• Title/Summary/Keyword: ThreeStep Process

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Facile Regiocontrolled Three-Step Synthesis of Poly-Substituted Furans, Pyrroles, and Thiophenes: Consecutive Michael Addition of Methyl Cyanoacetate to α,β-Enone, CuI-Mediated Aerobic Oxidation, and Acid-Catalyzed Paal-Knorr Synthesis

  • Kim, Se-Hee;Lim, Jin-Woo;Lim, Cheol-Hee;Kim, Jae-Nyoung
    • Bulletin of the Korean Chemical Society
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    • v.33 no.2
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    • pp.620-624
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    • 2012
  • An efficient synthesis of poly-substituted furans, pyrroles, and thiophenes was carried out in a regiocontrolled manner via a three-step process; (i) conjugate addition of methyl cyanoacetate derivatives to ${\alpha}$,${\beta}$-enones, (ii) CuI-mediated aerobic oxidation, and (iii) Paal-Knorr type synthesis of five-membered heterocycles.

$360^{\circ}$ Cold Bending of Ti-6Al-4V Large-Diameter Seamless Tube (대 직경 이음매 없는 Ti-6Al-4V 튜브의 $360^{\circ}$ 냉간 굽힘)

  • 허선무;박종승
    • Journal of the Korea Institute of Military Science and Technology
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    • v.3 no.1
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    • pp.176-182
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    • 2000
  • $360^{\circ}$ bending of Ti-6Al-4V large-diameter seamless tube(62.37 mm $OD {\times} 4.40mm$ wall thickness) has been achieved at room temperature without heating. The bending process comprised two steps : the first step is $360^{\circ}$ bending by an uniquely designed rotary bender allowing spring back, which is subsequently eliminated by the second or finishing step which comprised repeated bending processes by powered three roll bender, In odor to prevent collapse of tube during bending, Cerro $Tru^{TM}$(Trade name of a non-ferrous low melting point alloy)has been employed as a filler metal. The resultant ovality(out of roundness) obtained was 1.28%, as compared with 6~8% without applying Cerro $Tru^{TM}$.

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The Calculation of Three-Dimensional Viscous Flow in a Transonic, Multi-Stage Axial Compressor (다단축류압축기내의 천음속 점성유동에 대한 삼차원 수치해석)

  • Yi H. W.;Kim K. Y.
    • 한국전산유체공학회:학술대회논문집
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    • 1998.05a
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    • pp.181-189
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    • 1998
  • A numerical study based on the three-dimensional Reynolds averaged Navier-Stokes equations is presented to analyze the transonic flowfield through two-stage axial compressor. Explicit four-step Runge-Kutta scheme is used for solution algorithm, and local time step and implicit residual averaging are introduced for enhancing the convergency. Artificial dissipation model is adopted to assure the stability of solution. The solver is coupled with Baldwin-Lomax model to describe turbulence. To avoid calculating the unsteady flow, a mixing process is modeled at a station between rotating and stationary blade rows. Results show a variety of important physical phenomena. Comparison of the flowfields with and without tip clearance shows that the effect is considerable in this flowfield. Comparisons with experimental data carried out to validate the calculational results show reasonable agreements. Some remedies are also suggested to improve the revealed problems.

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A Three Steps Data Reduction Model for Healthcare Systems (헬스케어 시스템을 위한 세단계 데이터 축소 모델)

  • Ali, Rahman;Lee, Sungyoung;Chung, Tae Choong
    • Proceedings of the Korea Information Processing Society Conference
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    • 2013.05a
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    • pp.474-475
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    • 2013
  • In healthcare systems, the accuracy of a classifier for classifying medical diseases depends on a reduced dataset. Key to achieve true classification results is the reduction of data to a set of optimal number of significant features. The initial step towards data reduction is the integration of heterogeneous data sources to a unified reduced dataset which is further reduced by considering the range of values of all the attributes and then finally filtering and dropping out the least significant features from the dataset. This paper proposes a three step data reduction model which plays a vital role in the classification process.

Fabrication of $MgB_2$ Thin Films by rf-sputtering (rf-sputtering을 이용한 $MgB_2$ 박막 제작)

  • 안종록;황윤석;이순걸
    • Progress in Superconductivity
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    • v.4 no.2
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    • pp.153-156
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    • 2003
  • We have studied fabrication of $MgB_2$ thin film on $SrTiO_3$ (001) and r-cut $A1_2$$O_3$ substrates by rf magnetron sputtering method using and $ MgB_2$ single target and two targets of Mg and B, respectively. Based on P -T phase diagram of $MgB_2$ and vapor pressure curves of Mg and B, a three-step process was employed. B layer was deposited at the bottom to enhance the film adhesion to the substrate. Secondly, co-sputtering of Mg and B was done. Finally, Mg was sputtered on top to compensate fur the loss of Mg during annealing. Subsequently, $MgB_2$ films were in-situ annealed in various conditions. The sample fabricated using the three-step process showed $T_{c}$ of 24 K and formation of superconducting $MgB_2$ phase was confirmed by XRD spectra. In case of co-sputtering deposition, $T_{c}$ depended on annealing time and argon pressure. However, those made by single-target sputtering showed non-superconducting behavior or low transition temperature, at best.est.

