• Title/Summary/Keyword: T6 Heat Treatment

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Effect of Heat Treatment Conditions on the Microstructure and Wear Behavior of Ni-based Self-flux Alloy Coatings (니켈기 자융성 합금 코팅층의 미세구조 및 마모거동에 미치는 후열처리 조건의 영향)

  • Kim, K.T.;Oh, M.S.;Kim, Y.S.
    • Journal of Power System Engineering
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    • v.11 no.1
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    • pp.121-126
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    • 2007
  • This study aims at investigating the effect of heat treatment conditions on the dry sliding wear behavior of thermally sprayed Ni-based self-flux alloy coatings. Ni-based self-flux alloy powders were sprayed onto a carbon steel substrate and then heat-treated at 700, 800, 900 and $1000^{\circ}C$ for 30 minutes in a vacuum furnace. Dry sliding wear tests were performed using sliding speed of 0.4 m/s and applied load of 6 N. AISI 52100 ball(diameter 8 mm) was used as counterparts. Microstructure and wear behavior of both as-sprayed and heat-treated Ni-based self-flux alloy coatings were studied using a scanning electron microscope(SEM), energy dispersive X-ray spectroscopy(EDX), electron probe micro-analysis(EPMA) and X-ray diffraction(XRD). It was revealed that microstructure and wear behavior of thermally sprayed Ni-based self-flux alloy coatings were much influenced by heat treatment conditions.

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Ablation Characteristics of Bovine Liver According to Cool-Tip Temperature of RFA Equipment (고주파 열치료 장비의 Cool-Tip 온도에 따른 소간의 소작 특성)

  • Choi, Young-Jae;Kim, Jeong-Koo
    • Journal of radiological science and technology
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    • v.38 no.2
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    • pp.155-161
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    • 2015
  • This study confirmed the correlation between the change of the cooling water in internal cooling system and the size of the ablation site of bovine liver in RF heat treatment equipment. The bovine liver was resection with $4{\times}4{\times}4cm^3$ in 2cm cool-tip and with $6{\times}6{\times}6cm^3$ in 3cm cool-tip for the experiments. Area and perimeter of the ablation site for bovine liver were measured by Freehand techniques of MRI. It showed area and perimeter decreased during cool-tip temperature rises 6 and 12 minutes ablation using a 2cm and 3cm cool-tip. The correlation of cool-tip temperature and area and perimeter was statistically significant the result are shown(p=.000). The measurements of area and perimeter were more accurate with MRI in actual measurements and MRI for ablation range. The statistical results using Paired sample T-test was also significant(p=.038). The ablation range of bovine liver decreased according as cooling water temperature increases in RF heat treatment equipment for reason of carbonization occurred due to does not accurately pass the RF energy. Therefore, it is considered the effect of RF heat treatment would be increased if the temperature of the cooling water consistently maintain the low temperature in order to reduce the generation of carbide at RF heat treatment and RF energy is delivered accurately.

Creep Characteristics of Ti-6Al-4V Alloy Surface Modified by Plasma Carburized/CrN Coating (복합처리(Carburized/CrN Coating)로 표면개질된 Ti-6Al-4V합금의 크리프 특성)

  • Park, Yong-Gwon;Park, Jung-Ung;Wey, Myeong-Yong
    • Journal of the Korean Society for Heat Treatment
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    • v.18 no.3
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    • pp.183-189
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    • 2005
  • The effects of duplex-treatment of plasma carburization and CrN coating onto Ti-6Al-4V alloy on its creep properties were investigated by means of a constant stress creep tester. Applying duplex-treatment, specimens having an inner carburized layer of about $150{\mu}m$ in depth and outer CrN layer of about $7.5{\mu}m$ in thickness were prepared. The hardness of duplex-treatment surface was about 1,960 VHN. It also appeared that the duplex-treatment improved the roughness of the surface significantly; $Ra=0.045{\mu}m$ for treated alloy while $Ra=0.321{\mu}m$ for untreated alloy. The steady-state creep behaviors were investigated in a temperature range of $510{\sim}550^{\circ}C$ ($0.42{\sim}0.44T_m$) under an applied stress range of 200~275 MPa. The stress exponent, n, was derived assuming the power law creep behavior. The surface treatment showed a decrease in a value from 9.32 (untreated) to 8.79 (treated). Also the activation energy obtained from an Arrhenius plot increased from 238 to 257 kJ/mol.

