• 한국환경농학회지
• /
• 제16권3호
• /
• pp.264-268
• /
• 1997

식물이 토양미생물 유래 유기화합물의 선택적인 흡수에 주목하여 근권주위의 토양시료로부터 방선균을 중심으로 분리하였다. 방선균 K9301주 배양액에 식물유묘를 24시간 처리후하였다. 처리후의 배양액중의 하나의 대사산물이 소식됨을 알수 있었다. 이 대사산물은 벼뿐만 아니라 밀에서도 선택적으로 흡수되었다. TLC상의 Rf0.6의 대사산물 spot를 분리하였으며 2-aminobenzamide로 동정되었다.

• 약학회지
• /
• 제34권3호
• /
• pp.192-198
• /
• 1990

Three sugar glass dispersions of sulfamerazine were prepared using dextrose, galactose and sucrose as the carriers, with the ratio of the drug to the carrier was 1:9. The chemical stability of sulfamerazine in the glass dispersion system was studied using TLC. TLC revealed no additional spot and there was good correspondence with the Sulfamerazine itself. While time required to dissolve 50%($T_{50%}$) of sulfamerazine powder was 390 min that of dextrose glass dispersion system was 1.5 min. and galactose system was 4.0 min. in distilled water. 23) $T_{50%}$ of physical mixture with dextrose, galactose and sucrose were 26.4 min., 26.5 min., and 26.0 min. respectively in distilled water. $T_{50%}$ of control was 54 min. and those of all of the glass dispersion systems were within 1 min. in 0.1N HCl. The dissolution rates of sulfamerazine from sugar glass dispersion system in distilled water was greater than that in 0.1N HCl.

• 약학회지
• /
• 제45권2호
• /
• pp.169-179
• /
• 2001

In previous study, Gyrophora esculenta showed significant inhibitory effect on $\alpha$-glucosidases in vitro and blood glucose elevation in vivo. In the isolating process of active substance, orcinol was separated from Gyrophora esculenta. Orcinol is known to be toxic, therefore, in this study, it was analysed by the TLC densitometry method for quantitative determination from Gyrophora esculenta. The average amount of orcinol of Gyrophora esculenta was 0.2%. For the purpose of removing orcinol, the water extract of Gyrophora esculenta was sequentially fractionated by organic solvents, and the acute toxicity of each fraction was assessed in mice. Among them, the LD50 of butanol fraction was 1.19 g/kg(p.o.) and the weight increase of mice in that group was somewhat retarded.

• Journal of Applied Biological Chemistry
• /
• 제43권4호
• /
• pp.269-272
• /
• 2000

The ginseng growth-promoting bacterium Pseudomonas fluorescens KGPP 207 synthesized indole-3- acetic acid (IAA) from L-tryptophan, indole-3-pyruvic acid (IPyA), and indole-3-acetaldehyde (IAAld), but not from indole-3-acetamide (lAM) and other intermediates of various IAA biosynthetic pathways in the experiment with indole compound supplemented cell suspensions. TLC, HPLC, and GC-MS analyses revealed the presence of IPyA, indole-3-ethanol, indole-3-lactic acid and its methyl ester, IAA and its methyl, and ethyl esters in the culture supernatant of the bacterium. IAAld was detected in the supernatant using sodium bisulfite and TLC. The results indicate that unlike gall-forming bacteria which can synthesize IAA by lAM, the indole-3-pyruvic acid pathway is the route for IAA biosynthesis in this beneficial strain of P. fluorescens.

• 한국식품저장유통학회:학술대회논문집
• /
• 한국식품저장유통학회 2003년도 제23차 추계총회 및 국제학술심포지움
• /
• pp.136.1-136
• /
• 2003

Aristolochic acid has been known to be a carcinogenic compound and to cause Chinese herbs nephrophathy. To determine the content of aristolochic acid in various medicinal herbs marketed domestically, samples of Aristolochia fangchi, Aristolochia fructus, Aristolochia radix, Asiasari radix, Saussureae radix, and Akebia caulis were analyzed using TLC and HPLC. The optimal conditions for TLC and HPLC were established for the quantitative analysis of aristolochic acid. This study showed that Aristolochia fangchi and Aristolochia fructus examined in this study contain aristolochic acid of 3.9 and 2.3 mg/g sample, respectively. In contrast, aristolochic acid was not detected in other samples.

