• 한국기계가공학회지
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• 제13권6호
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• pp.145-151
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• 2014

The glass used for mobile display windows is required to have high strength. Chemical strengthening by means of ion exchange is widely used glass. The depth of the layer and the compressed stress are affected by tempering temperature and time. The purpose of this study is to investigate the range of DOL and CS, which to less breakage during reliability tests such as the ball drop test, hole drop test, 3-point bending test, drop test, and tumble test with Soda-lime Glass.

• 열처리공학회지
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• 제14권1호
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• pp.27-34
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• 2001

The effects of pre-heat treatment(Q/T) on microstructure and hardness of STD11 and STD61 tool steel nitrided by micro-pulse plasma were investigated. The quenching temperature for obtaining matrix hardness of STD11 and STD61 steel on range of HRC 50 to HRC 60 desired for machine parts is about $1070^{\circ}C$ and $1020^{\circ}C$ respectively. The hardness of STD11 and STD61 quenched at the temperature was HRC 63 and HRC 56 respectively. The nitrided case depth of STD11 and STD61 nitrided at $550^{\circ}C$ for 5 hours was independent of pre-heat treatment condition and the depth was approximately $100{\mu}m$. However, hardness and compactness of nitrided layer on Q/T treated specimen were higher than the annealed specimen. The case depth increased linearly with the increase of nitriding temperature, however, the hardness of nitrided layer decreased with the increase of temperature. Phase mixture of ${\gamma}-Fe_4N$ and ${\varepsilon}-Fe_{2-3}N$ was detected by XRD analysis in the nitrided layer formed at the optimum nitriding condition. The optimum nitriding temperature was approximately $490^{\circ}C$ which was $10^{\circ}C$ lower than the tempering temperature for preventing softening behavior of STD11 and STD61 matrix during nitriding process and the surface hardness of nitrided layer obtained by optimum pre-heat treatment condition was about Hv1400.

• 열처리공학회지
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• 제30권3호
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• pp.117-126
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• 2017

The variation in microstructure and mechanical properties during heat treatment was examined in a series of 0.27% C-1.5% Mn-1.0% Cr steels with silicon contents in the range of 0 to 1.0 wt%. It was found that addition of 0.5%~1.0% silicon increased both tensile strength and impact toughness through solid solution strengthening and microstructural refinement. 0.27% C-1.0% Si-1.5% Mn-1.0% Cr steel showed tensile strength of 1,700 MPa in the as-quenched condition and the steel revealed a full martensitic structure even after air cooling from $900^{\circ}C$ to room temperature, showing air hardening characteristics. Tempering at $150^{\circ}C$ which corresponds to the typical paint-baking temperature after painting of body in white, slightly decreased the tensile strength and increased elongation, but substantially increased the impact toughness compared to the as-quenched steel.

• 한국결정학회지
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• 제1권1호
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• pp.29-34
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• 1990

할로겐 램프를 열원으로 하는 image furnace를 사용하여 소위 traveling solvent floating zone법에 의해 Mg TiO3(가이킬라이트) 고용체 단결정을 육성했다. 육성된 결정은 직경 8mm, 길이 100mm이였으며 성장측은(1010)이었다. MgTiO, 상은 고온에서 일정한 공용영역을 나타내고 있으며 완만한 속도로 냉각시키면 TiO, 성분이 결정학적 방위의 콘트롤을 받아 (0001)면에 평행하게 용출됨으로써 광채효과를 나타낸다. 육성된 boul은 검은색을 띠고 있으나 1100℃ 산소분위기에서 annealing시킬 경우 반투명한 단양한 색깔을 보여 준다. 따라서 가이킬라이트는 새로운 종류의 인공캣츠아이로 활용될 수 있다.