Effect of Sr and (Ti-B) Additives on Tensile Properties of AC4A Recycled Aluminum Casting Alloys (재활용 AC4A 알루미늄 합금의 인장특성에 미치는 (Ti-B), Sr 첨가제의 영향)

  • Oh, Seung-Hwan;Kim, Heon-Joo
    • Journal of Korea Foundry Society
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    • v.38 no.5
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    • pp.87-94
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    • 2018
  • The effects of Sr and (Ti-B) additives on the tensile properties of AC4A recycled (35% scrap content) aluminum alloys were investigated. An acicular morphology of the eutectic Si phase of as-cast specimens was converted to a fibrous morphology upon the addition of Sr. Moreover, morphology of the Sr modified eutectic Si phase became finer due to a T6 heat treatment. The grain size of the ${\alpha}$-solid solution was decreased by the addition of (Ti-B) additives. Depending on the treatment conditions of the as-cast specimens, i.e., no addition, a Sr addition and a (Ti-B)+Sr addition, the tensile strength levels of the as-cast specimens were 182, 192, and 204MPa, respectively. The corresponding strengths of T6 heat-treated specimens were 293, 308, and 318MPa. Elongations of the as-cast specimens were 2.2, 3.1, and 5.6%, and the corresponding elongations of the T6 heat-treated specimens were 4.6, 6.1, and 7.6%. The percentage of the reduced section area in the tensile specimens was also increased by the Sr and (Ti-B) additives. Sr and (Ti-B) additives changed the microstructure and the distribution of defects in the castings, resulting in an improvement of the tensile properties of AC4A aluminum alloys. According to our test results, recycled (35% scrap content) AC4A aluminum alloy met all of the KS requirements of the tensile strength and elongation values of AC4A aluminum alloy except for the elongation value of the one specimen condition, in this case the as-cast no-addition condition.

Structural Analysis of Differential Gear System for Balancing Module Design (Balancing 모듈 설계를 위한 Differential Gear System의 구조해석에 관한 연구)

  • Jang, T.H.;Kim, D.J.;Moon, C.H;Lee, S.J.;Kim, T.G.
    • Journal of the Korean Society for Heat Treatment
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    • v.32 no.6
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    • pp.270-274
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    • 2019
  • In this study, simulation structure analysis was performed for the differential gear system for passenger cars as a prerequisite for the design of the balancing module. The differential gear system was modeled by using CATIA and simulation structure analysis was performed using ANSYS software. The material of the modeled differential gear system uses the mechanical properties of S45C (Q&T). In the structural analysis of the differential gear, the areas where the maximum stress and the maximum strain occurred can be identified. The maximum stress and maximum strain occurred in the pitch circle of the bevel gear. In evaluating the safety factor, it was found that sufficient safety factor was secured. Based on the analysis results for the differential gear, it is expected that it will be a good reference if we design the balancing module device.

RRA Treatment of Semi-Solid Al-Zn-Mg-Cu Al Alloy Fabricated by Cooling Plate (냉각판으로 제조된 Al-Zn-Mg-Cu계 반응고 알루미늄 합금의 RRA 처리)

  • Kim, Dae-Hwan;Shim, Sung-Yong;Kim, Young-Hwa;Lim, Su-Gun
    • Journal of Korea Foundry Society
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    • v.29 no.6
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    • pp.265-269
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    • 2009
  • The optimum RRA heat treating conditions and SCC (stress corrosion cracking) resistance of semi-solid Al-Zn-Mg-Cu alloy fabricated by inclined cooling plate were compared with those of conventional mould cast alloys. The non-stirring method characterized by using a cooling plate can effectively eliminate dendritic structure and form a fine globular semisolid microstructure in as-cast Al-Zn-Mg-Cu alloy and the SCC resistance of semi-solid Al-Zn-Mg-Cu alloy was higher than that of conventional mold cast alloy. Also, after retrogressed treatment at RRA heat treatment of semi-solid Al-Zn-Mg-Cu alloy, retrogressed treatment time has increased more than 10 minutes at $180^{\circ}C$ to recovery the T6 heat treatment strength.

The effects of aluminium contents on the mechanical properties of magnesium-aluminium alloy (Mg-Al계 합금의 기계적 성질에 미치는 Al의 영향)

  • Maeng, W.Y.;Bac, J.H.;Oh, I.S.;Nam, T.W.
    • Journal of the Korean Society for Heat Treatment
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    • v.7 no.2
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    • pp.139-146
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    • 1994
  • In the molten state, magnesium alloys vigousey react with oxygen in the air, is protected from oxidation and burning by the addition of $SF_6$ to $CO_2$ atmosphere over the melt. The mechanical properties and metallographic examinatin have made of Mg-Al alloys containing 3, 6, 9% in the solution treated state and precipitated state, comparing mechanical properties obtained during unidirectional solidification with me chanical properties obtained during conventional casting. For a given solution treatment, a higher aluminum contents produce more or less fine grains in conventional casting. For a given artifical aging treatment, a higher aluminum contents produces much precitates at the grain boundary as well as within the grain in unidirectional solidification. As a result of this experiment, for a given heat treatment, the higher is aluminum contents the higher is the ultimate tensile strength, yield strength, hardness while the lower the elongation. Also the mechanical properties of unidirectional solidification is larger than that of conventional casting.

