• Title/Summary/Keyword: Thermo-mechanical aging

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Characteristic Accelerated Aging Assessment for Coolant Rubber Hose of Automotive Radiator (자동차 냉각기 고무호스의 가속 노화거동 평가)

  • Kwak, Seung-Bum;Choi, Nak-Sam;Kang, Bong-Sung;Shin, Sei-Moon
    • Proceedings of the Korean Reliability Society Conference
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    • 2006.05a
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    • pp.27-31
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    • 2006
  • Rubber hoses for automobile radiators are apt to degraded and thus failed due to the influence of contacting stresses of air and coolant liquid under thermal and mechanical loadings. The aging behaviors of the skin part of the hoses due to thermo-oxidative and electro-chemical stresses were experimentally analyzed. Through the thermo-oxidative aging test, it was shown that the surface hardness IRHD(International Rubber Hardness Degrees) of the rubber increased with a considerable reduction of failure strain as the aging time and temperature were large. On account of the penetration of coolant liquid into the skin part the weight of rubber specimens influenced by electro-chemical degradation (ECD) test increased, whereas their failure strain and IRHD hardness decreased. The hardness decreased further as the test site on the hose skin approached to the negative pole.

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The effect of thermo-mechanical fatigue on the retentive force and dimensional changes in polyetheretherketone clasps with different thickness and undercut

  • Guleryuz, Aysegul;Korkmaz, Cumhur;Sener, Ayse;Tas, Mehmet Ozan
    • The Journal of Advanced Prosthodontics
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    • v.13 no.5
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    • pp.304-315
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    • 2021
  • PURPOSE. Esthetic expectations have increased the use of polyetheretherketone (PEEK) clasps as alternatives to Cr-Co in removable partial dentures (RPDs). The objective of this study was to evaluate the retentive force and dimensional change of clasps with different thickness and undercut made from PEEK by the thermo-mechanical fatigue. MATERIALS AND METHODS. PEEK clasps (N = 48) with thicknesses of 1 or 1.50 mm and 48 premolar monolithic zirconia crowns with undercuts of 0.25 mm or 0.50 mm were fabricated. Samples are divided into four groups (C1-C4) and were subjected to 7200 thermal aging cycles (at 5 - 55℃). The changes in the retentive force and dimensions of the clasps were measured by micro-stress testing and micro-CT devices from five measurement points (M1 - M5). One-way ANOVA, paired t-test, two-way repeated ANOVA, and post-hoc tests were used to analyze the data (P < .05). RESULTS. The retentive forces of C1, C2, C3, and C4 groups in initial and final test were found to be 4.389-3.388 N, 4.67 - 3.396 N, 5.161 - 4.096 N, 5.459 - 4.141 N, respectively. The effects of retentive force of all PEEK clasps groups were significant decreased. Thermo-mechanical cycles caused significant dimensional changes at points with M2, M4, and M5, and abraded the clasp corners and increased the distance between the ends of the clasp, resulting in reduced retentive forces (P* = .016, P* = .042, P < .001, respectively). CONCLUSION. Thermo-mechanical aging decreases the retentive forces in PEEK clasps. Increasing the thickness and undercut amount of clasps decreases the amount of dimensional change. The values measured after aging are within the clinically acceptable limits.

Degradation Behavior and Micro-Hardness Analysis of a Coolant Rubber Hose for Automotive Radiator (자동차용 냉각기 고무호스의 노화거동과 미소경도분석)

  • Kwak, Seung-Bum;Shin, Sei-Moon;Shin, Wae-Gi;Choi, Nak-Sam
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.31 no.9
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    • pp.915-923
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    • 2007
  • Rubber hoses for automobile radiators are apt to be degraded and thus failed due to the influence of contacting stresses of air and coolant liquid under thermal and mechanical loadings. The aging behaviors of the skin part of the hoses due to thermo-oxidative and electro-chemical stresses were experimentally analyzed. Through the thermo-oxidative aging test, it was shown that the surface hardness IRHD(International Rubber Hardness Degrees) of the rubber increased with a considerable reduction of failure strain as the aging time and temperature increased. On account of the penetration of coolant liquid into the skin part influenced by the electro-chemical degradation(ECD) test the weight of the rubber hose increased, whereas their failure strain and IRHD hardness decreased. The hardness of the hose in the side of the negative pole was the most deteriorated at the test site of the hose skin just below the coolant surface.

