• Restorative Dentistry and Endodontics
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• v.31 no.1
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• pp.58-65
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• 2006

The possibility of applying a hi-axial flexure strength test on composite resin was examined using three point and hi-axial flexure strength tests to measure the strength of the light-cured resin and to compare the relative reliability using the Weibull modulus. The materials used in this study were light-curing restorative materials, $MICRONEW^{TM},\;RENEW^{(R)}$ (Bisco, Schaumburg, USA). The hi-axial flexure strength measurements used the piston-on-3-ball test according to the regulations of the International Organization for Standardization (ISO) 6872 and were divided into 6 groups, where the radius of the specimens were 12mm (radius connecting the 3-balls: 3.75mm), 16 mm(radius connecting the 3-balls: 5mm), and the thickness were 0.5mm, 1mm, 2mn for each radius. The hi-axial flexure strength of the $MICRONEW^{TM}\;and\;RENEW^{(R)}$ were higher than the three point flexure strength and the Weibull modulus value were also higher in all of the bi-axial flexure strength groups, indicating that the hi-axial strength test is relatively less affected by experimental error. In addition, the 2 mm thick specimens had the highest Weibull modulus values in the hi-axial flexure strength test, and the $MICRONEW^{TM}$ group showed no significant statistical difference (p>0.05). Besides the 2mm $MICRONEW^{TM}$ group, each group showed significant statistical differences (p<0.05) according to the thickness of the specimen and the radius connecting the 3-balls. The results indicate that for the 2mm group, the hi-axial flexure strength test is a more reliable testing method than the three point flexure strength test.

• Steel and Composite Structures
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• v.38 no.5
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• pp.599-615
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• 2021

The ultimate strength behaviour of sandwich composite beams with J-hooks and normal weight concrete (SCSSBJNs) are studied through two-point loading tests on ten full-scale SCSSBJNs. The test results show that the SCSSBJN with different parameters under two-point loads exhibits three types of failure modes, i.e., flexure, shear, and combined shear and flexure mode. SCSSBJN failed in different failure modes exhibits different load-deflection behaviours, and the main difference of these three types of behaviours exist in their last working stages. The influences of thickness of steel faceplate, shear span ratio, concrete core strength, and spacing of J-hooks on structural behaviours of SCSSBJN are discussed and analysed. These test results show that the failure mode of SCSSBJN was sensitive to the thickness of steel faceplate, shear span ratio, and concrete core strength. Theoretical models are developed to estimate the cracking, yielding, and ultimate bending resistance of SCSSBJN as well as its transverse cross-sectional shear resistance. The validations of predictions by these theoretical models proved that they are capable of estimating strengths of novel SCSSBJNs.

• Proceedings of the KACD Conference
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• 2003.11a
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• pp.575-575
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• 2003

The majority of studies comparing the mechanical properties of brittle dental restorative materials now include use of the Weibull Modulus (m). This modulus is determined from analysis of the statistical distribution of strength measurements, which can be determined using a variety of methods, including biaxial flexure, 3pt bend and 4pt bend. In comparing materials it is usually implicitly assumed that the modulus (m) is independent of test method although it is recognised to be highly dependent on flaw distributions. However, in some cases flaw distributions can be modified by sample preparation and test method may modify stressing patterns. This study investigated the pattern of strength and m in two light setting materials.

• The Journal of Korean Academy of Prosthodontics
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• v.38 no.5
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• pp.575-582
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• 2000

This investigation was designed to determine whether heat-pressing and/or simulated heat treatments affected the flexure strength and the microstructure of the lithium disilicate glass-ceramic in the IPS Empress 2 system. Four groups of the specimens were prepared as follows: group 1 - as-received material, group 2 - heat-pressed material; group 3 - heat-pressed and simulated initial heat-treated material; group 4 - heat-pressed and the simulated heat-treated material with full firings for a final restoration. The three-point bending test and the scanning elec-tron microscope (SEM) analysis was conducted for the purpose of this study. The flexure strength of group 2 was significantly higher than that of group 1. However, there were no significant differences in strength among group 2, 3, and 4, and between group 1 and 4. The SEM micrographs of the lithium disilicate glass-ceramic showed the closely packed, multi-directionally interlocking microstructure of numerous lithium disilicate crystals protruding from the glass matrix. The crystals of the heat-pressed materials (group 2, 3, and 4) were a little denser and about two times bigger than those of the as-received material (group 1). This change of microstructure is more obviously exhibited particularly between group 1 and 2. However, there was no a marked difference among group 2, 3, and 4 after the heat-pressing procedure. Although there were significant increase of the strength and some changes of the microstructure after the heat-pressing operation, the combination of the heat-pressing and the simulated subsequent heat treatments did not produce the increase of strength of IPS Empress 2 glass-ceramic.

