• 공업화학
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• 제10권6호
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• pp.857-862
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• 1999

아민화된 poly(ether sulfone)(APES)는 poly(ether sulfone)(PES)를 질산과 황산(촉매)의 혼산으로 니트로화한 poly(ether sulfone)(NPES)를 아민화하여 제조되었다. FT-IR의 분석 결과 1537과 $1351cm^{-1}$에서 $NO_2$의 비대칭 신축진동과 대칭 신축진동에 의한 흡수피크로 니트로화가 되었음이 확인되었다. 또한 NPES의 아민화는 $NO_2$에 의한 흡수피크가 사라지고 3470과 $3374cm^{-1}$에서 $NH_2$기에 의한 비대칭 신축진동과 대칭 신축진동의 흡수피크로 확인되었다. PES(5 g; 21.55 mmol.)에 대한 니트로화의 최적 조건은 반응시간 12시간, 반응온도 $120^{\circ}C$, 질산의 농도 28.00 mmol. 황산의 농도 52.00 mmol. 이었다. APES의 원소분석결과 반복단위당 0.89개의 아민기가 도입되었다. 실리카겔이나 활성탄소보다 흡착속도는 느리나 NO에 대한 흡착능이 우수하였고, 화학적인 흡착속도는 물리적 흡착속도보다 느리며, 화학적 흡착량이 물리적 흡착량 보다 높은 것을 알 수 있었다.

• 대한기관식도과학회지
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• 제2권1호
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• pp.71-81
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• 1996

1992년 1월부터 1994년 12월까지 전남대학병원에서 경부 전산화단층촬영을 시행한 환자 중 경부에 종양, 염증성 질환 등 기질적인 질환 및 경부외상의 기왕력이 없는 45례의 경부 전산화단층촬영상에서 캘리퍼스 및 분도기를 이용하여 후두의 좌우 대칭성, 설골 및 성문의 위치, 후두의 길이 및 좌우 갑상 연골이 이루는 각도 등을 계측하여 다음과 같은 결과를 얻었다. 1. 대부분의 경우에서 후두구조는 어느 정도 비대칭성을 보였고 우측편위가 좌측편위보다 많았으며 성별 및 연령별에 따라 의의있는 차이는 없었다. 2. 설골의 높이는 제 2-3경추 부위에서 제 5-6경추 부위까지 위치하고 있었고 제 3-4경추 부위 가 가장 흔한 부위였다. 3. 성문의 높이는 제 4경추 부위에서 제 6-7경추간까지 위치하고 있었고 제 5경추 부위가 가장 흔한 부위였다. 4. 양측 갑상연골이 이루는 각도는 58도에서 100도까지 다양하였고 평균 81.5도였으며, 평균각도는 남성에서 77.24도, 여성에서 87.88도였다.

• 대한화학회지
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• 제41권5호
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• pp.251-255
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• 1997

유로퓸의 조성을 2~33% $Eu_2O_3$ 범위에서 변화시키면서 제조한 붕규산유리 매질에서의 $Eu^{3+}$ 이온에 대한 형광 및 형광붕괴시간을 측정하였다. 붕규산유리 매질 내에서 $Eu^{3+}$ 이온의 형광은 $f^b$ 전자구조내의 SL 결합에 의해 이루어진 준위간의 $5D0{\rightarrow}7FJ$(J=0, 1, 2, 3, 4) 전이들이고, 스펙트럼에서 양자수 J에 따른 Stark 부준위의 수로부터 $Eu^{3+}$ 이온 주변결정장의 대칭성 위수가 $n{\leq}2$ 인 낮은 대칭성을 갖고 있음을 알았다. 붕규산유리 매질 내의 음이온성 산소와 $Eu^{3+}$ 이온의 상대적 비에 따라 형광수명들의 종류 및 분률이 달라졌으며, 이로부터 붕규산유리 매질 내의 $Eu^{3+}$ 이온에 대한 주변의 결합조건을 추정하였다.