• 한국식품영양과학회지
• /
• 제6권1호
• /
• pp.66-71
• /
• 1977

An investigation of certain tar food colorants required a relatively inexpensive TLC adsorbent to be used in preparative thin-layer chromatography procedure. As will be shown activated clay and Kieselguhr has excellent physical characteristics for T LC applications, is easily applied, and is good for analytical work as well as showing good separator capabilities with selected groups of compounds. In addition to its usefulness its economical price suggested this article.

• 대한화학회지
• /
• 제18권5호
• /
• pp.368-372
• /
• 1974

Bombina Orientalis(무당개구리)의 복피로부터 추출한 암적색의 색소를 TLC, PLC(preparative thin layer chromatography) 및 column chromatography로 분리 및 정제하여 물리, 화학적 성질 visible 및 IR-spectral 특성을 이용하여 세번째주색소인 ${\alpha}$-cryptoxanthin(3-hydroxy-${\alpha}$-carotene)을 확인하였다

• 대한기계학회:학술대회논문집
• /
• 대한기계학회 2008년도 추계학술대회B
• /
• pp.2352-2356
• /
• 2008

Heat transfer and performance characteristics have been investigated for a rectangular wavy duct with dimple or protrusion arrays. The test duct was 15mm in height and 105mm wide. The print diameter of the dimple/protrusion wall was 12.99mm and the depth/height of the dimple/protrusion was 3.75mm. Local heat transfer coefficients on the dimple/protrusion wall were measured using a transient TLC technique. The Reynolds number was varied from 3,000 to 10,000. For the wavy duct tested in this study, adverse static pressure characteristics occurred at turning region of the wavy duct due to secondary flows. For the wavy duct with protrusion array, higher heat transfer enhancement level of 7.4 times than smooth straight case in maximum was obtained at low Reynolds number due to the high heat transfer enhancement by vortex flows. Also, the protrusion array increased the performance level of 3.0 at low Reynolds number of 3,000.

• 약학회지
• /
• 제55권4호
• /
• pp.289-294
• /
• 2011

Illegal addition of steroids into cosmetics, ointments or drugs have been increased and their careless usage induced detrimental effect on health. We developed simultaneous analytical method using TLC, HPLC and LC/MS for the identification of 40 corticosteroids. 34 corticosteroids were well separated in HPLC with isocratic mode and remaining 6 drugs were also separated with gradient mode. All of the 40 corticosteroids were detected in negative mode in LC/MS. Halcinonide, prednisolone, triamcinolone acetonide and methylprednisolone hemisuccinate were detected in real samples.

• ETRI Journal
• /
• 제8권3호
• /
• pp.29-43
• /
• 1986

어떤 고장이 시스팀의 기능을 완전히 마비시키는 것이 아니라 그 성능이 저하된 상태에서 운용할 수 있는 degradable system에서는 고전적인 신뢰도 모형을 적용하기가 어려우며, 여기서 성능과 신뢰도는 매우 밀접한 관련이 있다. 본고에서는 성능신뢰도(Performance reliability)에 대한 개념 및 모형화 방법에 대해 살펴보고 실제로 TDX-1의스위치 네트워크인 SWCD의 성능을 해석하여 성능신뢰도를 구하였다. SWCD의 성능척도인 통화성공률에 영향을 미치는 요인으로는 스위치 네트워크 내에서의 blocking, T-SW 및 S-SW의 고장, 그리고 T-SW 및 S-SW의 고장으로 인해 DLC 와 TLC의 가용한 서비스 채널이 감소함으로써 발생하는 DLC 및 TLC에서의 blocking등을 들 수 있는데 이 요인들을 고려하여 SWCD의 성능을 해석하였으며, SWCD에 요구되는 표준성능(Normalized performance) 이 0.99라 할 때 single unit라고 가정한 경우 SWCD의 성능 신뢰도는 MTUO(Mean Time to Unreliable Operation)가 3076.7시간이었다. 또한 성능을 해석하는 과정에서 디지틀 스위치 네트워크인 SWC만의 최대 발신 통화처리 용량을 구한 결과, 스위치 네트워크 내에서의 blocking 확률에 대한 최대 허용치를 $10^-3$으로 하였을 때 약 1,700Erlang이었다.