• Restorative Dentistry and Endodontics
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• 제26권1호
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• pp.23-31
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• 2001

The purpose of this study was to search the optimal silane concentrations for filler- silanization of seven experimental composites. Silica filer was a 25micron crushed type. 0.0%, 0.5%, 1.0%, 1.5%, 2.0%, 2.5%, and 3.0% silane($\gamma$-methacrylooxypropyltrimethoxysilane)were added into silica-filler with weight percentage (wt%). Mixtures(silica filler/silane)were reacted at 6$0^{\circ}C$ for 72hours, and crushed into fine particles those were used as fillers for 7 experimental composites. Monomer was a 3 : 1 mixture of Bis-GMA and TEGDMA containing 0.2% tertiary amine and 0.4% camphoroquinone for light curability. A ratio for mixing the monomer and filler was 75% and 25% respectively. Seven experimental composites was classified with the concentration of silane treated, and the specimen number for each test was 10. Specimens with 6mm diameter and 3mm height dimension for measuring the diametral tensile strength were destroyed with 1mm/min cross-head speed on Instron universal testing machine (No. 4467, USA). Shear bond strength was measured on the specimens bonded to bovine enamel etched with 37% phosphoric acid solution for 1 minute Fractured surfaces were observed by SEM (Hitachi S-3200, Japan) among that of the highest values measured from each groups. Following results were obtained: 1. Experimental composites containing silanized filter showed the significantly higher diametral tensile strength and shear bond strength than the composites containing un-silanized fillers(Group1) (p<0.05). 2. In silanized filler composite resins(Group 2~7), Diametral tensile strength of Group 3 showed the significantly higher than that of Group 2 and Group 6(p<0.05). 3. Shear bond strength was higher in Group 3 than that of Group 7 (p＜0.05)in silanized fillers composite resins. 4. Fracture surface was formed in resin matrixes on the specimens from composites containing the fillers treated with 0.5% 1.0%, and 1.5% silane. These results mean that the optimal silane concentrations are exist for each fillet with its size and surface area, and that 1.0% is a optimal value for concentration to coat the 25$\mu\textrm{m}$ filler with silane.

• Restorative Dentistry and Endodontics
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• 제26권1호
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• pp.41-50
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• 2001

The purpose of this study was to examine the influences of camphoroquinone on the properties of five experimental composites. The contents of camphoroquinone were varied as 0.2%, 0.3%, 0.4%, 0.5%, and 0.6%, with silanized filler 75% and tertiary amine 0.2%. Five kinds of experimental composites were prepared, and diametral tensile strength, shear bond strength, depth of cure and yellowish discoloration were tested as a measurement. Specimen numbers of 10 were applied to all test items and experimental groups. Specimens for testing the diametral tensile strengths with internal diameter of 6mm in diameter and 3mm in height were filled with 5 experimental composites which were crushed with 1mm/min cross-head speed on Instron universal testing machine (Model No. 4467). Shear bond strength was measured on specimens attached to bovine teeth enamel etched with 37% phosphoric acid. Depth of cure was measured by the measurement of height of specimens which were removed the un-polymerized portion with acetone. Yellowness measurements were made by chromometer(Minolta Co. Japan) using L$^*$a$^*$b$^*$ values. ANOVA and Multiple range tests were used analyzed data with confidence level at 95%. The mean value of the shear bond strengths ranged from 31.03MPa to 39.49MPa. Following results were obtained ; 1. Diametral tensile strength was highest in experimental group 3, then was not affected by the contents of camphoroquinone ($r^2$=0.0422). 2. Composite resins containing 0.4% camphoroquinone showed the highest shear bond strength, but there was no statistical significance (p=0.3718). 3. Camphoroquinone reduces the depth of cure in the composite resins (p=0.0004, $r^2$=0.9483). 4. Camphoroquinone made the composites yellowish ($r^2$=0.9815). These results mean that increased content of camphoroquinone reduces the depth of cure, and that camphoroquinone make composites yellowish.

