• Title/Summary/Keyword: Thermal Sizing

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Plasma Engineering for Nano-Materials

  • Kim, Seong-In;Shin, Myoung-Sun;Son, Byung-Koo;Song, Seok-Kyun;Choi, Sun-Yong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.08a
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    • pp.79-79
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    • 2012
  • A high temperature and a low temperature plasma process technologies were developed and demonstrated for synthesis, hybrid formation, surface treatment and CVD engineering of nano powder. RF thermal plasma is used for synthesis of spherical nano particles in a diameter ranged from 10 nm to 100 nm. A variety of nano particules such as Si, Ni, has been synthesized. The diameter of the nano-particles can be controlled by RF plasma power, pressure, gas flow rate and raw material feed rate. A modified RF thermal plasma also produces nano hybrid materials with graphene. Hemispherical nano-materials such as Ag, Ni, Si, SiO2, Al2O3, size ranged from 30 to 100 nm, has been grown on graphene nanoplatelet surface. The coverage ranged from 0.1 to 0.7 has been achieved uniformly over the graphene surface. Low temperature AC plasma is developed for surface modification of nano-powder. In order to have a three dimensional and lengthy plasma treatment, a spiral type of reactor has been developed. A similar plasma reactor has been modfied for nano plasma CVD process. The reactor can be heated with halogen lamp.

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Phenylethynyl-terminated polyimide, exfoliated graphite nanoplatelets, and the composites: an overview

  • Cho, Donghwan;Drzal, Lawrence T.
    • Carbon letters
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    • v.19
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    • pp.1-11
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    • 2016
  • In efforts to characterize and understand the properties and processing of phenylethynyl-terminated imide (LaRC PETI-5, simply referred to as PETI-5) oligomers and polymers as a high-temperature sizing material for carbon fiber-reinforced polymer matrix composites, PETI-5 imidization and thermal curing behaviors have been extensively investigated based on the phenylethynyl end-group reaction. These studies are reviewed here. In addition, the use of PETI-5 to enhance interfacial adhesion between carbon fibers and a bismaleimide (BMI) matrix, as well as the dynamic mechanical properties of carbon/BMI composites, are discussed. Reports on the thermal expansion behavior of intercalated graphite flake, and the effects of exfoliated graphite nanoplatelets (xGnP) on the properties of PETI-5 matrix composites are also reviewed. The dynamic mechanical and thermal properties and the electrical resistivity of xGnP/PETI-5 composites are characterized. The effect of liquid rubber amine-terminated poly(butadiene-co-acrylonitrile) (ATBN)-coated xGnP particles incorporated into epoxy resin on the toughness of xGnP/epoxy composites is examined in terms of its impact on Izod strength. This paper provides an extensive overview from fundamental studies on PETI-5 and xGnP, as well as applied studies on relevant composite materials.

A Research on the Characteristics of Spray-Induced Mixing and Thermal Decomposition of Urea Solution in SCR System (SCR 시스템의 요소용액 미립화 및 분해반응 특성 예측에 관한 전산 해석 연구)

  • 김주연;민병수;하지수;류승협
    • Journal of Advanced Marine Engineering and Technology
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    • v.28 no.5
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    • pp.818-826
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    • 2004
  • The spray-induced mixing characteristics and thermal decomposition of aqueous urea solution into ammonia have been studied to design optimum sizes and geometries of the mixing chamber in SCR(Selective Catalytic Reduction) system. The cold flow tests about the urea-injection nozzle were performed to clarify the parameters of spray mixing characteristics such as mean diameter and velocity of drops and spray width determined from the interactions between incoming air and injected drops. Discrete particle model in Fluent code was adopted to simulate spray-induced mixing process and the experimental results on the spray characteristics were used as input data of numerical calculations. The simulation results on the spray-induced mixing were verified by comparing the spray width extracted from the digital images with the simulated Particle tracks of injected drops. The single kinetic model was adopted to predict thermal decomposition of urea solution into ammonia and solved simultaneously along with the verified spray model. The hot air generator was designed to match the flow rate and temperature of the exhaust gas of the real engines The measured ammonia productions in the hot air generator were compared with the numerical predictions and the comparison results showed good agreements. Finally, we concluded that the design capabilities for sizing optimum mixing chamber were established.

