors(S. I. F) of arbitrarily shaped cracks which had been regarded as almost impossible by conventional method, the slab analogy was reevaluated. Measuring of slab curvature was replaced by three simple measuring factors to overcome vital slab-analogy's shortcoming by joint use of the shadow-moire method. A determination formula was also derived from the theory of fracture mechanics. By this newly exploited method, it was found that the slab analogy still has its great advantage in determination of S.I.F. of arbitrarily shaped cracks with considerable accuracy compared with existent experimental methods.

• 대한의용생체공학회:의공학회지
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• 제22권3호
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• pp.269-273
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• 2001

Proper determination of pacing threshold is important for patient safety and pacemaker longevity. In general, cardiac muscle contractions caused by pacing pulses are verified by observing the morphology of surface ECG displayed on a monitor. In this study, a method of automatic pacing threshold determination based on morphological difference between intrinsic and paced ECGs was developed. First, characteristics of intrinsic ECG and paced ECG were analyzed in time and frequency domain and a proper discrimination parameter was extracted. Then, the automatic capture verification method based on the parameter was developed and applied to 23 pacemaker patients. The selected parameter was the area of ventricular depolarization wave during 80ms after pacing stimulus. It was found that the method was reliable and effective in identifying paced ECG and, thereby, determing a proper pacing threshold.