• 대한금속재료학회지
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• 제46권12호
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• pp.780-787
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• 2008

For the advanced high strength steels (AHSS), high-manganese TWIP (twinning induced plasticity) steels exhibit high tensile strength (800-1000 MPa) and high elongation (50-60%). However, the TWIP steels need to be understood of delayed fracture following the cup drawing test. Among the factors to cause delayed fracture, i.e, martensite transformation, hydrogen embrittlement and residual stress, the effects of martensite transformation (${\gamma}{\rightarrow}{\varepsilon}$ or ${\gamma}{\rightarrow}{\alpha}^{\prime}$) were investigated on the delayed fracture phenomenon. Microstructural phase analysis was conducted for cold rolled (20, 60, 80% reduction ratio) steels and tensile deformed (20, 40, 60% strain) steels. For the Al-added TWIP steels, no martensite phase was found in the cold rolled and tensile deformed specimen. But, the TWIP steels with no Al addition indicated the martensite transformation. The cup drawing specimens showed the martensite transformation irrespective of the Al-addition to the TWIP steel. However, the TWIP steel with no Al exhibited the larger amount of martensite than the case of the TWIP steel with Al addition. For the reason, it was possible to conclude that the Al addition suppressed the martensite transformation in TWIP steels, therefore preventing the delayed fracture effectively. However, it was interesting to note that the mechanism of delayed fracture should be incorporated with hydrogen embrittlement and/or residual stress as well as the martensite transformation.

• 한국산학기술학회논문지
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• 제17권12호
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• pp.285-291
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• 2016

본 연구의 목적은 유공강판 전단연결재로 보강된 강관말뚝의 인발실험을 통하여 구조성능을 평가하는 것이다. 인발실험에 앞서 재료의 특성을 파악하기 위하여 콘크리트 압축장도 실험을 수행하였으며, 실험에 사용되는 철근 및 철판의 항복하중, 인장강도 및 연신율 등의 재료적 특성을 미리 파악하였다. 유공강판 전단연결재로 보강된 강관말뚝의 인발실험은 2,000kN 용량의 UTM을 이용하여 0.01mm/sec 재하속도의 변위제어 방법으로 실험을 수행하였다. 계측을 위하여 철근 및 유공강판 중앙에 strain gauge를 부착하였으며, 가력판과 충전콘크리트 사이의 상대변위 측정을 위하여 변위계(LVDT)를 설치하였다. 유공강판 전단연결재로 보강된 실험체의 항복하중은 각각 923.8kN과 981.1kN으로 기존 설계법에 의하여 제작된 실험체의 항복하중인 641.7kN에 비하여 1.44배 ~ 1.53배 증가됨을 알 수 있었다. 또한 유공강판 전단연결재로 보강된 실험체의 극한하중은 각각 1004.4kN과 1055.5kN으로 기존 설계법에 의하여 제작된 실험체의 극한하중인 813.7kN에 비하여 1.23배 ~ 1.29배 증가됨을 알 수 있었다. 반면, 유공강판 전단연결재로 보강된 실험체의 항복변위 및 극한상태의 변위는 기존 설계법에 의하여 제작된 실험체에 비하여 각각 0.61배 및 0.42배 감소됨을 알 수 있었다. 따라서 유공강판 전단연결재로 보강된 강관말뚝은 강성은 증가하고 상대변위 및 변형률은 낮게 측정되어 기존 말뚝머리 보강방법을 대체할 수 있는 적절한 보강방법임 알 수 있었다.

• Journal of Advanced Marine Engineering and Technology
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• 제9권2호
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• pp.126-142
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• 1985