A Study on Properties Cu-Sn Matrix Used in Diamond Wheel for Grinding Glass (Diamond Wheel용 Cu-Sn 기지의 유리연삭에 미치는 특성에 관한 연구)

  • Choi, Sung-Kook;Suh, Hyung-Suck;Choe, Jeong-Cheol
    • Journal of Korea Foundry Society
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    • v.12 no.4
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    • pp.317-325
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    • 1992
  • Diamond is the hardest material known to humans, also possesses the highest thermal conductivity and a very low thermal expansion coefficient. Therefore, these properties of diamond make them logical choices for many difficult grinding application. Bonding material is a very important factor to performance of a grinding wheel. Grinding glass constitutes one of the major application areas of diamond grinding wheels, and Cu-Sn tin bronze matrix is widely used as a metal bond of diamond wheel in grinding glass but these studies are rarely reported. The bronze test pieces excluding diamond are sintered by the method of hot sizing respectively at $600^{\circ}C$, $650^{\circ}C$, $700^{\circ}C$, with a composition(Cu-10wt%Sn) on ${\alpha}$ phase and two compositions(Cu-20wt%Sn and Cu-23wt%Sn) on ${\alpha}+{\beta}$ phase. The rupture strength of Cu-10wt%Sn is highest. The bronze bonded diamond wheels are manufactured by same conditions as the bronze test pieces. The results of grinding ratio of wheels are highest in case of Cu-10wt%Sn bonded wheel sintered at $650^{\circ}C$ and grinding power is highest in same composition sintered at $700^{\circ}C$.

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The Effects of the Tempered Materials on the Thermal Runaway Characteristics in the Resol Resin Synthesis Reaction (레졸수지 합성반응에서 온도조절 물질이 열폭주 특성에 미치는 영향)

  • Lee, Jung-Suk;Lee, Keun-Won
    • Journal of the Korean Institute of Gas
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    • v.18 no.4
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    • pp.27-34
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    • 2014
  • In this study, we evaluated an effect of the tempered materials on the thermal runaway characteristics in the resol resin synthesis reaction using the adiabatic calorimetry of vent sizing package 2(VSP2). The kinetic parameters, such as an activation energy and heat of reaction, were estimated using the test results. As the results, the instantaneous characteristics to express the intensity of runaway reaction decreased at the low solid content. However, the sudden loss of the tempered materials triggered the second runaway reaction rapidly. In this condition, the heat of reaction and the activation energy of phenol and p-formaldehyde were about 157 kJ/mol and 60 kJ/mol, respectively.

Optimization of three small-scale solar membrane distillation desalination systems

  • Chang, Hsuan;Hung, Chen-Yu;Chang, Cheng-Liang;Cheng, Tung-Wen;Ho, Chii-Dong
    • Membrane and Water Treatment
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    • v.6 no.6
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    • pp.451-476
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    • 2015
  • Membrane distillation (MD), which can utilize low-grade thermal energy, has been extensively studied for desalination. By incorporating solar thermal energy, the solar membrane distillation desalination system (SMDDS) is a potential technology for resolving the energy and water resource problems. Small-scale SMDDS (s-SMDDS) is an attractive and viable option for the production of fresh water for small communities in remote arid areas. The minimum-cost design and operation of s-SMDDS are determined by a systematic method, which involves a pseudo steady state approach for equipment sizing and the dynamic optimization using overall system mathematical models. The s-SMDDS employing three MD configurations, including the air gap (AGMD), direct contact (DCMD) and vacuum (VMD) types, are optimized. The membrane area of each system is $11.5m^2$. The AGMD system operated for 500 kg/day water production rate gives the lowest unit cost of $5.92/m^3$. The performance ratio and recovery ratio are 0.85 and 4.07%, respectively. For the commercial membrane employed in this study, the increase of membrane mass transfer coefficient up to two times is beneficial for cost reduction and the reduction of membrane heat transfer coefficient only affects the cost of the DCMD system.

