• Title/Summary/Keyword: TEM Journal

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Ultrashort Pulsed Laser Machining for Biomolecule Trapping

  • Choi, Hae-Woon;Farson, Dave F.;Lee, L.James;Lee, Ho
    • Journal of the Optical Society of Korea
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    • v.13 no.3
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    • pp.335-340
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    • 2009
  • Ultrashort pulse laser drilling of polycarbonate track-etched membrane (pTEM) material was used to fabricate a mouse embryo cell trapping device. Holes with a diameter of $2{\mu}m$ to $5{\mu}m$ were fabricated on a $10{\mu}m$ thick membrane using a femtosecond laser with a 150 fs pulse width and 775 nm wavelength and multiple-pulse irradiation. In cell trapping tests, the overall cell occupancy of the machined holes in the fabricated pTEM was found to be more than 80%. The results of a single pulse and multiple pulse irradiation were compared in terms of the surface quality. It was generally found that a single pulse with high energy was less desirable than irradiation with multiple pulses of lower energy.

Evaluation of Elevated Temperature Strength of Al-Cr-Zr Alloys Strengthened by Nanostructured Crystallines and Intermetallic Compounds (I) (나노 결정립과 금속간화합물상에 의해 강화된 고온, 고강도 Al-Cr-Zr 합금개발 및 특성평가 (I))

  • 양상선
    • Journal of Powder Materials
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    • v.6 no.1
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    • pp.49-55
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    • 1999
  • Al-Cr-Zr nanocomposite metal powders were prepared by mechnical alloying (MA) in order to develop aircraft structure materials with lighter weight and lower cost than the conventional Ti and Ni alloys. The morphological changes and microstrutural evolution of Al-6wt.%Cr-3wt.%Zr nanocomposite metal powders during MA were investigated by SEM, XRD and TEM. The approximately 50$\mu$m sized Al-Cr-Zr nanocomposite metal powders has been formed after 20 h of MA. The individual X-ray diffraction peaks of Al, Cr and Zr were broadened and peak intensitied were decreased as a function of MA time. The observed Al crystallite size by TEM was in the range of 20 nm, which is a simliar value calculated by Scherrer equation. The microhardness of Al-Cr-Zr nanocomposite metal powders increases alomost linearly with increase of the processing time, reaching a saturation hardness value of 127 kg/$mm^2$ after 20 h of processing. The intermetallic compound phase of $Al_3Zr_4$ in the matrix was identifed by XRD and TEM.

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Probe Design and Fabrication for Measuring Near Field (근역장 측정용 프로브의 설계 및 제작)

  • 김병찬;최형도;이애경;이형수
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.13 no.2
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    • pp.164-169
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    • 2002
  • This paper reports on design and fabrication of near field probe operating at 300~3000 MHz. Design parameters are extracted by equivalent circuit of E-field probe and simulation using S parameter is performed to predict probes performance. The probe consists of a dipole antenna with 3.25 mm length, a zero bias Schottky diode and a highly resistive transmission line. A TEM cell was used for performance evaluation.

Heat Radiation of Multichip 10W LED Light Using Thermoelectric Module(TEM) (열전소자를 이용한 10W급 멀티칩 LED조명의 방열)

  • Cho, Young-Tae
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.21 no.1
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    • pp.46-50
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    • 2012
  • This paper amis at improving the heat radiation performance of thermoelectric module (TEM) for a commercialization of high-powered LED light with using a multichip LED module. In addition, a 10W multichip LED light was prepared for the heat performance on radiating of which LED light was made for a use of testing by the driving of the thermoelectric module. So, it was found that about 30% in the effect of temperature reduction was confirmed if compared with the radiation heat by heat sink only.

TEM Characterization of Oxide Films Formed on Al1050 and Al7075 Alloys under Atmospheric Corrosion Conditions (대기 부식에 의해 생성된 Al1050 및 Al7075 알루미늄 합금 산화막에 대한 투과전자현미경 분석)

  • Kim, Sungyu;Lee, Chanhyeong;Bahn, Chi Bum
    • Journal of Surface Science and Engineering
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    • v.50 no.6
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    • pp.447-454
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    • 2017
  • Al1050 and Al7075 alloy specimens were exposed to atmospheric conditions for maximum 12 months and analyzed by Transmission Electron Microscopy (TEM) to characterize the early-stage corrosion behavior and thin surface oxide layers. By comparing of oxide films between Al1050 and Al7075 alloys, it is concluded that Al7075 has a relatively thicker surface oxide film than Al1050 but Al1050 has relatively more significant oxygen penetration through grain boundaries. The oxygen penetration through grain boundaries appeared to be influenced by intermetallic particles at the grain boundary. In the case of aluminum alloys, localized corrosion like pitting or intergranular corrosion should be considered as well as uniform corrosion when estimating the atmospheric corrosion rate.