The plane bending corrosiion fatigue test for the welded metal parats was performed in the air and in the natural sea water with and without applying cathodic protection. The specimens tested were the weld of SM41 steel plates, SM58 steel plates and of SM41 to SM58, which were all prepared by submerged arc welding. The main results obtained from the experiment are summarized as follows: (1) In case with SM41 and SM58 steel plates, lower value of impact strength, higher value of hardness and more noble electrode potential were observed in the welded metal part than in the HAZ and base metal. Also the lowest hardness zone in the HAZ was observed with SM58 which was not found with SM41. In case with weld specimen of SM41 to SM58, the impact strength and the electrode potential of the welded metal part showed again the lowest and most noble value but the hardness value was located between those of SM41 and SM58 base metal. (2) In the fatigue test, the specimens tested in the air and under the cathodic protection were both cracked in a purely mechanical mode, but the specimens tested without cathodic protection were cracked by the combination of mechanical fracture and electro-chemical corrosion. (3) The corrosion fatigue limit of the welded metal parts of the specimen was increased by the cathodic protection. As the protection potential was varied down to -800 mV vs. SCE the fatigue limit was increased to the value tested in the air, and the maximum fatigue limit appeared at the -1, 000 - -1, 200 mV vs. SCE. However, as the protection potential was further decreased below -1, 200 mV vs.SCE, the fatigue limit of weld of SM58 and of SM41-SM58 joining was decreased but the limit was almost constant in the case of weld of SM41. (4) It is suggested that when designing steel ship the corrosion fatigue limit of welded metal parts should be stressed as a designing strength of the structure of steel ship in addition to the conventional basis considering simply tensile strength of steel and safety factor.

• Computers and Concrete
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• 제32권4호
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• pp.351-363
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• 2023

Reducing the self-weight of reinforced concrete structures problem is discussed in this paper by using two types of self-weight reduction, the first is by using lightweight coarse aggregate (crushed brick) and the second is by using styropor block. Experimental and Numerical studies are conducted on (LWAC) lightweight aggregate reinforced concrete slabs, having styropor blocks with various sizes of blocks and the ratio of shear span to the effective depth (a/d). The experimental part included testing eleven lightweight concrete one-way simply supported slabs, comprising three as reference slabs (solid slabs) and eight as styropor block slabs (SBS) with a total reduction in cross-sectional area of (43.3% and 49.7%) were considered. The holes were formed by placing styropor at the ineffective concrete zones in resisting the tensile stresses. The length, width, and thickness of specimen dimensions were 1.1 m, 0.6 m, and 0.12 m respectively, except one specimen had a depth of 85 mm (which has a cross-sectional area equal to styropor block slab with a weight reduction of 49.7%). Two shear spans to effective depth ratios (a/d) of (3.125) for load case (A) and (a/d) of (2) for load case (B), (two-line monotonic loads) are considered. The test results showed under loading cases A and B (using minimum shear reinforcement and the reduction in cross-sectional area of styropor block slab by 29.1%) caused an increase in strength capacity by 60.4% and 54.6 % compared to the lightweight reference slab. Also, the best percentage of reduction in cross-sectional area is found to be 49.7%. Numerically, the computer program named (ANSYS) was used to study the behavior of these reinforced concrete slabs by using the finite element method. The results show acceptable agreement with the experimental test results. The average difference between experimental and numerical results is found to be (11.06%) in ultimate strength and (5.33%) in ultimate deflection.

• 한국구조물진단유지관리공학회 논문집
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• 제12권6호
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• pp.249-256
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• 2008

해양콘크리트 구조물의 내구성은 염분의 침투와 확산에 의해 심하게 저하한다. 이로 인해 많은 연구자들이 해양구조물에 대한 내구성을 향상시키기 위한 연구를 수행하여 왔다. 이 연구에서는 광물질 혼화재, 코팅철근, 부식억제제를 사용한 휨 부재에 대하여 4점 휨 시험을 수행함으로써 휨 거동을 비교 평가하고 해양구조물로의 적용성을 검토하였다. 결과에 따르면, 광물질 혼화재와 부식억제제는 초기균열 안전성과 휨 저항에 효율적인 것으로 나타났다. 내구성 재료를 사용하여도 동일 휨 모멘트 구간에서의 인장철근 응력 변화는 적고 부재도 안정된 거동을 보인다. 또한, 내구성 재료를 사용한 부재의 균열간격도 크지 않게 나타났다.

