• Title/Summary/Keyword: TEM Journal

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Evaluation of C. Albicans and S. Mutans adherence on different provisional crown materials

  • Ozel, Gulsum Sayin;Guneser, Mehmet Burak;Inan, Ozgur;Eldeniz, Ayce Unverdi
    • The Journal of Advanced Prosthodontics
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    • v.9 no.5
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    • pp.335-340
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    • 2017
  • PURPOSE. Bacterial adhesion on provisional crown materials retained for a long time can influence the duration for which permanent prosthetic restorations can be healthily worn in the oral cavity. The aim of this study was to compare seven different commonly used provisional crown materials with regard to Streptococcus mutans and Candida albicans surface adhesion. MATERIALS AND METHODS. For each group, twenty specimens of the provisional fixed prosthodontic materials TemDent ($Sch{\ddot{u}}tz$), Imident (Imicryl), Tab 2000 (Kerr), Structur Premium (Voco), Systemp (Ivoclar Vivadent), Acrytemp (Zhermack), and Takilon-BBF (Takilon) were prepared (diameter, 10.0 mm; height, 2.0 mm). Surface roughness was assessed by atomic force microscopy. Each group was then divided into 2 subgroups (n=10) according to the microbial suspensions used: S. mutans and C. albicans. The specimens were incubated at $37^{\circ}C$ with S. mutans or C. albicans for seven days. Bacterial adherence on surfaces was assessed using the 2,3-bis[2-methyloxy-4-nitro-5-sulfophenyl]-2H-tetrazolium-5-carboxanilide (XTT) assay. RESULTS. S. mutans showed maximum adhesion to Structur, followed by Systemp, Acrytemp, Takilon, Tab 2000, Imident, and TemDent (P<.05). The highest vital C. albicans adhesion was noted on Takilon, followed by Imident and Tab 2000; the lowest adhesion was noted on Systemp (P<.05). CONCLUSION. The materials showed significant differences in the degree of bacterial adhesion. C. albicans showed higher surface adhesion than S. mutans on provisional crown and fixed partial denture denture materials.

Nano-Sized Mullite(3Al2O3.42SiO2) Colloids Fabricated by Spray Combustion Synthesis (SCS) Technique (분무연소합성(SCS)법에 의한 나노크기 물라이트(3Al2O3.42SiO2) 콜로이드 제조)

  • Lee, Sang-Jin;Jun, Byung-Sei
    • Journal of the Korean Ceramic Society
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    • v.41 no.4
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    • pp.297-301
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    • 2004
  • Nano-sized mullite (3Al$_2$O$_3$$.$2SiO$_2$) colloids were prepared by use of the spray combustion method. For combustion reaction, Al(NO$_3$)$_3$$.$9$H_2O$, and CH$_{6}$N$_4$O were used as an oxidizer and a fuel respectively, and then colloidal silica was also added as 2SiO$_2$source for mullite. The temperature of the reaction chamber was kept at 80$0^{\circ}C$ to initiate the ignition of droplets of the mixed precursors. For preventing droplet coagulation, the droplet number concentration was reduced using the metal screen filter, and the residence time of aerosol was kept at 2.5 seconds for laminar flow. The synthesized colloidal particles had an uniform spherical shape with 130 nanometer size and the crystalline phase showed the mullite with stoichiometry in the observations of XRD and TEM.

Preparation of Mullite Precursor Using Silicic Acid Extracted by Tetrahydrofuran from Sodium Silicate (규산나트륨으로부터 Tetrahydrofuran으로 추출된 규산을 이용한 Mullite 전구체 제조)

  • 노재성;홍성수;이범재;이병기;박은희;정홍호
    • Journal of the Korean Ceramic Society
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    • v.33 no.8
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    • pp.915-920
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    • 1996
  • Fine mullite precursor was prepared by colloidal sol-gel processes. Aluminum isopropoxide $[Al(i-OC_3H_7)_3]$ as a starting material of $Al_2O_3$ and silicic acid extracted by THF from sodium silicate as a starting material of $SiO_2$ were used. Sodium silicate was first acidified by dilute sulfuric acid to form silicic acid. ; followed by extraction using THF, Mullite precursor was synthesized by sol-gel processes from aluminum isopropoxide and sillicic acid considering the degree of extraction of Si and the removal efficiency of Na. The impurity content of silicic acid extracted by THF was below 0.04% Synthetic mullite precursor consisted of $3Al_2O_3{\cdot}2SiO_2$ and showd spherical particles of $0.05{\mu}m$ diameter and below 0.462% of impurites. The mullite precursor was characterized by EDS, XRD, TG/DSC SEM, FT-IR spectroscopy ICP and TEM.