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Effects of Ca, Si on the Microstructure and Aging Characteristic of AZ91 Alloy (AZ91합금의 조직(組織)과 시효특성(時效特性)에 미치는 Ca 및 Si의 영향(影響))

  • Jhee, T.G.;Kim, Y.K.
    • Journal of the Korean Society for Heat Treatment
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    • v.15 no.6
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    • pp.260-268
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    • 2002
  • The effects of calcium and silicon on microstructure and aging characteristics of AZ91 magnesium alloy during T5 treatment was investigated. The addition of 0.88% calcium or 0.25% silicon to AZ91 alloy made dendrite cell smaller. Especially, silicon is more effectively acted as refinement of the dendrite cell than calcium. It is due to that $Mg_2Si$ precipitated at the dendrite cell boundary or in the matrix during T5 treatment of Si added AZ91 alloy retarded the growth of the secondary phase. In the mean while, without inducing the precipitates containing calcium, calcium was segregated mainly around secondary phase such as $Mg_{17}Al_{12}$ and partially dissolved in ternary eutectic (Mg-Al-Ca) structure. In the AZ91 alloy containing both silicon and calcium, more finely distributed $Mg_2Si$ in matrix homogeneously and much finer microstructure were obtained than those containing silicon or calcium. Hence, An AZ91 containing both silicon and calcium was more effective to retarding the growth of the secondary phase than the other AZ91 alloy such as AZ91 alloy containing silicon or AZ91 alloy containing calcium.

Aging Behaviors of a Rapidly Solidified AI-Li-Cu Alloy (급냉응고된 Al-Li-Cu 합금의 시효거동)

  • Hong, Y.J.;Kim, S.H.;Kang, M.C.;Kim, I.B.
    • Journal of the Korean Society for Heat Treatment
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    • v.6 no.3
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    • pp.138-143
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    • 1993
  • Effects of aging treatment on the microstructural evolution of a rapidly solidified Al-Li-Cu alloy were investigated by differential scanning calorimetry (DSC) and transmission electron microscopy(TEM). It was found that the precipitation sequence was: supersaturated solid solution ${\alpha}^{\prime}$ ${\rightarrow}$ metastable ${\delta}^{\prime}$ + stable precipitate $T_1$ ${\rightarrow}$ stable precipitates ${\delta}+T_1$. Two exothermic and two endothermic peaks are detected by DSC analysis. The two exothermic and endothermic peaks corresponded to ${\delta}^{\prime}$ and ${\delta}+T_1$ precipitation and dissolution reactions respectively. The enthalpy of ${\delta}^{\prime}$ precipitation decreased with increasing of aging temperature and time until the finishing point of precipitation. The activation energy for precipitation of ${\delta}^{\prime}$ was measured as 80KJ/mol and the energy for dissolution was 93KJ/mol. These values arc higher than those of AI-Li binary alloy. Peak hardness value (Hv 170) was obtamed at $210^{\circ}C$ for 1hr aging treatment which coincided with finishing point of ${\delta}^{\prime}$ precipitation.

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Enhanced compatibility and initial stability of Ti6Al4V alloy orthodontic miniscrews subjected to anodization, cyclic precalcification, and heat treatment

  • Oh, Eun-Ju;Nguyen, Thuy-Duong T.;Lee, Seung-Youp;Jeon, Young-Mi;Bae, Tae-Sung;Kim, Jong-Gee
    • The korean journal of orthodontics
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    • v.44 no.5
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    • pp.246-253
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    • 2014
  • Objective: To evaluate the bioactivity, and the biomechanical and bone-regenerative properties of Ti6Al4V miniscrews subjected to anodization, cyclic precalcification, and heat treatment (APH treatment) and their potential clinical use. Methods: The surfaces of Ti6Al4V alloys were modified by APH treatment. Bioactivity was assessed after immersion in simulated body fluid for 3 days. The hydrophilicity and the roughness of APH-treated surfaces were compared with those of untreated (UT) and anodized and heat-treated (AH) samples. For in vivo tests, 32 miniscrews (16 UT and 16 APH) were inserted into 16 Wistar rats, one UT and one APH-treated miniscrew in either tibia. The miniscrews were extracted after 3 and 6 weeks and their osseointegration (n = 8 for each time point and group) was investigated by surface and histological analyses and removal torque measurements. Results: APH treatment formed a dense surface array of nanotubular TiO2 layer covered with a compact apatite-like film. APH-treated samples showed better bioactivity and biocompatibility compared with UT and AH samples. In vivo, APH-treated miniscrews showed higher removal torque and bone-to-implant contact than did UT miniscrews, after both 3 and 6 weeks (p < 0.05). Also, early deposition of densely mineralized bone around APH-treated miniscrews was observed, implying good bonding to the treated surface. Conclusions: APH treatment enhanced the bioactivity, and the biomechanical and bone regenerative properties of the Ti6Al4V alloy miniscrews. The enhanced initial stability afforded should be valuable in orthodontic applications.