• 한국압력기기공학회 논문집
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• 제10권1호
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• pp.100-106
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• 2014

There is a growing need to introduce advanced pressure vessel steels with higher strength and toughness for the optimizatiooCn of the design and construction of longer life and larger capacity nuclear power plants. SA508 Gr.4N Ni-Cr-Mo low alloy steels have superior strength and fracture toughness, compared to SA508 Gr.3 Mn-Mo-Ni low alloy steel. Therefore, the application of SA508 Gr.4N low alloy steel could be considered to satisfy the strength and toughness required in advanced nuclear power plants. The purpose of this study is to characterize the microstructure and mechanical properties of SA508 Gr.4N low alloy steels. 1 ton ingot of SA508 Gr.4N model alloy was fabricated by vacuum induction melting followed by forging, quenching, and tempering. The predominant microstructure of the SA508 Gr.4N model alloy is tempered martensite having small packet and fine Cr-rich carbides. The yield strength at room temperature was 540MPa, and it was decreased with an increase of test temperature while DSA phenomenon occurred at around $288^{\circ}C$. Overall transition property of SA508 Gr.4N model alloy was much better than SA508 Gr.3 low alloy steel. The index temperature, $T_{41J}$, of SA508 Gr.4N model alloy was $-132^{\circ}C$ in Charpy impact tests, and reference nil-ductility transition temperature, $RT_{NDT}$ of $-105^{\circ}C$ was obtained from drop weight tests. From the fracture toughness tests performed in accordance with the ASTM standard E1921 Master curve method, the reference temperature, $T_0$ was $-147^{\circ}C$, which was improved more than $60^{\circ}C$ compared to SA508 Gr.3 low alloy steels.

• 한국해양공학회지
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• 제25권6호
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• pp.97-104
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• 2011

Modified C95600 bronze contains Fe component of 0.7 weight percentage besides Cu-7Al-2.5Si composition. The shape of centrifugal cast is a circular pipe with thick wall. Specimens machined from the centrifugal cast were quenched in oil after isothermal holding at a given heat treatment temperature in the range of $700{\sim}900^{\circ}C$. Mechanical properties and structural morphology are depended on the quenching heat treatment temperature regardless of isothermal holding time. Tensile strength or Brinell hardness is increased with increasing heat treatment temperature. The microstructure caused by quenching contains mixing phases of ${\alpha}+{\beta}'+FeSi+{\kappa}$ which martensite of ${\beta}'$ phase has been transformed from ${\beta}$ phase. Effect of isothermal holding temperature on mechanical properties in case of quenching heat treatment attributes to the change of volume fraction of ${\beta}'$ on the structural morphology. Mechanical characteristics of specimen, initially quenched from $850^{\circ}C$, and then tempered at $500^{\circ}C$, does not show an obvious softening indication, because disappearance of ${\beta}'$ during tempering process can be compensated by precipitation of brittle phase ${\gamma}$.

• 대한금속재료학회지
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• 제46권8호
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• pp.477-481
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• 2008

The secondary hardening and fracture behavior in P/M high speed steels bearing V content of 9 to 10 wt% have been investigated in terms of austenitizing temperature and precipitation behavior. Austenitizing was conducted at 1,100 and $1,175^{\circ}C$ of relatively low and high temperatures. Coarse primary carbides retained after austenitization were mainly V-rich MC type. They give a significant influence on hardeness and toughness, as well as wear resistance. Tempering was performed in the range of $500{\sim}600^{\circ}C$. The peak hardness resulting from the precipitation of the fine MC secondary carbides was observed near 520, irrespective of austenitizing temperature. Aging acceleration(or deceleration) did not occur with increasing austenitizing temperature because it mainly influences contents of V and C of matrix through the dissloution of coarse primary MC containing lots of V and C. The precipitation of secondary MC carbides, which also contain V and C, did not change the aging kinetics itself. In the 10V alloy containing much higher C content, the impact toughness was lower than 9V alloy, because of the larger amount of primary carbide and high hardness.

