• Title/Summary/Keyword: Texture Evolution

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Five New Species of Genus Hyattella (Dictyoceratida: Spongiidae) from Korea

  • Sim, Chung Ja;Kim, Young A;Lee, Kyung Jin
    • Animal Systematics, Evolution and Diversity
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    • v.31 no.1
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    • pp.8-14
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    • 2015
  • Five new species of the genus Hyattella (Dictyoceratida: Spongiidae); Hyattella chaguiensis n. sp., H. munseomensis n. sp., H. sumsangiensis n. sp., H. bakusi n. sp., and H. purpurea n. sp., were collected from Jeju-do, Korea. Hyattella chaguiensis n. sp. is similar to H. mara Sim and Lee, 2014 in shape, but differs in dermal membrane and primary fibres. Hyattella munseomensis n. sp. differs in cored primary fibres, having middle-size sand. Hyattella sumsangiensis n. sp. is characterized by color changes and very soft texture. Hyattella bakusi n. sp. and H. purpurea n. sp. are similar in shape, having tube-like elevated holes, but differ in skeletal structures.

Development of Textures and Microstructures during Compression in a Hot-Extruded AZ31 Mg Alloy (고온압출한 AZ 31 마그네슘 합금의 압축변형 중 집합조직과 미세조직의 발달)

  • Jung, Byung Jo;Lee, Myung Jae;Park, Yong-Bum
    • Korean Journal of Metals and Materials
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    • v.48 no.4
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    • pp.305-314
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    • 2010
  • The development of textures and microstructures during plastic deformation in a hot-extruded AZ 31 Mg alloy was investigated using a compression test with such parameters as deformation temperature, strain rate. It was observed from true stress-strain curves that twinning involves changes of the flow stresses. In the early stages of deformation at temperatures lower than $200^{\circ}C$, the occurrence of twins resulted in a decrease of the work-hardening rate, which increased drastically at a true strain of -0.05. The evolution of the deformation textures were assessed with the aid of EBSD analyses in terms of the competition between twinning and slip activity.

Fabrication of TFA-MOD YBCO Films Using Y2Ba1Cu1Ox Process (Y2Ba1Cu1Ox공정을 이용한 TFA-MOC YBCO 박막 공정 개발)

  • Lim, Jun-Hyung;Jang, Seok-Hern;Kim, Kyu-Tae;Lee, Jin-Sung;Yoon, Kyung-Min;Ha, Hong-Soo;Joo, Jinho;Nah, Wansoo
    • Journal of the Korean Ceramic Society
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    • v.43 no.2 s.285
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    • pp.98-105
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    • 2006
  • YBCO film was synthesized by using a new approach to the TFA-MOD method. In the fabrication process, $Y_2Ba_1Cu_1O_x\;and\;Ba_3Cu_5O_8$ powders were used as precursors (the so called '211 process'), instead of Y-, Ba-, and Cu-based acetates, and dissolved in trifluoroacetic acid followed by calcining and firing heat treatment. Consequently, we successfully fabricated YBCO film and evaluated the phase formation, texture evolution, and critical properties as a function of the calcining and firing temperature and humidity, in order to explore its possible application in coated conductor fabrication. The films were calcined at $430-460^{\circ}C$ and then fired at $750-800^{\circ}C\;in\;a\;0-20\%$ humidified $Ar-O_2$ atmosphere. We observed that $BaF_2$ phase was effectively reduced and that a sharp and strong biaxial texture formed under humidified atmosphere leading to increased critical properties. In addition, we found that the microstructure varied significantly with the firing temperature: the grain grew further, the film became denser, and the degree of texture and phase purity varied as the firing temperature increased. For the film fired at $775^{\circ}C$ after calcining at $460^{\circ}C$, the critical current was obtained to be 39 A/cm-width (corresponding critical current density is $2.0\;MA/cm^2$ which was probably attributed to such factors as the enhanced phase purity and out-of-plane texture, the moderate film density and grain size, and crack-free surface.

Analysis of Postharvest 1-MCP Treatment and CA Storage Effects on Quality Changes of 'Fuji' Apples during Export Simulation (모의 수출 '후지' 사과의 품질에 미치는 수확후 1-MCP 처리 및 CA저장 효과)