Heat Transfer Analysis for Optimum Design of a Thermoelectric Cooler (열전 냉각기의 최적 설계를 위한 열전달 해석)

  • 김제익;박찬형;강용태;최창균
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.15 no.11
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    • pp.889-894
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    • 2003
  • The objectives of this study are to present a proper mathematical model for a thermoelectric cooler equipped with the spacer and to investigate the effect of its geometries by heat transfer analysis. In order to enhance the efficiency of the thermoelectric cooler, the spacer is inserted between TEM (thermoelectric module) and cold plate. The theoretical results show that the COP (coefficient of performance) increases nonlinearly as high as 0.63 with increasing the depth of spacer and the depth of TEM and with decreasing the area of insulator.

Observation of Defects in the Alpha-Alumina Single Crystal by TEM and REM Techniques (투과전자현미경(TEM)과 반사전자현미경법(REM)을 이용한 알루미나 단결정내의 결함들에 관한 관찰)

  • Kim, Yootaek
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.3 no.2
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    • pp.131-139
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    • 1993
  • Transmission electron microscopy( lEM) technique which is useful for investigating the crystalline structure and defects, and reflection electron microscopy( REM) of which technique has very high sensitivity of detecting the defects on the crystal surfaces were applied to study the behaviour of dislocations and twins in or on the $a- AI_20_3$ single crystals.

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Effect of Preparation Method for Pd/C Catalysts on Pd Characterization and their Catalytic Activity (Pd/C 촉매 제조 방법에 따른 Pd 금속의 특성 및 촉매 활성)

  • Kim, Ji Sun;Hong, Seong-Soo;Kim, Jong-Hwa;Lee, Man Sig
    • Applied Chemistry for Engineering
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    • v.26 no.5
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    • pp.575-580
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    • 2015
  • Pd/C catalysts were prepared by various preparation methods such as ion exchange, impregnation and polyol method and also characterized by nitrogen adsorption-desorption isothermal, XRD, FE-TEM and CO-chemisorption. The activities of these catalysts were tested in the hydrogenation of cyclohexene to cyclohexane. Catalytic activities of Pd/C catalysts were found to be effected by the chosen preparation methods. Pd dispersions of each Pd/C catalysts prepared by ion exchange, impregnation and polyol method were 17.55, 13.82% and 1.35%, respectively, confirmed by CO-chemisorption analysis. These were also in good agreement with the FE-TEM results. The Pd/C catalyst prepared by ion exchange method exhibits good performance with the cyclohexene conversion rate of 71% for 15 min. These results indicate that Pd/C catalyst having higher dispersion and lower particle size is in favor of hydrogenation cyclohexene and also Pd dispersion increases with the increment of catalytic activity.

Measuring the Tensile Properties of the Nanostructure Using a Force Sensor (힘센서를 이용한 나노구조체의 인장물성 측정)

  • Jeon, Sang-Gu;Jang, Hoon-Sik;Kwon, Oh-Heon;Nahm, Seung-Hoon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.34 no.2
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    • pp.211-217
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    • 2010
  • It is important to measure the mechanical properties of nanostructures because they are required to determine the lifetime and reliability of nanodevices developed for various fields. In this study, tensile tests for a multi-walled carbon nanotube (MWCNT) and a ZnO nanorod were performed in a scanning electron microscope (SEM). The force sensor was a cantilever type and was mounted in front of a nanomanipulator placed in the chamber. The nanomanipulator was controlled using a joystick and personal computer. The nanostructures dispersed on the cut area of a transmission electron microscope (TEM) grid were gripped with the force sensor by exposing an electron beam in the SEM; the tensile tests were the performed. The in situ tensile loads of the nanostructure were obtained. After the tensile test, the cross-sectional areas of the nanostructures were observed by TEM and SEM. Based on the TEM and SEM results, the elastic modulus of the MWCNT and ZnO nanorod were calculated to be 0.98 TPa and 55.85 GPa, respectively.