• The Journal of Korean Academy of Prosthodontics
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• v.32 no.1
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• pp.47-76
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• 1994

This study was carried out to evaluate the effect of the crack propagation characteristics and bond stress of ceramo-metal system. In order to characterize the crack propagation, the static crack propagation stored in $37^{\circ}C$ distilled water of two commerical porcelains and the dynamic crack propagation under cyclic flexure load of ceramo-metal system were examined. In order to characterize the bond stress, the shear bond test, the 3-point flexure bond test, and the finite element stress analysis of ceramo-metal system were conducted. The results obtained were as follows : 1. Bulk densities and Young's moduli of opaque porcelains increased with repeated firing. 2. Maximum fracture toughness during 4 firing cycles showed at the group of 4 firing cycles in Ceramco porcelain and 2 firing cycles in Vita porcelain. 3. Shear bond strength and flexure bond strength of Ceramco-Verabond specimen were larger than those of Ceramco-Degudent G specimen (p<0.05). 4. Interfacial stresses under three point flexure bond test were concentrated at the edges of ceramometal system. 5. When a cyclic flexure load was applied, the crack growth rate of porcelain surface of ceramometal specimens was decreased as load cycles increased.

• The Journal of Korean Academy of Prosthodontics
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• v.41 no.1
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• pp.89-98
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• 2003

Titanium requires special ceramic system for veneering. Low fusing dental ceramics with coefficients of thermal expansion matching that of titanium have been developed. The purpose of this study was determine the bond strengths between cast and noncast pure titanium and two commercial titanium porcelains, and to compare the results with a conventional nickel-chromium alloy-ceramic system. The bond strengths were determined using a 3-point flexure test. Three-point flexure specimens $25{\times}3{\times}0.5mm$ were prepared After removal of ${\alpha}-case$ layer, they were veneered with $8{\times}3{\times}1mm$ of ceramics at the center of the bar. Specimens were tested in a universal testing machine. Within the limits of this study, the following conclusions were drawn: 1. The bond strengths between pure titanium and two commercial porcelains exceeded th lower limit of the bonding strength value in ISO 9693(25MPa). 2. There was no significant difference between cast and noncast titanium-porcelain bonds. 3. There was no significant difference between two commercial titanium porcelains. 4. The bond strengths of the titanium-porcelain systems ranged from 73% to 79% of that of the Ni-Cr-conventional porcelain system.

• Korean Journal of Dental Materials
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• v.44 no.1
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• pp.69-77
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• 2017

The aim of this study was to investigate the effects of chitosan powder addition on the strengthening of conventional glass ionomer cement. Two types of chitosan powders with different molecular weight were mixed with conventional glass ionomer cement (GIC): low-molecular weight chitosan (CL; 50~190 kDa), high-molecular weight chitosan (CH; 310~375 kDa). The chitosan powders (CL and CH) were separately added into the GIC liquid (0.25-0.5 wt%) under magnetic stirring, or mixed with the GIC powder by ball-milling for 24 h using zirconia balls. The mixing ratio of prepared cement was 2:1 for powder to liquid. Net setting time of cements was measured by ISO 9917-1. The specimens for the compressive strength (CS; $4{\times}6mm$), diametral tensile strength (DTS; $6{\times}4mm$), three-point flexure (FS; $2{\times}2{\times}25mm$) with flexure modulus (FM) were obtained from cements at 1, 7, and 14 days after storing in distilled water at $(37{\pm}1)^{\circ}C$. All mechanical strength tests were conducted with a cross-head speed of 1 mm/min. Data were statistically analyzed by one-way ANOVA and Tukey HSD post-hoc test. The mechanical properties of conventional glass ionomer cement was significantly enhanced by addition of 0.5 wt% CL to cement liquid (CS, DTS), or by addition of 10 wt% CH (FS) to cement powder. The CL particles incorporated into the set cement were firmly bonded to the GIC matrix (SEM). Within the limitation of this study, the results indicated that chitosan powders can be successfully added to enhance the mechanical properties of conventional GIC.

