• Title/Summary/Keyword: Synchrotron X-ray and neutron diffraction

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X-Ray Diffraction line profile analysis of defects and precipitates in high displacement damage neutron-irradiated austenitic stainless steels

  • Shreevalli M.;Ran Vijay Kumar;Divakar R.;Ashish K.;Padmaprabu C.;Karthik V.;Archna Sagdeo
    • Nuclear Engineering and Technology
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    • v.56 no.1
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    • pp.114-122
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    • 2024
  • Irradiation-induced defects and the precipitates in the wrapper material of the Indian Fast Breeder Test Reactor (FBTR), SS 316 are analyzed using the synchrotron source-based Angle Dispersive X-Ray Diffraction (ADXRD) technique with X-rays of energy 17.185 keV (wavelength ~0.72146 Å). The differences and similarities in the high displacement damage samples as a function of dpa (displacement per atom) and dpa rate in the range of 2.9 × 10-7- 9 × 10-7 dpa/s are studied. Ferrite and M23C6 are commonly observed in the present set of high displacement damage 40-74 dpa SS 316 samples irradiated at temperatures in the range of 400-483 ℃. Also, the dislocation density has increased as a function of the irradiation dose. The X-ray diffraction peak profile parameters quantified such as peak shift and asymmetry show that the irradiation-induced defects are sensitive to the dpa rate-irradiation temperature combinations. The increase in yield strength as a function of displacement damage is also correlated to the dislocation density.

Evaluation of Residual Stresses in 12%-Cr Steel Friction Stir Welds by the Eigenstrain Reconstruction Method

  • Jun, Tea-Sung;Korsunsky, Alexander M.
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.24 no.1
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    • pp.15-22
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    • 2015
  • In the present paper we report the results of a study into Friction Stir Welds (FSWs) made in 13 mm-thick 12%-Cr steel plates. Based on residual strains obtained by diffraction techniques, eigenstrain analysis was performed using the Eigenstrain Reconstruction Method (ERM), which is a novel methodology for the reconstruction of full-field residual strain and stress distributions within engineering components. Significant eigenstrain distributions were found at around Thermo-Mechanically Affected Zone (TMAZ) where the most severe plastic deformation was occurred. Microstructure analysis was used to elucidate this phenomenon showing that the grain structure in TMAZ was bent and not successfully recrystallised, resulting in severe deformation behaviour. The reconstructed residual strain distributions by the ERM agree well with the experimental results. It was found that the approach based on theory of eigenstrain is a powerful basis for reconstructing the full-field residual strain/stress distributions in engineering components and structures.