• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2009.05a
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• pp.190-190
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• 2009

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1999.03b
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• pp.153.2-158
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• 1999

A study has been made to investigate how the fomability of Ti-10V-2Fe-3Al alloy is related to the initial microstructure and process variables such as temperature and strain rate. It has been found that the deformation resistance at high temperature is increased with the increase in the thickness of grain boundary a (GB)a and/or acicular a phase and however the effect of a morphology on the hot formability is considered insignificant due to the breakage of GB a and/or acicular a into several equiaxed a particles

• Transactions of Materials Processing
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• v.12 no.4
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• pp.370-375
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• 2003

Determination of the interface heat transfer coefficient was investigated in non-isothermal bulk forming of glass-coated Ti-6Al-4V. FE analysis and experiments were conducted. Equipment consisting of AISI Hl3 die was instrumented with thermocouples located at sub-surface of the bottom die. Die temperature changes were investigated in related to the process variables such as reduction, lubricant and initial die temperature. The calibration approach based on heat conduction and FE analysis using an inverse algorithm were used to evaluate the interface heat transfer between graphite-lubricated die and glass-coated workpiece. The coefficients determined were affected mainly by the contact pressure. The validation of the coefficients was made by the comparison between experimental data and FE analysis results.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2008.05a
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• pp.528-530
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• 2008

The effect of consolidation temperature on the microstructure, density and mechanical properties (especially, wear property) of $Al_{92.5}-Fe_{2.5}-Cr_{2.5}-Ti_{2.5}$ alloy fabricated by gas atomization and magnetic pulsed compaction was investigated. All consolidated alloys consisted of homogeneously distributed fine-grained fcc-Al matrix and intermetallic compounds. Relative higher mechanical properties in the MPCed specimen were attributed to the retention of the nanostructure in consolidated bulk without cracks. The as consolidated bulk by magnetic pulsed compaction showed the enhanced wear properties than that of a general consolidation process. In addition, the wear mechanism and fracture mode of MPCed bulk was discussed.

• Journal of Welding and Joining
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• v.15 no.5
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• pp.104-114
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• 1997

The microstructure and bond strength were investigated on the SiC/SiC and SiC/mild steel joints brazed by Ag-5at%Ti alloy. Ag-5at%Ti-2at%Fe and -5at%Fe brazing alloys were also used to see the effects of Fe addition on the bond strength of SiC/SiC brazed joints. Brazing temperature and brazing gap were selected and examined as brazing variables. The microstructure of SiC/SiC brazed joints was affected by Fe addition to the Ag-5at%Ti alloy, but the bond strength was not. Increasing brazing temperature also changed the microstructure of $Ti_5Si_3$ reaction layer and brazing alloy matrix of the SiC/SiC and SiC/mild steel joints, but not the bond strength. Brazing gap had a great effects on the bond strength. Decreasing brazing gap from 0.2 mm to 0.1 mm in SiC/SiC brazing increased the bond strength from 187 MPa to 263 MPa and, in SiC/mild steel brazing, from 189 MPa to 212 MPa. It was concluded that the most important parameter on the bond strength in SiC/SiC and SiC/mild steel brazing was the relative ratio between brazing gap and specimen size.

• Journal of Magnetics
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• v.6 no.2
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• pp.57-60
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• 2001

Mechanically alloyed $TbCu_7 -type \;Sm_{12.5}Fe_{87.5-x}Ti_x$(x=0, 2.5, 5, 7.5),and their nitrides have been studied systematically by X-ray diffraction, A.C. initial susceptibility, and pulsed magnetization measurement. In this series, the volume expansion by nitriding is 5.6%~7.3%, and the increment of the Curie temperature is in the range of 21$0^{\circ}C$~35$0^{\circ}C$. With increasing Ti content, the remanence decreases linearly due to the substitution of non-magnetic Ti, and the coercivity decreases rapidly from 34.6 kA/cm (43.5 kOe) for $\chi$=0 to 14.3 kA/cm (18 kOe) for $\chi$=7.5. In the $Sm_{12.5}Fe_{87.5-x}Ti_xN_y$ series, the best magnetic properties were obtained from .7Ti7Ny series, the best magnetic properties were obtained from $Sm_{12.5}Fe_{87.5}N_y$($\chi$=0) with $_iH_c$=34.6 kA/cm (43.5 kOe), $B_r=0.75 \;T, \;and (BH)_{max}=113.8 kJ/m^3$(10.9 MGOe).