• 한국해양공학회지
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• 제29권1호
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• pp.34-44
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• 2015

A hydraulic tensile test machine (HSTM) is one of the devices used to obtain the flow stress of a material during high-speed elongation. This paper first describes some features of a newly built HSTM. The improvement histories of the upper and lower jigs, which are the most vital parts of the HSTM, are also presented. We have frequently witnessed test failures with 1st generation jigs and specimens due to slip between the jig and specimen. 2nd generation jigs provide more stable test results, but the use of a longer upper jig induces excessive vibration and consequently makes it difficult to attach an environment chamber. 3rd generation jigs have some advances in terms of the symmetric fastening between the upper jig and specimen, as well as an exemption from direct contact between the lower jig and specimen. The performance of an environment chamber is verified by high and low temperature tests. A high-speed displacement measurement system is introduced based on a high-speed camera and motion-tracking software with aid of a surface grid device for the specimen.

• International Journal of Aeronautical and Space Sciences
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• 제16권2호
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• pp.190-205
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• 2015

In this paper, the impact damage behavior of USN-150B carbon/epoxy composite laminates subjected to high velocity impact was studied experimentally and numerically. Square composite laminates stacked with $[45/0/-45/90]_{ns}$ quasi-symmetric and $[0/90]_{ns}$ cross-ply stacking sequences and a conical shape projectile with steel core, copper skin and lead filler were considered. First high-velocity impact tests were conducted under various test conditions. Three tests were repeated under the same impact condition. Projectile velocity before and after penetration were measured by infrared ray sensors and magnetic sensors. High-speed camera shots and C-Scan images were also taken to measure the projectile velocities and to obtain the information on the damage shapes of the projectile and the laminate specimens. Next, the numerical simulation was performed using explicit finite element code LS-DYNA. Both the projectile and the composite laminate were modeled using three-dimensional solid elements. Residual velocity history of the impact projectile and the failure shape and extents of the laminates were predicted and systematically examined. The results of this study can provide the understanding on the penetration process of laminated composites during ballistic impact, as well as the damage amount and modes. These were thought to be utilized to predict the decrease of mechanical properties and also to help mitigate impact damage of composite structures.

• 대한기계학회논문집A
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• 제26권11호
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• pp.2390-2398
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• 2002

For integrity analysis of nuclear reactor pressure vessel, including the Pressurized thermal shock analysis, the fast and accurate calculation of the stress intensity factor at the crack tip is needed. For this, a simple approximation scheme is developed and the resulting stress intensity factors for axial semi-elliptical cracks in cylindrical vessel under various loading conditions are compared with those of the finite element method and other approximation methods, such as Raju-Newman's equation and ASME Sec. Xl approach. For these, three-dimensional finite-element analyses are performed to obtain the stress intensity factors for various surface cracks with t/R = 0.1. The approximation methods, incorporated in VINTIN (Vessel INTegrity analysis-INner flaws), utilizes the influence coefficients to calculate the stress intensity factor at the crack tip. This method has been compared with other solution methods including 3-D finite clement analysis for internal pressure, cooldown, and pressurized thermal shock loading conditions. The approximation solutions are within $\pm$2.5% of the those of FEA using symmetric model of one-forth of a vessel under pressure loading, and 1-3% higher under pressurized thermal shock condition. The analysis results confirm that the VINTIN method provides sufficiently accurate stress intensity factor values for axial semi-elliptical flaws on the surface of the reactor pressure vessel.

• The Journal of Korean Physical Therapy
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• 제13권2호
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• pp.381-397
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• 2001

In the patients with hemiplegia caused by stroke and TBI. postural sway is increased and open displaced laterally over the non-affected leg, reflecting asymmetry in weight bearing on lower extremities during standing balance. Recovery of symmetric weight bearing and postural stability is an important aim in physical therapy. Plastic AFO has been used for hemiplegic patients in order to help their abnormal walking patterns. Past studies have mainly focused on the AFO influences on hemiplegic walking patterns without balance function approaches. The purpose of this study was to identify the immediate effects of plastic AFO and shoes on the static balance in hemiplegic patients. The scale for static balance were weight bearing on affected leg(%), sway area(mm2), sway path(mm), maximal sway velocity(mm/s), anteroposterior sway angle($^{\circ}$ ), and lateral angle($^{\circ}$ ). Seventeen hemiplegic patients participated in this study: 13 men and 4 women, with an average age of 50.18 years. Static balance was measured using BPM(balance performance monitor; dataprint software version 5.3) under four standing condition namely bare-foot standing. standing in shoes, standing with AFO, and standing in shoes with AFO. In order to assure the statistical significance of the results, an one-way ANOVA, the independent t-test. and a pearson's correlation were applied at the .05 level of significant. The results of this study were as follows: 1) There were statistically significant differences in weight bearing(%) on the static balance between affected leg and non-affected leg(p<.01). 2) There were statistically significant differences in sway reverse frequence(Hz) in standing with AFO between affected leg and non-affected leg(p<.05). 3) Sway area(mm2) on standing in shoes with AFO was lower than bare-foot standing(p<.05), Lateral sway angle($^{\circ}$ ) on standing in shoes with AFO was lower than bare-foot standing and standing in shoes(p<.05). 4) Weight bearing in affected leg was not significantly correlated with postural sway.