Nondestructive Characterization of Degradation of EPDM Rubber for Automotive Radiator Hoses (자동차 냉각기 호스용 EPDM고무의 노화에 대한 비파괴 특성평가)

  • Kwak, Seung-Bum;Choi, Nak-Sam;Choi, Youn-Joung;Shin, Sei-Moon
    • Journal of the Korean Society for Nondestructive Testing
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    • v.25 no.5
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    • pp.368-376
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    • 2005
  • Coolant rubber hoses for automobile radiators can be degraded and thus failed due to the influence of contacting stresses of air and coolant liquid under thermal and mechanical loadings. In this study, for EPDM(ethylene-propylene diene monomer) rubber conventionally used as a radiator hose material the aging behaviors of the skin part due to thermo-oxidative and electro-chemical stresses were nondestructively evaluated. Through the thermo-oxidative aging test, it was shown that the surface hardness IRHD(International Rubber Hardness Degrees) of the rubber increased with a considerable reduction of failure strain. On account of the penetration of coolant liquid into the skin part the weight of rubber specimens degraded by electro-chemical degradation(ECD) test increased, whereas their. failure strain and IRHD hardness decreased largely. The penetration of coolant liquid seemed to induce some changes in inner structure and micro hardness distribution of the rubbers. Consequently, EPDM rubbers degraded by thermo-oxidative aging and ECD could be characterized nondestructively by micro-hardness and chemical structure analysis methods.

Dynamic Constitutive Equations of Auto-Body Steel Sheets with the Variation of Temperature (I) - Dynamic Material Characteristics with the Variation of Temperature - (차체용 강판의 온도에 따른 동적 구성방정식에 관한 연구 (I) - 온도에 따른 동적 물성 특성 -)

  • Lee, Hee-Jong;Song, Jung-Han;Park, Sung-Ho;Huh, Hoon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.31 no.2 s.257
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    • pp.174-181
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    • 2007
  • This paper is concerned with the thermo-mechanical behavior of steel sheet for an auto-body including temperature dependent strain rate sensitivity. In order to identify the temperature-dependent strain rate sensitivity of SPRC35R, SPRC45E and TRIP60, uniaxial tensile tests are performed with the variation of the strain rates from 0.001/sec to 200/sec and the variation of environmental temperatures from $-40^{\circ}C$ to $200^{\circ}C$. The thermo-mechanical response at the quasi-static state is obtained from the static tensile test and that at the intermediate strain rate is obtained from the high speed tensile test. Experimental results show that the variation of the flow stress and fracture elongation becomes sensitive to the temperature as the strain rate increases. It is observed that the dynamic strain aging occurs with TRIP60 at the temperature above $150^{\circ}C$. Results also indicate that the flow stress and tincture elongation of SPRC35R are more dependent on the changes of strain rates and temperature than those of SPRC45E and TRIP60.

A Study of Aging Effect for Train Carbody Using Accelerated Aging Tester

  • Nam, Jeong-Pyo;LI, Qingfen;LI, Hong
    • International Journal of Railway
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    • v.1 no.3
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    • pp.113-116
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    • 2008
  • The long-tenn exposure of polymeric composite materials to extreme-use environments, such as pressure, temperature, moisture, and load cycles, results in changes in the original properties of the material. In this study, the effect of combined environmental factors such as ultraviolet ray, high temperature and high moisture on mechanical and thermal analysis properties of glass fabric and phenolic composites are evaluated through a 2.5 KW accelerated environmental aging tester. The environmental factors such as temperature, moisture and ultraviolet ray applied of specimens. A xenon-arc lamp is utilized for ultraviolet light and exposure time of up to 3000 hours are applied. Several types of specimens - tensile, bending, and shear specimens that are warp direction and fill direction are used to investigate the effects of environmental factors on mechanical properties of the composites. Mechanical degradations for tensile, bending and shear properties are evaluated through a Universal Testing Machine (UTM). Also, storage shear modulus, loss shear modulus and tan a are measured as a function of exposure time through a Dynamic Mechanical Analyzer (DMA). From the experimental results, changes in material properties of glass fabric and phenolic composites are shown to be slightly degraded due to combined environmental effects.