• 한국수산과학회지
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• 제14권4호
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• pp.269-275
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• 1981

연근해 어업용 낚시 6가지형에 대하여 만능실험기로 인장속도를 290mm/min와 780mm/min로 하여 실험한 결과는 다음과 같다. 1) 낚시의 직경은 d, 미늘 기부에서 허리굽이까지의 거리를 w라 하면 낚시의 파단하중은 $B={\alpha}\;wd^2+\beta$ (단, B는 kg, w와 d는 mm)로 나타내며, 인장연도가 290mm/min 일 때의 $\alpha,\;\beta$는 둥근형 낚시 $SR_{p}-F_{1}B,\;SR_{p}-F_{1}S$는 $\alpha_{s}=0.5,\;\beta_{s}=1.6$, 모난형 낚시 $SA_{a}-F_{1}S,\;SA_{a}-F_{1}S_k,\;LA_{a}-F_{1}S_{k}$는 $\alpha_{s}=1.1,\;\beta_{s}=2.0$긴 낚시 $LA_{p}-F_{1}S$는 $\alpha_{s}=0.4,\;\beta_{s}=1.5$정도이다. 2) 인장속도가 780mm/min 일 때 윗식에서 $\alpha,\;\beta$는 둥근형 낚시는 $\alpha_{f}=0.4,\;\beta_{f}=1.4$모난형 낚시는 $\alpha_{f}=1.0$ 일본산은 $\beta_{f}=0.9$, 국산은 $\beta_{f}=-2.5$ 긴 낚시는 $\alpha_{=}0.6,\;\beta_{f}=0.4$ 정도이다. 3) 낚시의 파단변형률은 $40\sim60\%$ 정도이며, 인장속도가 빠를 때의 변형률은 느릴 때에의 $95\%$ 정도이나, 빠를 때의 파단하중은 느릴 때의 $80\%$ 정도이다. 4) 낚시가 파단되는 부위는 인장속도에 관계없이 거의 모두 허리굽이 부분이며 꼭지 기부에서 파단점까지의 거리는 낚시 길이와 거의 같다.

• 한국재료학회지
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• 제3권3호
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• pp.253-260
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• 1993

용해와 주조, 압출과 열처리 기술의개선으로 고강도, 고파괴인성의 AI-Li-Cu 합금(2090 AI합금)을 제조하였다. 또한 준 산업용 규모(20kg)의 잉고트 제조공정을 확립하기 위해서 (1)선 (2)기계적 성질들에 미치는 열처리 영향 (3) 인장시험, 파괴인성 시험($K_{Ic}$) 및 피로균열 전파시계를 갖고 있으며 최종 제품의 인장강도는 최대시효 조건에서 534MPa부터 566MPa이었고 연신율은 9%에서 11.9%정도였다. C-T 시편을 이용한 파괴인성 시험 결과 최대시효 조건에서 평면변형 파괴인성 ($K_{Ic}$)값은 39MPa$\surd$m였고 미시효 조건에서는 23MPa$\surd$m였다. 또한 0.1, 0.3, 0.5의 하중비에서 피로균열 전파시험을 행하였을때 임계응력 확대계수(${\Delta}K_{th}$)는 각각 6.0, 5.3, 4.3 MPa$\surd$m이었다.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2001년도 춘계학술대회논문집A
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• pp.181-186
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• 2001

JLF-1 steel (Fe-9Cr-2W-V-Ta), low activation ferritic steel, is one of the promising candidate materials fer fusion reactor applications. High temperature fatigue life and tensile strength of JLF-1 steel and its TIG welded joints were investigated at the room temperature and $400^{\circ}C$. The strength of base metal (JLF-1) is in between those of weld metal and the HAZ. When the test temperature was increased from room temperature to $400^{\circ}C$, both strength and ductility decreased for base metal, weld metal and the HAZ. The longitudinal specimens of base metal showed similar strength and ductility compared with those of the transverse specimens at room temperature and $400^{\circ}C$. Little anisotropy was observed in the JLF-1 steel base metal in terms of rolling direction. Fatigue limit of weld metal which was obtained from cross-weld specimen is 495MPa. Thus, the weld metal showed the higher fatigue limit than those of base metal at both room temperature and $400^{\circ}C$. Little anisotropy of fatigue properties was observed for JLF-1 base metal in terms of rolling direction. When the test temperature was increased from room temperature to $400^{\circ}C$, the fatigue limit of both base metal and weld metal decreased substantially.