• Korean Journal of Metals and Materials
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• v.47 no.1
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• pp.50-58
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• 2009

In this study, alumina matrix composites reinforced with carbon nanotubes (CNTs) were fabricated by ultrasonic dispersion, ball milling, mixing, compaction, and sintering processes, and their relative density, electrical resistance, hardness, flexure strength, and fracture toughness were evaluated. 0~3 vol.% of CNTs were relatively homogeneously dispersed in the composites in spite of the existence of some pores. The three-point bending test results indicated that the flexure strength increased with increasing volume fraction of CNTs, and reached the maximum when the CNT fraction was 1.5 vol.%. The fracture toughness increased as the CNT fraction increased, and the fracture toughness of the composite containing 3 vol.% of CNTs was higher by 40% than that of the monolithic alumina. According to observation of the crack propagation path after the indentation fracture test, a new toughening mechanism of grain interface bridging-induced CNT bridging was suggested to explain the improvement of fracture toughness in the alumina matrix composites reinforced with CNTs.

• Steel and Composite Structures
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• v.45 no.2
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• pp.193-204
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• 2022

The need for establishing the contribution of pultruded FRP encasements and additional FRP wraps around these encasements to the shear strength and load-deflection behavior of reinforced concrete beams is the main motivation of the present study. This paper primarily focuses on the effect of additional wrapping around the composite beam on the flexural and shear behavior of the pultruded GFRP (Glass Fiber Reinforced Polymer) beams infilled with reinforced concrete, taking into account different types of failure according to av/H ratio (arch action, shear-tension, shear-compression and pure bending). For this purpose, nine hybrid beams with variable shear span-to-depth ratio (av/H) were tested. Hybrid beams with 500 mm, 1000 mm, and 1500 mm lengths and cross-sections of 150x100 mm and 100x100 mm were tested under three-point and four-point loading. Based on the testing load-displacement relationship, ductility ratio, energy dissipation capacity of the beams were evaluated with comprehensive macro damage analysis on pultruded GFRP profile and GFRP wrapping. The GFRP wraps were established to have a major contribution to the composite beam ductility (90-125%) and strength (40-75%) in all ranges of beam behavior (shear-dominated or dominated by the coupling of shear and flexure). The composite beams with wraps were showns to reach ductilities and strength values of their counterparts with much greater beam depth.

• The Journal of the Korea Contents Association
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• v.20 no.6
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• pp.433-438
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• 2020

The aim of this study was to investigate the mechanical properties of pit and fissure sealant containing cerium oxide nano particles(CNP). Used to mix with pit and fissure sealant (Concise^TM, USA). CNP was added into liquid (0- 4.0 wt%) of pit and fissure sealant. The specimens for the vickers hardness (VHN; 10 × 2 mm), Three-point flexure (FS; 2 × 2 × 25 mm) with flexure modulus (FM) were obtained from cements at 1, 7, and 14 days after storing in (37±1)℃ distilled water. All mechanical strength tests were conducted using machine (Instron 3344) with a cross-head speed of 1 mm/min. Data were statistically analyzed by one-way ANOVA and Duncan posthoc test(p<0.05). Mechanical properties of conventional pit and fissure sealant could be enhanced by addition of CNP. Three-point flexure and modulus of pit and fissure sealant containing CNP were showed a slightly higher value not significantly with the group(p>0.05). The vickers hardness values were increase significantly with incubation time(p<0.05). Results indicated that CNP can be used considered as potential reinforcing agent for increasing mechanical properties for conventional pit and fissure sealant. Therefore, it was suggest that the additional effects of CNP and research on a wide range of substances.