• 제목/요약/키워드: ThreeStep Process

검색결과 705건 처리시간 0.024초

Facile Regiocontrolled Three-Step Synthesis of Poly-Substituted Furans, Pyrroles, and Thiophenes: Consecutive Michael Addition of Methyl Cyanoacetate to α,β-Enone, CuI-Mediated Aerobic Oxidation, and Acid-Catalyzed Paal-Knorr Synthesis

  • Kim, Se-Hee;Lim, Jin-Woo;Lim, Cheol-Hee;Kim, Jae-Nyoung
    • Bulletin of the Korean Chemical Society
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    • 제33권2호
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    • pp.620-624
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    • 2012
  • An efficient synthesis of poly-substituted furans, pyrroles, and thiophenes was carried out in a regiocontrolled manner via a three-step process; (i) conjugate addition of methyl cyanoacetate derivatives to ${\alpha}$,${\beta}$-enones, (ii) CuI-mediated aerobic oxidation, and (iii) Paal-Knorr type synthesis of five-membered heterocycles.

대 직경 이음매 없는 Ti-6Al-4V 튜브의 $360^{\circ}$ 냉간 굽힘 ($360^{\circ}$ Cold Bending of Ti-6Al-4V Large-Diameter Seamless Tube)

  • 허선무;박종승
    • 한국군사과학기술학회지
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    • 제3권1호
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    • pp.176-182
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    • 2000
  • $360^{\circ}$ bending of Ti-6Al-4V large-diameter seamless tube(62.37 mm $OD {\times} 4.40mm$ wall thickness) has been achieved at room temperature without heating. The bending process comprised two steps : the first step is $360^{\circ}$ bending by an uniquely designed rotary bender allowing spring back, which is subsequently eliminated by the second or finishing step which comprised repeated bending processes by powered three roll bender, In odor to prevent collapse of tube during bending, Cerro $Tru^{TM}$(Trade name of a non-ferrous low melting point alloy)has been employed as a filler metal. The resultant ovality(out of roundness) obtained was 1.28%, as compared with 6~8% without applying Cerro $Tru^{TM}$.

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다단축류압축기내의 천음속 점성유동에 대한 삼차원 수치해석 (The Calculation of Three-Dimensional Viscous Flow in a Transonic, Multi-Stage Axial Compressor)

  • 이형욱;김광용
    • 한국전산유체공학회:학술대회논문집
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    • 한국전산유체공학회 1998년도 춘계 학술대회논문집
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    • pp.181-189
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    • 1998
  • A numerical study based on the three-dimensional Reynolds averaged Navier-Stokes equations is presented to analyze the transonic flowfield through two-stage axial compressor. Explicit four-step Runge-Kutta scheme is used for solution algorithm, and local time step and implicit residual averaging are introduced for enhancing the convergency. Artificial dissipation model is adopted to assure the stability of solution. The solver is coupled with Baldwin-Lomax model to describe turbulence. To avoid calculating the unsteady flow, a mixing process is modeled at a station between rotating and stationary blade rows. Results show a variety of important physical phenomena. Comparison of the flowfields with and without tip clearance shows that the effect is considerable in this flowfield. Comparisons with experimental data carried out to validate the calculational results show reasonable agreements. Some remedies are also suggested to improve the revealed problems.

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헬스케어 시스템을 위한 세단계 데이터 축소 모델 (A Three Steps Data Reduction Model for Healthcare Systems)

  • 라하만알리;이승룡;정태충
    • 한국정보처리학회:학술대회논문집
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    • 한국정보처리학회 2013년도 춘계학술발표대회
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    • pp.474-475
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    • 2013
  • In healthcare systems, the accuracy of a classifier for classifying medical diseases depends on a reduced dataset. Key to achieve true classification results is the reduction of data to a set of optimal number of significant features. The initial step towards data reduction is the integration of heterogeneous data sources to a unified reduced dataset which is further reduced by considering the range of values of all the attributes and then finally filtering and dropping out the least significant features from the dataset. This paper proposes a three step data reduction model which plays a vital role in the classification process.

rf-sputtering을 이용한 $MgB_2$ 박막 제작 (Fabrication of $MgB_2$ Thin Films by rf-sputtering)

  • 안종록;황윤석;이순걸
    • Progress in Superconductivity
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    • 제4권2호
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    • pp.153-156
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    • 2003
  • We have studied fabrication of $MgB_2$ thin film on $SrTiO_3$ (001) and r-cut $A1_2$$O_3$ substrates by rf magnetron sputtering method using and $ MgB_2$ single target and two targets of Mg and B, respectively. Based on P -T phase diagram of $MgB_2$ and vapor pressure curves of Mg and B, a three-step process was employed. B layer was deposited at the bottom to enhance the film adhesion to the substrate. Secondly, co-sputtering of Mg and B was done. Finally, Mg was sputtered on top to compensate fur the loss of Mg during annealing. Subsequently, $MgB_2$ films were in-situ annealed in various conditions. The sample fabricated using the three-step process showed $T_{c}$ of 24 K and formation of superconducting $MgB_2$ phase was confirmed by XRD spectra. In case of co-sputtering deposition, $T_{c}$ depended on annealing time and argon pressure. However, those made by single-target sputtering showed non-superconducting behavior or low transition temperature, at best.est.