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Effect of Heat Treatment on the Martensitic Transformation and Tensile Deformation Behavior in Ti-Ni-B shape Memory Alloy (Ti-Ni-B 형상기억합금의 마르텐사이트변태 및 인장변형거동에 미치는 열처리의 영향)

  • Lee, O.Y.;Park, Y.K.;Ahn, H.K.
    • Journal of the Korean Society for Heat Treatment
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    • v.8 no.1
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    • pp.75-83
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    • 1995
  • The purpose of this study is to investigate the effect of heat treatments on the martensite transformation and tensile deformation behavior in Ti-Ni-B alloys with various boron concentration. Three types of heat treatment are given to the specimens; i) solution treatment ii) aging iii) thermo-mechanical treatment. In solution treated specimens. R-phase transition which is related to abnormal increase of electrical resistance prior to martensitic transformation has been formed at a boron content of 0.2at % and the $M_s$ temperature has been decreased with the increasing of boron content. However. It has not been affected by aging, while that of thermo-mechanically treated specimens has been remarkably increased in the vicinity of recrystallization temperature. The thermo-mechanically treated specimen has showed a good thermal fatigue characteristics, shape memory effect and superelasticity in comparison with the solution treated specimen.

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The Effect of Fumed Silica Loading on the Thermal Stability of Fluorosilicone Composites

  • Muhammet Iz;Jinhyok Lee;Myungchan Choi;Yumi Yun;Hyunmin Kang;Jungwan Kim;Jongwoo Bae
    • Elastomers and Composites
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    • v.57 no.4
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    • pp.165-174
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    • 2022
  • The effect of fumed silica loading on the thermal stability and mechanical properties of fluorosilicone (FVMQ) rubber was investigated. The distribution of fumed silica inside FVMQ was characterized using scanning electron microscopy, and the thermal stability of composites was evaluated using thermogravimetric analysis and by the changes in mechanical performance during thermo-oxidative aging. The function mechanism of fumed silica was studied by Fourier transform infrared spectroscopy. The results show that with increasing silica content, the crosslink density of composites, the modulus at 100%, and tensile strength also increased, whereas the elongation at break decreased. Furthermore, increasing the silica content of composites increased the initial decomposition temperature (Td) and residual weight of the composite after exposure to nitrogen. In addition, the thermal oxidative aging experiment demonstrated improved aging resistance of the FVMQ composites, including lower change in tensile strength, elongation at break, and modulus at 100%.

Microstructures and Mechanical Properties of DA Alloy 718 (직접시효 처리된 Alloy718 합금의 미세조직과 기계적 특성)

  • Eum C. Y.;Yeom J. T.;Park N. K.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2004.10a
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    • pp.222-225
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    • 2004
  • Alloy 718 is normally used for the stationary and rotating parts of gas turbines due to its excellent combination of high temperature mechanical properties, formability and weldability. The mechanical properties of the Alloy 718 depend very much on grain size, as well as the strengthening phases, ${\gamma}'\;and\;{\gamma}'$. Direct aging is normally used to enhance tensile strengths at high temperatures. The grain structure of the superalloy components is mainly controlled during thermo-mechanical process by the dynamic, meta-dynamic recrystallization and grain growth. In this study, the influence of grain structure and heat treatment on tensile properties of direct-aged Alloy 718 was evaluated.

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Strength Evaluation of Aluminum Alloy Bolt by Nano-Indentation Hardness Test

  • KUBOTA Yoshihiro;NAKAMURA Tamotsu;KOBAYASHI Mitsuo;FUKUDA Katsumi
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2003.10b
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    • pp.123-126
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    • 2003
  • A high strength aluminum alloy bolt (A7050, T7 temper treatment) has been developed by the authors. The bolt has a small grain size in the whole area of the bolt because of the large equivalent strain followed by thermo-mechanical treatment. As the bolt made of A 7050 has a risk of stress corrosion cracking, each grain should be strengthened the grain inside than the grain boundary in order to improve the stress corrosion cracking resistance. It has been confirmed that the nano-indentation hardness at each grain inside increased with the increasing equivalent strain by thermo-mechanical treatment processing.

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