• Electronic Materials Letters
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• v.14 no.6
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• pp.725-732
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• 2018

The thermoelectric and transport properties of Ti-doped FeVSb half-Heusler alloys were studied in this study. $FeV_{1-x}Ti_xSb$ (0.1 < x < 0.5) half-Heusler alloys were synthesized by mechanical alloying process and subsequent vacuum hot pressing. After vacuum hot pressing, a near singe phase with a small fraction of second phase was obtained in this experiment. Investigation of microstructure revealed that both grain and particle sizes were decreased on doping which would influence on thermal conductivity. No foreign elements pick up from the vial was seen during milling process. Thermoelectric properties were investigated as a function of temperature and doping level. The absolute value of Seebeck coefficient showed transition from negative to positive with increasing doping concentrations ($x{\geq}0.3$). Electrical conductivity, Seebeck coefficient and power factor increased with the increasing amount of Ti contents. The lattice thermal conductivity decreased considerably, possibly due to the mass disorder and grain boundary scattering. All of these turned out to increase in power factor significantly. As a result, the thermoelectric figure of merit increased comprehensively with Ti doping for this experiment, resulting in maximum thermoelectric figure of merit for $FeV_{0.7}Ti_{0.3}Sb$ at 658 K.

• Journal of the Korean institute of surface engineering
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• v.29 no.5
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• pp.393-398
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• 1996

Soft magnetic properties and microstructural evolution of FeTaNC films were investigated, and compared with FeTaN and FeTaC films. Effects of substrate species (glass vs. $CaTiO_3$) on the magnetic properties were also investigated. Co-addition of N and C significantly enhance the grain refinments and magnetism, compared with N or C addition only. Good soft magnetic characteristics of coercivity of 0.17 Oe, permeability of 4000 (5MHz), and saturation flux density of 17 kG can be obtained in the FeTaNC in the relatively wide process windows. While these values appears to be similar to those of FeTaN on glass substrate, most distinctive difference between FeTaNC and FeTaN(or C) is in the effects of substrate. Whereas FeTaNC films show good magnetic characteristics for both glass and $CaTiO_3$ substrates, FeTaN(or C) films show significant degradation on the $CaTiO_3$ substrate.

• Journal of the Korean Society for Heat Treatment
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• v.7 no.4
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• pp.288-297
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• 1994

In this study, lattice parameter, binding energy and microstructures of TiC layer according to the addition of Fe, Cr were investigated in the reactive deposition coating. From the results, the lattice parameters of the TiC layers by using ferro-titanium as a precursor were 4.329~4.339A but the lattice parameters of the TiC layers formed by ferro-titanium and ferro-chromium decreased to 4.316~4.330A. The hardness of the former's was HV(100g) 3,000~3,400kg/mm and the hardness of the latter's was HV (100g) 3,800~3,900. But, regardless of Cr and Fe, the binding energy of TiC layers were 454.75 eV for $Ti2p_{3/2}$ and were 281.85 eV for Cls. Meanwhile, the TiC layers were densified by addition of Fe, Cr and internal defects were reduced Therefore. it can be concluded that the remarkable hardness increment was obtained by the improvement of microstructures of TiC rather than the increase of bond strength or Peierls stress.

• Journal of the Korean Ceramic Society
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• v.28 no.11
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• pp.897-907
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• 1991

This study was conducted to research the formation and the color development of CoO-ZnO-Fe2O3-TiO2-SnO2 system for the purpose of synthesizing the spinel pigments which are stable at high temperature. After preparing CoO-ZnO-Fe2O3, in which CoO causes the color, as a basic composition, $\chi$CoO.(1-$\chi$)ZnO.Fe2O3 system, $\chi$CoO.(1-$\chi$)ZnO.TiO2 system and $\chi$CoO.(1-$\chi$)ZnO.SnO2 system were prepared with $\chi$=0, 0.2, 0.5, 0.7, 1.0 mole ratio respectively. The manufacturing was carried out at 128$0^{\circ}C$ for 90 minutes. These specimens were analyzed by the reflectance measurement and the X-ray diffraction analysis and the results were summarized as follows: 1. All of the specimens formed the spinel structure and were colored with stable yellow or blue. 2. As the content of CoO and Fe2O3 in the specimens being increased, the reflectance of each specimen was measured becoming lower and the colors were changed from yellow to greyish blue and from blue to dark blue. 3. As the substituting amount of Co2+ ion for Zn2+ ion in $\chi$CoO-ZnO-TiO2-SnO2 system being increased, the colors were changed from blue to greyish blue. The colors were changed from yellow to grayish green owing to the tetrahedral Co2+ ions being increased, the octahedral Co2+ ions being decreased with increasing the amount of Sn4+ ions. 4. CoO-ZnO-Fe2O3-TiO2-SnO2 system, in which Zn2+ was substituted with Co2+ and Fe3+ was substituted with Ti4+ and Sn4+, easily formed the spinel structure without regard to the amount of substitution or the ion owing to the selectivity of the coordination number: 4 of Zn2+, 4 of Co2+, 6 of Fe3+ or 6 of Ti4+ and Sn4+.