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A Small-Area Solenoid Inductor Based Digitally Controlled Oscillator

  • Park, Hyung-Gu;Kim, SoYoung;Lee, Kang-Yoon
    • JSTS:Journal of Semiconductor Technology and Science
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    • 제13권3호
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    • pp.198-206
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    • 2013
  • This paper presents a wide band, fine-resolution digitally controlled oscillator (DCO) with an on-chip 3-D solenoid inductor using the 0.13 ${\mu}m$ digital CMOS process. The on-chip solenoid inductor is vertically constructed by using Metal and Via layers with a horizontal scalability. Compared to a spiral inductor, it has the advantage of occupying a small area and this is due to its 3-D structure. To control the frequency of the DCO, active capacitor and active inductor are tuned digitally. To cover the wide tuning range, a three-step coarse tuning scheme is used. In addition, the DCO gain needs to be calibrated digitally to compensate for gain variations. The DCO with solenoid inductor is fabricated in 0.13 ${\mu}m$ process and the die area of the solenoid inductor is 0.013 $mm^2$. The DCO tuning range is about 54 % at 4.1 GHz, and the power consumption is 6.6 mW from a 1.2 V supply voltage. An effective frequency resolution is 0.14 kHz. The measured phase noise of the DCO output at 5.195 GHz is -110.61 dBc/Hz at 1 MHz offset.

텅스텐 카바이드 미세축의 전해가공 (Electrochemical Machining of Tungsten Carbide Microshaft)

  • 이강희
    • 한국생산제조학회지
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    • 제19권3호
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    • pp.370-375
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    • 2010
  • 본 연구에서는 전해가공을 이용해서 직경이 균일한 텅스텐 카바이드 미세축을 제작하는 실험을 수행하였다. 전해가공을 통해 미세축으로 사용 가능한 형상을 얻기 위한 최적의 가공 조건에 대해 고찰하였다 이 과정에서 미세축의 형상에 영향을 주는 여러 인자들을 적절하게 조절하여 최적의 형상을 얻을 수 있었다. 그리고 가공된 미세축을 이용하여 적절한 조건으로 2차, 3차 가공을 수행하여 초미세축을 가공할 수 있음을 보였다. 그리하여 실험 결과 직경 $30{\mu}m$, 길이 $500{\mu}m$의 텅스텐 카바이드 미세축을 제작하였다.

블록 내의 움직임 정보를 이용한 다단계 움직임 예측 알고리즘 (Multi-Level Motion Estimation Algorithm Using Motion Information in Blocks)

  • Heak Bong Kwon
    • 한국멀티미디어학회논문지
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    • 제6권2호
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    • pp.259-266
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    • 2003
  • 본 논문에서는 블록 내의 움직임 정도에 따라 다단계의 블록 레벨을 설정하고, 각 블록 레벨에 따라 각기 다른 움직임 예측을 수행하는 다단계 움직임 예측 알고리즘을 제안한다. 이는 움직임이 없거나 적은 영역에서의 잉여 탐색 과정을 제거하여 계산적 효율성을 증대하고, 움직임 정도가 큰 영역에 대해서는 움직임 예측 과정을 심화시켜 예측의 정확성을 향상시킨다. 실험결과 프레임 당 적은 수의 블록으로 고정된 크기의 블록을 가진 전역 탐색 블록 정합 알고리즘과 Three-Step 탐색 알고리즘보다 MSE를 20% 정도 감소시켰으며 연산량은 전역 탐색 블록 정합 알고리즘과 비교하여 98%, Three-Step 탐색 알고리즘과 비교하여 56% 정도 절감하는 효과를 얼을 수 있었다.

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유한요소법을 이용한 임의의 단면 딥드로잉 제품의 소재형상설계 (Blank Design for the General Shaped Deep Drawing Products by F.E.M)

  • 김상도;박민호;서대교
    • 소성∙가공
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    • 제4권4호
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    • pp.302-321
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    • 1995
  • A method of determining an optimum blank shape for the non-circular deep drawing process is investigated. The rigid-plastic finite element method is introduced and the computer program code is developed. The ideal shape of a drawn cup with uniform wall height is assumed and metal flow is traced back-ward step by step to predict an initial blank shape of the ideal cup. For examples of the non-circular deep drawing products, three cases of drawn cup with quadrilateral punch shape are considered and optimum blank shapes for each case are proposed and compared with experimental results.

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퍼지의 사다리꼴 타입과 영상 단계적 분할을 이용한 동적 적응적 이진화 방법 (Dynamic Adaptive Binarization Method Using Fuzzy Trapezoidal Type and Image Stepwise Segmentation)

  • 이호창
    • 한국멀티미디어학회논문지
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    • 제25권5호
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    • pp.670-675
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    • 2022
  • This study proposes an improved binarization method to improve image recognition rate. The research goal is to minimize the information loss that occurs during the binarization process, and to transform the object of the original image that cannot be determined through the transformation process into an image that can be judged. The proposed method uses a stepwise segmentation method of an image and divides blocks using prime numbers. Also, within one block, a trapezoidal type of fuzzy is applied. The fuzzy trapezoid is binarized by dividing the brightness histogram area into three parts according to the degree of membership. As a result of the experiment, information loss was minimized in general images. In addition, it was found that the converted binarized image expressed the object better than the original image in the special image in which the brightness region was tilted to one side.