A study of guaranteeing reliability for IC of electronic instruments according temperature

  • Yoon, Geon;Park, Yong-Oon;Kwon, Soon-Chang
    • 제어로봇시스템학회:학술대회논문집
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    • 2005.06a
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    • pp.320-323
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    • 2005
  • This paper discusses heat problem of IC, which composes the electronic instruments, to guarantee reliability of electronic instruments. And also proposes the unified equivalent model for various electronic instrument products to guarantee reliability and life of its parts. Because electronic instruments are down sizing and operated with high frequency, the internal temperature of electronic instruments is rising steadily. The internal temperature of the electronic instruments gives a big effect to electronic instrument's reliability and life. The semiconductor parts are the representative heat generation parts because of its complicated function, high frequency and high density. Consequently, guaranteeing reliability and life of electronic semiconductor is the important start point in securing the reliability and life of the electronic instrument product. Unfortunately, there are many factors, which affect heat dissipation efficiency. The heat dissipation efficiency follows the environment where the electronic instrument products are used. Therefore it is very difficult to define reliability and life of the electronic manufactures. Electronic instrument products are composed of printed circuit board (PCB), integrated circuit (IC), resistance, and capacitor and so on. And there are superposed thermal resistances, because the parts are arrayed on the printed circuit board (PCB), Therefore the total thermal resistance is variable. Consequently it cannot have same thermal model for each electronic instrument products. In the next part, we propose the unified equivalent model for various electronic instruments. And using the proposed equivalent model proofs the method for analysis reliability of electronic parts.

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Study of Thermal Decomposition of Kevlar/EPDM (Kevlar/EPDM 고무계 내열재의 열반응 연구)

  • Kim, Yun-Chul;Jung, Sang-Ki;Kang, Yoon-Goo;Lee, Seung-Goo
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2010.11a
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    • pp.257-260
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    • 2010
  • The purpose of this paper is to introduce a method to predict the case thermal insulation charred and erosion thickness as a function of the exposure time to combustion gases and in solid rocket motors. The sizing of the insulator requires a good estimation of the thermal and mechanical loads at the wall. The method is particularly suitable for internal insulation areas subjected to high radiative, convective heat fluxes and $Al_2O_3$ slag pool. The mathematical approach and lab-scale experiment were intentionally simplified in order to obtain some simple and rapid relationships particularly useful for trade-off studies and thermal insulation preliminary design. The method was utilized to compute the charred and erosion thicknesses of the insulation on the aft chamber domes. A comparison between theoretical and experimental insulator char thicknesses of the motor insulation is reported, indicating the applicability of the predictive method employed.

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Measurement of Defects with Scanning Acoustic Microscope and Acoustic Emission (초음파 현미경 및 AE에 의한 결함 측정)

  • Choi, Man-Yong;Park, Ik-Gun;Han, Eung-Kyo
    • Journal of the Korean Society for Precision Engineering
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    • v.8 no.4
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    • pp.118-125
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    • 1991
  • Acoustic microscopy has attracted much interest recently as potential nondestructive evaluation technique for detecting and sizing defects of surface and sub-surface. Also acoustic emission testing method has been developed for detecting microcracks which is more than 30${\mu}m$ in length quantitatively on ceramics. In the present paper, acoustic emission during the four point bending test in hot-pressed sintered $Si_3N_4$ specimen which was stressed by thermal shock, has been measured by high sensitive sensing system. The surface and sub-surface cracks were detected by scanning acoustic micrscope of 800 MHz and conventional ultrasonic testing in C-scope image. The purpose was to investigate the location and size of cracks by SAM and AE technique, whose experimental data demonstrate good for detecting microcracks.

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A Characteristic Analysis of Solar Radiation Resources in Korea (국내 일사량 자원 특성분석)

  • Jo, Dok-Ki;Yun, Chang-Yeol;Kim, Kwang-Deuk;Kang, Young-Heak
    • 한국신재생에너지학회:학술대회논문집
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    • 2009.11a
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    • pp.413-416
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    • 2009
  • Since the solar radiation is main input for sizing any solar photovoltaic system and solar thermal power system, it will be necessary to understand and evaluate the insolation data. The Korea Institute of Energy Research(KIER) has begun collecting horizontal global insolation data since May, 1982 and direct normal insolation data since December 1992 at 16 different locations. Because of a poor reliability of existing data, KIER's new data will be extensively used by solar energy system users as well as by research institutes. Among some significant results, the yearly averaged horizontal global insolation was turned out 3.61 kWh/$m^2$/day and the yearly mean 5.38 kWh/$m^2$/day of the direct normal insolation was evaluated for clear days.

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