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Phase transition of indium hydroxide to indium oxide at low temperatures (저온에서의 indium hydroxide에서 indium oxide로의 상전이)

  • Choi, Eun-Kyoung;Lee, Won-Jun;Han, Kyu-Sung;Kim, Ung-Soo;Kim, Jin-Ho;Hwang, wang-Teak;Hwang, Hae-Jin;Shim, Kwang-Bo;Cho, Woo-Seok
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.28 no.2
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    • pp.91-97
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    • 2018
  • Indium hydroxide powder was prepared by precipitation method. The reaction temperature ($150{\sim}250^{\circ}C$) and the holding time at each reaction temperature (1~72 h) were used as experimental variables. The particle size, microstructure and crystal phase of each prepared powder were observed through X-ray diffraction (XRD), Transmission electron microscope (FE-TEM) and BET. In this study, we investigated the phase and microstructural change induced by heat treatment of indium hydroxide nanoparticles at various temperatures for different holding times.

Transmission Line Parameter Extraction and Signal Integrity Verification of VLSI Interconnects Under Silicon Substrate Effect (실리콘 기판 효과를 고려한 VLSI 인터컨넥트의 전송선 파라미터 추출 및 시그널 인테그러티 검증)

  • 유한종;어영선
    • Journal of the Korean Institute of Telematics and Electronics C
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    • v.36C no.3
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    • pp.26-34
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    • 1999
  • A new silicon-based IC interconnect transmission line parameter extraction methodology is presented and experimentally examined. Unlike the PCB or MCM interconnects, a dominant energy propagation mode in the silicon-based IC interconnects is not quasi-TEM but slow wave mode(SWM). The transmission line parameters are extracted taking the silicon substrate effect (i.e., slow wave mode) into account. The capacitances are calculated considering silicon substrate surface as a ground. Whereas the inductances are calculated by using an effective dielectric constant. In order to verify the proposed method, test patterns were designed. Experimental data have agreement within 10%. Further, crosstalk noise simulation shows excellent agreements with the measurements which are performed with high-speed time domain measurement ( i.e., TDR/TDT measurements) for test pattern, while RC model or RLC model without silicon substrate effect show about 20~25% underestimation error.

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Leaky Wave Radiation and Surface Wave Launching Problem in a Dielectrically Covered Periodically Slitted Parallel-Plate Waveguide (주기적인 슬릿을 갖고 유전체층으로 덮힌 평행평판 도파관에서의 누설파 복사 및 표면파 launching)

  • 이종익;이철훈;조영기
    • Journal of the Korean Institute of Telematics and Electronics D
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    • v.36D no.4
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    • pp.25-33
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    • 1999
  • Leaky wave radiation and surface wave launching problems in a dielectrically covered and periodically slitted parallel-plate waveguide(PPW) are considered for the TEM wave incidence case. Both the infinite and finite periodic geometries are analyzed by use of the method of moments. Some numerical results for the reflected and transmitted powers in the PPW, radiation efficiency into the free space, surface wave launching efficiency into the slab, antenna gain, and radiation patterns against dielectric thickness are presented to show the effect of the dielectric cover on the performances of the slitted leaky wave antenna. In addition, the method for improving surface wave launching efficiency using the proposed periodic geometry is described and maximum launching efficiency of 97.5% is obtained theoretically. So this structure is thought to be promising as an efficient feeder of dielectric grating antenna as well as image guide.

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The Comparative Study of Koanbok between the koryo and Sung Dynasty (고려시대와 송대의 관복 비교연구 - 공.상복을 중심으로 -)