  • Park, Youn-Moon;Park, Hyo-Geun;Lim, Byung-Sun
    • Horticultural Science & Technology
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    • v.29 no.3
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    • pp.224-231
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    • 2011
  • Effects of 1-methylcyclopropene (1-MCP) treatment and controlled atmosphere (CA) storage was analyzed for the export quality of 'Fuji' apples after 8-month storage. Apples were harvested from two orchards located in different regions at relatively late stage of maturity for long-term storage. Fruit were treated with 1 ${\mu}L{\cdot}L^{-1}$ 1-MCP and then stored in $0^{\circ}C$ air or CA with 1.5 kPa $O_2$ and < 1.0 kPa $CO_2$ for 8 months. To simulate poststorage export process such as 2-week refrigerated container shipment plus 7-day local distribution, fruit were put in $0^{\circ}C$ air storage for additional two weeks and then on the shelf for 7 days at $20^{\circ}C$. Both the 1-MCP treatment and CA storage reduced respiration and ethylene evolution after storage and shipping simulation, and successfully maintained titratable acidity and flesh firmness even after the export process. In 'Fuji' apples harvested after adequate stage of maturity for long-term storage, however, 1-MCP treatment alone seemed not to be satisfactory for the maintenance of sensorial fruit texture for export market. CA storage or 1-MCP treatment/CA storage combination program should be applied for lately harvested 'Fuji' apples exported after eight months storage.

Texture Evolution during Primary Recrystallization and Effect of Number of Cold Rolling Passes, Heating Rate, and Si Contents in Grain-Oriented Electrical Steel (방향성 전기강판에서 1차 재결정시 Si 함량과 냉간압연 횟수, 승온 속도에 따른 집합조직 발달)

  • Jeon, Soeng-Ho;Park, No Jin
    • Journal of the Korean Society for Heat Treatment
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    • v.31 no.6
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    • pp.269-274
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    • 2018
  • Grain-oriented electrical steel sheets are mainly used as core materials for transformers and motors. They should have excellent magnetic properties such as low core loss, high magnetic flux density and high permeability. In order to improve the magnetic properties of the electrical steel sheet, it is important to form Goss oriented grains with a very strong {110}<001> orientation. Recently, efforts have been made to develop Goss grains by controlling processes such as hot rolling, cold rolling, and primary and secondary recrystallization. In this study, the sheets containing 3.2 and 3.4wt.% Si were used, which were rolled with 1 and 10 passes with total thickness reduction of 89%. Heating was carried out for primary recrystallization with different heating rates of $25^{\circ}C/s$ and $24^{\circ}C/min$ until $720^{\circ}C$. The behavior of Goss-, {411}<148>-, and {111}<112>-oriented grains were analyzed using X-ray diffraction(XRD) and electron back-scatter diffraction(EBSD) analysis. The area fraction of Goss-oriented grains increased with the number of rolling passes during cold rolling; however, after the primary recrystallization, the area fraction of the Goss grains was higher and exact Goss grains were found in the specimens subjected to rapid heating after one rolling pass.

The effect of the heat treatment of MOCVD Cu thin film on electromigration (MOCVD Copper 박막의 열처리가 Electromigration 특성에 미치는 영향 연구)

  • 이원석;배성찬;손승현;최시영
    • Journal of the Korean Vacuum Society
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    • v.11 no.4
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    • pp.194-200
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    • 2002
  • MOCVD(metal-organic chemical vapor deposition) copper thin film was annealed at various conditions and the eletrical properties and micro-structures were investigated to find the optimal annealing condition and its effect. Cu thin film annealed at Ar 1 torr, $400^{\circ}C$ had the most improved resistivity of 1.98 $\mu\Omega$cm, and texture; the ratio of $I_{(111)}/I_{(200)}$ was varied from 2.03 to 3.11, and Cu thin film annealed at Ar 1 torr, $450^{\circ}C$ had the largest grain size and uniformity. After the annealing, the EM(electromigration) test was followed to ensure the improved properties by annealing. Compare to other conditions, Cu patterns annealed at Ar 1 torr, $400 ^{\circ}C$ had the most improved properties when it came to the EM resistance, which was due to the low resistivity, the preferential evolution of texture to (111) plane, and the reduction of surface roughness of annealed copper film.

Potential of Initial CA Condition on Quality Maintenance of 'Fuji' Apples during Export Simulation after Long-term Storage

  • Park, Youn-Moon;Park, Hyo-Geun
    • Horticultural Science & Technology
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    • v.30 no.4
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    • pp.400-408
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    • 2012
  • Effects of initial controlled atmosphere (CA) treatment on quality maintenance of 'Fuji' apples were assessed and compared with 1-methylcyclopropene (1-MCP) treatment and continuous CA storage. Apples were harvested twice at different maturity, treated with 1 ${\mu}L{\cdot}L^{-1}$ 1-MCP and then stored for 8 months at $0^{\circ}C$ under 3 conditions: air, CA for the first month followed by air (initial CA), and continuous CA (full CA). CA storage was performed with 1.5 kPa $O_2$ and < 1.0 kPa ($N_2$ balance). Following long-term storage, export simulation, refrigerated shipment and local distribution, were performed by holding apples at $0^{\circ}C$ for 2 weeks and on the shelf at $20^{\circ}C$ for 7 days. Both the application of 1-MCP and CA storage reduced ethylene production and respiration rates. Initial CA storage was also effective on reducing the metabolism although the effects were not as noticeable as full CA. Full CA storage with or without 1-MCP treatment maintained titratable acidity, flesh firmness, and sensory quality at the acceptable to excellent level even after the export simulation following 8-month storage regardless of harvest maturity. In contrast, effects of initial CA storage were limited to the maintenance of firmness and texture in early-harvested apples. Overall results indicated that harvest maturity is the critical factor for export fruit quality after long-term storage when separate treatment of initial CA storage or 1-MCP treatment is applied as a postharvest program.