• 대한수학회지
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• 제35권4호
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• pp.1045-1060
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• 1998

Recently, Chung and et al. ([11], 1991c) introduced a new concept of a manifold, denoted by ＊g-SE $X_{n}$ , in Einstein's n-dimensional ＊g-unified field theory. The manifold ＊g-SE $X_{n}$ is a generalized n-dimensional Riemannian manifold on which the differential geometric structure is imposed by the unified field tensor ＊ $g^{λν}$ through the SE-connection which is both Einstein and semi-symmetric. In this paper, they proved a necessary and sufficient condition for the unique existence of SE-connection and presented a beautiful and surveyable tensorial representation of the SE-connection in terms of the tensor ＊ $g^{λν}$. This paper is the first part of the following series of two papers: I. The SE-curvature tensor of ＊g-SE $X_{n}$ II. The contracted SE-curvature tensors of ＊g-SE $X_{n}$ In the present paper we investigate the properties of SE-curvature tensor of ＊g-SE $X_{n}$ , with main emphasis on the derivation of several useful generalized identities involving it. In our subsequent paper, we are concerned with contracted curvature tensors of ＊g-SE $X_{n}$ and several generalized identities involving them. In particular, we prove the first variation of the generalized Bianchi's identity in ＊g-SE $X_{n}$ , which has a great deal of useful physical applications.tions.

• 전력전자학회논문지
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• 제17권6호
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• pp.486-494
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• 2012

In this paper, we proposes the three-phase embedded Z-source inverter consisting of the three embedded Z-source converters and it's the output voltage control method. Each embedded Z-source converter can produce the bipolar output capacitor voltages according to duty ratio D such as single-phase PWM inverter. The output AC voltage of the proposed system is obtained as the difference in the output capacitor voltages of each converter, and the L-C output filter is not required. Because the output AC voltage can be stepped up and down, the boost DC converter in the conventional two-stage inverter is unnecessary. To confirm the validity of the proposed system, PSIM simulation and a DSP based experiment were performed under the condition of the input DC voltage 38V, load $100{\Omega}$, and switching frequency 30kHz. Each converter is connected by Y-connection for three-phase loads. In case that the output phase voltage is the same $38V_{peak}$ as the input DC voltage and is the 1.5 times($57V_{peak}$), the simulation and experimental results ; capacitor voltages, output phase voltages, output line voltages, inductor currents, and switch voltages were verified and discussed.

• 한국지반환경공학회 논문집
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• 제10권5호
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• pp.69-73
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• 2009

본 연구에서는 수평력을 받는 캡과 연결된 무리말뚝의 거동을 파악하고 상호작용계수(p-multiplier)를 산정하기 위하여 $1{\times}3$ 말뚝에 대하여 말뚝간격(s)을 3D, 4D, 5D로 변화시키면서 3차원 수치해석을 수행하였다. 이때 모델링은 해석시간을 줄이기 위하여 대칭경계조건을 사용하였고 콘크리트 말뚝은 탄성모델을 적용하였으며 흙의 경우는 Druker-Prager 모델을 이용하였다. 화강풍화토에서 수평력을 받는 무리말뚝의 수치해석결과를 이용하여 말뚝간격에 따른 수평저항력을 외말뚝의 해석결과와 비교 분석하여 p-y 곡선을 구하였고, 이를 이용하여 수평력을 받는 무리말뚝의 각 열에 대해 상호작용계수를 산정하였다. 그 결과 말뚝간격이 증가함에 따라 상호작용계수 값도 증가하였으나 그림자효과에 의해 1.0보다 작은 값으로 나타났다.