  • 서옥경
    • Journal of the Korean Society of Costume
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    • v.31
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    • pp.131-144
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    • 1997
  • This thesis is mainly on the study of Gongbok and Sangbok in the system of official outfit of the Koryo dyn-asty which has not yet fully studied in the history of Koren dress and its ornaments. Even in this difficult circumstances the sys-tem of dress and its ornaments can be under-stood with the help of remaining Buddhi-stliterature. Thus the system of official outfit in the Koryo dynasty has been studied here with some documentary records such as Koryo-dokyung Koryosa-yeobokji (The His-tory of Dress And Its Ornaments in The Koryo Dynasty) and so on. As the Koryo dynasty de-veloped her international relationships continu-ously with her neighbouring nation which were geographically closely connected so the systems of official outfit in the Chinese dyn-asty of Sung had to be studied and compared with, In the Koryo dynasty the same four colour system of purple red, deep red and green had survived until the year of 1123 from the year of 960 not using the blue colour from the four colour system of purple Chinese red green and blue of the Sung dynasty. The four colour system of purple deep red green and black under the regin of the King Euijong was exactly the same as that of official outfit of the Sung dynasty in he year of 1078 the first year of Wonpung's regin and wearing Eodae is a sure sign of influence of the system of Sung dynasty. Even though Koryo was invaded by Yuan druing the period of the regin of the King Chungyul the four colour system was not changed of purple deep red. green and black along with the same Dae-sudanryung(long sleeve and round collar). In 1387 the thirteenth year of the King Woo of the Koryo dynasty Pumdae was used ofor different official ranks and the sys-tem of wearing Samo and Dayung was established for the official outfit of every government officers.

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Degradation of Soft Magnetic Properties of Fe-Hf-N Films After Annealing (Fe-Hf-N 박막의 열처리 후 연차기특성 열화)

  • 제해준;박재환;김영환;김병국
    • Korean Journal of Crystallography
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    • v.12 no.3
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    • pp.182-187
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    • 2001
  • The purpose of this study is to investigate the degradation of soft magnetic properties of Fe-Hf-N thin films after annealing in vacuum. They were annealed at 450℃∼650℃. The microstructure and crystal phase of the selected area of the thin films were analyzed by TEM and SAD. After annealing at 450℃-600℃, the coercivity of the films increased by 0.2 Oe and the effective permeability decreased by 1500 as compared with them before annealing due to the growth of α-Fe crystallites. The saturation magnetic flux density of the films increased by 0.5 KG after annealing under 600℃. However, the soft magnetic properties of the film annealed at 650℃ degraded abruptly, which was attributed to the destruction of nano-crystalline microstructure of the film due to the rapid growth of α-Fe crystallites with the segregation of N sited in the α-Fe lattice into HfN.

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The Effect of Composition and Current Condition on Magnetic Properties of Co-Fe-Ni Soft Magnetic Alloy (합금 조성과 전류조건이 CoFeNi 3원계 합금의 자기특성에 미치는 영향)

  • Jeung, Won-Young;Kim, Hyun-Kyung;Lee, Jeong-Oh
    • Journal of the Korean Magnetics Society
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    • v.15 no.4
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    • pp.241-245
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    • 2005
  • CoFeNi alloys are some of the most studied soft magnetic materials because of their applications as write-head core materials in HDD and MEMS. Ternary CoFeNi films with high saturation magnetic flux density, Bs and low coercivity, He were successfully grown by electrodeposition. The optimal composition was $Co_{30}\;Fe_{34}\;Ni_{36}(at\%)$, and Bs and Hc were 1.9 T and 0.16 A/m, respectively. The XRD and TEM results show that the low Hc of the CoFeNi films was due to very fine crystal particles and mixed fcc and bcc phases.

Molecular Approaches to Determine the Character of Serratia marcescens Associated with the Insect Pathogenicity to Brown Planthopper (Serratia marcescens의 곤충 병원성 관련형질 탐색을 위한 분자생물학적 연구)

  • 김희규;배동원;박진희;윤한대
    • Korean journal of applied entomology
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    • v.32 no.3
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    • pp.330-337
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    • 1993
  • A bacterium, pathogenic to Nilaparvata lugens Stal. causing high mortality in 3~5 days, were selected and identified as Serratuz marcescens biotype A2a which is not a nosocomlally infective strain. In order to determine the characters of Serratia marcesce'1lS associated with insect pathogenicity, Tn5 mutagenesis was carried out by conjugating with E. coli pJB4J1. Transconjugants were plate-assayed for missing chitinase, protease and DNase activity. A protease negative mutant was selected for missing JOseet pathogenicity. SEM and TEM revealed the presence of bacterial cells in the epithelial tissue of inner abdomal tissue of the hypodermic layer of abdomen. Such a colonization was limmited to the subjacent tissue inside the intacL cuticular epidermis. These observation supported our result of pathogenicity tests of transconjugants.

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