Anisotropy Studies on Hot-forged $\gamma$-TiAl Alloys (열간단조된 $\gamma$-TiAl 합금의 이방성에 관한 연구)

  • Lee, Jae-Seung;Park, No-Jin;Kim, Seong-Jin;Kim, Seung-Eon;O, Myeong-Hun
    • Korean Journal of Materials Research
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    • v.10 no.9
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    • pp.629-635
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    • 2000
  • The texture evolution during isothermal forging and subsequent heat treatment in Ti-48.5at%Al-0.6at%Mo alloy was investigated. Especially, in the present study, research interest was focused on the interrelation between lamellar volume fraction and textures varied with the change of heat-treated time and temperature. It was found that texture components having ND┴{302) and TD$\perp${100} with minor TD$\perp${111} were developed by isothermal forging. In addition, when the followed heat-treatment time and temperature increased from $1330^{\circ}C$/10h to $1350^{\circ}C$/20h respectively, both the lamellar volume fraction and the intensity of textures mentioned above also gradually increased. However, the tensile elongation at room temperature decreased oppositely, as the lamellar volume fraction increased. These results suggested that tensile properties of $\gamma$-TiAl with the nearly lamellar microstructure at room temperature were affected more strongly by the microstructural features such as lamellar volume fraction rather than by textures.

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Anodic Properties of Needle Cokes-derived Graphitic Materials in Lithium Secondary Batteries (침상 코크스(needle cokes)로부터 제조된 흑연질 탄소재료의 리튬 2차전지 음극특성)

  • Park Chul Wan;Oh Seung M.
    • Journal of the Korean Electrochemical Society
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    • v.2 no.4
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    • pp.221-226
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    • 1999
  • Two needle cokes (NC-A and NC-B) that differ in both the texture and impurity content to each other were graphitized at $2000-3000{\circ}C$, and the average particle size, size distribution and surface area were compared after milling. Their anodic properties in Li secondary batteries were also analyzed. Two materials showed a higher degree of graphitization with an increase in the preparation temperature, however, the NC-B series was less graphitized than NC-A due to the presence of impurities and less ordered mosaic texture. The mein particle size of the milled powder was proportional to the degree of graphitization, but the surface area showed the opposite trend. The highly graphitized materials yielded powders of lower uniformity in the size distribution. The discharge capacity of the resulting carbons steadily decreased in the temperature range of 1000 to $2000^{\circ}C$ due to the depletion of carbonaceous interlayers that contain crystal defects. A later increase in the discharge capacity was observed at $>2000^{\circ}C$, which arises from the formation of graphitic interlayers. The milling process gave rise to a sloping discharge curve at >1.0 V, but this was converted to a plateau at <0.25V after a repeated cycling or additional heat-treatment at $1000^{\circ}C$. The discharge at >1.0V likely comes from the disordered surface structure formed during the milling process. The evolution of a plateau at <0.25 V suggests that this disordered structure transforms to a more ordered graphitic one upon a cell cycling or heat-treatment.

A Study on Freezing Possibility of Jeung-Pyun Batter (증편 반죽의 냉동 가능성에 관한 연구)

  • 최원석;노정옥;우경자
    • Journal of the East Asian Society of Dietary Life
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    • v.13 no.6
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    • pp.593-600
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    • 2003
  • This study was carried out in order to investigate the possibility of frozen rice batter for the manufacturing of Jeung-pyun. Despite of its unique taste and texture, Jeung-pyun is not consumed much because it needs long time to make. The physicochemical, sensory, rheological and surface characteristics of Jeung-pyun were analyzed to develop the easy manufacture method. The storage condition of rice batter was used at -2$0^{\circ}C$ up to 4 weeks. Statistical data analysis was completed using a SAS program. The results are summarized as follow: The pH brix% and sugar content of all samples which added low-temperature tolerance raw yeast or regular raw yeast decreased during the fermentation. Kind of yeast did not influence on the moisture content of the Jeung-pyun batter. Specific volume and carbon dioxide evolution of Jeung-pyun batter were highest when the rice batter was frozen for 1 week regardless of the kind of yeast. Overall quality of frozen batter of Jeung-pyim at -2$0^{\circ}C$ for 4 weeks had the highest score among different samples. As the test results of mechanical characteristics, cohesiveness, gumminess, brittleness, hardness and springiness did not show any significant differences statistically. The result clearly suggests that freezing the rice batter is a possibile way to manufacture Jeung-pyun.

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