• International Journal of Automotive Technology
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• 제7권7호
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• pp.847-852
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• 2006

A fitting process carried out in the automobile transmission assembly line is classified into three classes; heat fitting, press fitting, and their combined fitting. Heat fitting is a method that applies heat in the outer diameter of a gear to a suitable range under the tempering temperature and assembles the gear and the shaft made larger than the inner radius of the gear. Its stress depends on the yield strength of a gear. Press fitting is a method that generally squeezes gear toward that of a shaft at room temperature by a press. Another method heats warmly gear and safely squeezes it toward that of a shaft. A warm shrink fitting process for an automobile transmission part is now gradually increased, but the parts (shaft/gear) assembled by the process produced dimensional change in both outer diameter and profile of the gear so that it may cause noise and vibration between gears. In order to solve these problems, we need an analysis of a warm shrink fitting process in which design parameters such as contact pressure according to fitting interference between outer diameter of a shaft and inner diameter of a gear, fitting temperature, and profile tolerance of gear are involved. In this study, an closed form equation to predict the contact pressure and fitting load was proposed in order to develop an optimization technique of a warm shrink fitting process and verified its reliability through the experimental results measured in the field and FEM, thermal-structural coupled field analysis. Actual loads measured in the field have a good agreement with the results obtained from theoretical and finite element analysis and also the expanded amounts of the outer diameters of the gears have a good agreement with the results.

• 한국정밀공학회지
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• 제23권9호
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• pp.54-60
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• 2006

Fitting process carried out in automobile transmission assembly line is classified into three classes; heat fitting, press fitting, and their combined fitting. Heat fitting is a method that heats gear to a suitable range under the tempering temperature and squeezes it toward the outer diameter of shaft. Its stress depends on the yield strength of gear. Press fitting is a method that generally squeezes gear toward that of shaft at room temperature by press. Another method heats warmly gear and safely squeezes it toward that of shaft. Warm shrink fitting process for automobile transmission part is now gradually increased, but the parts (shaft/gear) assembled by this process produced dimensional changes of gear profile in both radial and circumferential directions. So that it may cause noise and vibration between gears. In order to solve these problems, we need an analysis of warm shrink fitting process, in which design parameters are involved; contact pressure according to fitting interference between outer diameter of shaft and inner diameter of gear, fitting temperature, and profile tolerance of gear. In this study, an closed form equation to predict contact pressure and fitting load was proposed in order to develop optimization technique of warm shrink fitting process and verified its reliability through the experimental results measured in the field and FEM, that is, thermal-structural coupled field analysis. Actual loads measured in the field have a good agreement with the results obtained by theoretical and finite element analysis and also the expanded amounts of the gear profile in both radial and circumferential directions are within the limit tolerances used in the field.

• 대한기계학회논문집A
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• 제26권1호
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• pp.55-60
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• 2002

For the development of a new creep test technique, the availability of SP-Creep test is discussed for 1Cr-0.5Mo boiler header material. And some results are also compared with those of 2.25Cr- 1Mo steel which widely uses as boiler superheater tube. The results can be summarized as follows. The load exponents(n) obtained by SP-Creep test for 1Cr-0.5Mo steel are decreased with increasing creep temperature and the values are 15.67, 13.89, and 17.13 at 550$^{circ}C$ ,575$^{circ}C$ and 600$^{circ}C$, respectively. The temperature dependence of the load exponent is given by n = 107.19 - 0.1108T. This reason that load exponents show the extensive range of 10∼16 is attributed to the fine carbide such as M$_{23}$C$_{6}$ in lath tempered martensitic structures. At the same creep condition, the secondary creep rate of 1Cr-0.5Mo steel is lower than the 2.25Cr-1Mo steel1 due to the strengthening microstructure composed by normalizing and tempering treatments. Through a SEM observation, it can be summarized that the primary, secondary, and tertiary creep regions of SP-Creep specimen are corresponding to plastic bending, plastic membrane stretching, and plastic instability regions among the deformation behavior of four steps in SP test, respectively.y.