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A Small-Area Solenoid Inductor Based Digitally Controlled Oscillator

  • Park, Hyung-Gu;Kim, SoYoung;Lee, Kang-Yoon
    • JSTS:Journal of Semiconductor Technology and Science
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    • v.13 no.3
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    • pp.198-206
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    • 2013
  • This paper presents a wide band, fine-resolution digitally controlled oscillator (DCO) with an on-chip 3-D solenoid inductor using the 0.13 ${\mu}m$ digital CMOS process. The on-chip solenoid inductor is vertically constructed by using Metal and Via layers with a horizontal scalability. Compared to a spiral inductor, it has the advantage of occupying a small area and this is due to its 3-D structure. To control the frequency of the DCO, active capacitor and active inductor are tuned digitally. To cover the wide tuning range, a three-step coarse tuning scheme is used. In addition, the DCO gain needs to be calibrated digitally to compensate for gain variations. The DCO with solenoid inductor is fabricated in 0.13 ${\mu}m$ process and the die area of the solenoid inductor is 0.013 $mm^2$. The DCO tuning range is about 54 % at 4.1 GHz, and the power consumption is 6.6 mW from a 1.2 V supply voltage. An effective frequency resolution is 0.14 kHz. The measured phase noise of the DCO output at 5.195 GHz is -110.61 dBc/Hz at 1 MHz offset.

Electrochemical Machining of Tungsten Carbide Microshaft (텅스텐 카바이드 미세축의 전해가공)

  • Lee, Kang-Hee
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.19 no.3
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    • pp.370-375
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    • 2010
  • Tungsten carbide microshaft is used as micro punch, electrode of micro electro discharge machining, and micro tool because of its high hardness and rigidity. In this research, tungsten carbide microshaft was fabricated using electrochemical machining. $H_2SO_4$ solution was used as the electrolyte because it can dissolve tungsten carbide and cobalt simultaneously. Experimentally studied were the effects of electrolyte concentration, machining time, and machining voltage on material removal rate and the shape of the microshaft. To eliminate the effects of bubbles and metal corrosion layer on microshaft shape, the machining was performed below the electrolysis voltage. Three step electrochemical process was suggested to fabricate the straight tungsten carbide microshaft. As a result, a straight tungsten carbide microshaft of $30{\mu}m$ in diameter and $500{\mu}m$ in length was obtained through the proposed three step electrochemical process.

Multi-Level Motion Estimation Algorithm Using Motion Information in Blocks (블록 내의 움직임 정보를 이용한 다단계 움직임 예측 알고리즘)

  • Heak Bong Kwon
    • Journal of Korea Multimedia Society
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    • v.6 no.2
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    • pp.259-266
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    • 2003
  • In this paper, we propose a multi-level block matching algorithm using motion information in blocks. In the proposed algorithm, the block-level is decided by the motion degree in the block before motion searching procedure, and then adequate motion searching performs according to the block-level. This improves computational efficiency by eliminating the unnecessary searching Process in no motion or low motion regions, and brings more accurate estimation results by deepening motion searching Process in high motion regions. Simulation results show that the proposed algorithm brings the lower estimation error about 20% MSE reduction with the fewer blocks pet frame and the operation number was reduced to 56% compared to TSSA and 98% compared to FS -BMA with constant block size.

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Blank Design for the General Shaped Deep Drawing Products by F.E.M (유한요소법을 이용한 임의의 단면 딥드로잉 제품의 소재형상설계)

  • Kim, Sang-Do;Park, Min-Ho;Seo, Dae-Gyo
    • Transactions of Materials Processing
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    • v.4 no.4
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    • pp.302-321
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    • 1995
  • A method of determining an optimum blank shape for the non-circular deep drawing process is investigated. The rigid-plastic finite element method is introduced and the computer program code is developed. The ideal shape of a drawn cup with uniform wall height is assumed and metal flow is traced back-ward step by step to predict an initial blank shape of the ideal cup. For examples of the non-circular deep drawing products, three cases of drawn cup with quadrilateral punch shape are considered and optimum blank shapes for each case are proposed and compared with experimental results.

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Dynamic Adaptive Binarization Method Using Fuzzy Trapezoidal Type and Image Stepwise Segmentation (퍼지의 사다리꼴 타입과 영상 단계적 분할을 이용한 동적 적응적 이진화 방법)

  • Lee, Ho Chang
    • Journal of Korea Multimedia Society
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    • v.25 no.5
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    • pp.670-675
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    • 2022
  • This study proposes an improved binarization method to improve image recognition rate. The research goal is to minimize the information loss that occurs during the binarization process, and to transform the object of the original image that cannot be determined through the transformation process into an image that can be judged. The proposed method uses a stepwise segmentation method of an image and divides blocks using prime numbers. Also, within one block, a trapezoidal type of fuzzy is applied. The fuzzy trapezoid is binarized by dividing the brightness histogram area into three parts according to the degree of membership. As a result of the experiment, information loss was minimized in general images. In addition, it was found that the converted binarized image expressed the object better than the original image in the special image in which the brightness region was tilted to one side.