• Journal of the Korean Society for Precision Engineering
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• v.18 no.9
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• pp.122-130
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• 2001

Induction surface hardening is widely used to enhance local strength and hardness. However, most research is only to have a focus on fatigue life and fatigue behavior is not so much studied. So, in this study, Cr-Mo steel alloy(SCM440) was used to show the effect of residual stress and micro hole on the fatigue strength fur base metal and induction surface hardened specimen. In addition, the fatigue characteristic between surface hardened and fully hardened steel is somewhat different. It is caused by hardness distribution, residual stress and inclusions etc.. The modification of prediction equation of fatigue strength is proposed and predicted results show very good accuracy. A $textsc{k}$, which is calculated 1.46, is introduced to consider the effect of stationary crack with defect. A new method of modifying residual stress is proposed to examine the mean stress effect under fatigue loading.

• Journal of the Korean institute of surface engineering
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• v.36 no.5
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• pp.398-405
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• 2003

The stainless steel wire requires good corrosion resistance and mechanical properties, such as drawing ability, combined with a high resistance to corrosion. For increasing drawing ability of stainless steel, Ni coating methods have been used in this study. However, there is no information on the electrochemical corrosion behavior of drawed wires after Ni coating. To investigate corrosion resistance and mechanical property of drawed wire, the characteristics of Ni coated wires have been determined by tensile strength tester, hardness tester, field emission scanning microscope, energy dispersive x-ray analysis and potentiodynamic method in 0.1 M HCl. The drawed stainless steel wires showed the strain-induced martensitic structure, whereas non-drawed stainless steel wire showed annealing twin in the matrix of austenitic structure. The hardness and tensile strength of drawed stainless steel wire were higer than that of non-drawed stainless steel wire. Electrochemical measurements showed that, in the case of drawed stainless steel o ire after Ni coating, the corrosion resistance and pitting potential increased compared with non-coated and drawed stainless steel wire due to decrease in the surface roughness.

• Korean Journal of Materials Research
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• v.12 no.8
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• pp.669-675
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• 2002

CrN film coated by AIP method, improved the mechanical properties (Hardness, Roughness, wear and fatigue) of Ti-6Al-4V alloy. The properties were studied using GXRD, XPS, Hardness, Roughness, wear and fatigue testers. CrN thin film thickness was about 7.5$\mu\textrm{m}$ and grew with (111) orientation. Hardness of CrN thin film was very high (Hv 1390) and roughness of the surface layer was greatly improved (Ra=0.063$\mu\textrm{m}$) compared with matrix alloy (Ra=0.321$\mu\textrm{m}$). Such changes of hardness and roughness could be contributed to improving the wear resistance and fatigue life. Striation like pattern with dimples and voids, a typical fatigue fracture mode, was observed throughout the specimen.

• The Journal of Korean Academy of Prosthodontics
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• v.41 no.5
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• pp.596-605
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• 2003

Statement of problem : IPS Empress2 system was developed and used in prosthodontic treatment, but the cost of ingot is expensive for wide application. Purpose : This study was to investigate the possibility on recycling of IPS Empress 2 ceramic for wide application of IPS Empress 2 ceramic in prosthodontic treatment. Material and Method : 1st, 2nd and 3rd pressed disc-shaped($10{\times}1.5mm$) IPS Empress 2 specimens were made with IPS Empress ingot(200, Ivoclar, Liechtenstein) and pressing furnace(IPS Empress EP 500, Ivoclar, Liechtenstein). Vicker's surface hardness and fracture toughness, acid resistance, and pressing accuracy of IPS Empress 2 ceramic were measured and analyzed. Surface hardness was measured by microhardness tester(MTX 70. Matsuzawa, Japan), before and after surface treatment with 0.5% hydrofluoric acid and carbonic acid(Coca cola) for evaluation of acid resistance. Results : The surface hardness of 1st pressed specimen was the higher(5.11 GPa) than those of 2nd pressed(4.89 GPa) and 3rd pressed specimen(4.86 GPa), and the fracture toughness of 1st pressed ($1.58MPam^{1/2}$) and 2nd pressed specimen($1.51MPam^{1/2}$) were higher than that of 3rd pressed specimen($1.39MPam^{1/2}$). The changes of surface hardness of 1st, 2nd, and 3rd pressed specimens after treatment with fluoric acid were 0.17, 0.06, 0.05 (GPa) respectively, and those of 1st, 2nd, and 3rd pressed specimens after treatment with carbonic acid were 0.07, 0.00, 0.05(MPa) respectively. The pressing accuracy of 1st,2nd and 3rd specimen were 77.22%, 85.681%, and 75.05%. The pressing accuracy of 2nd pressed specimen was higher than that of the 3rd specimen. Conclusion : The changes of physical properties according to recycling of IPS Empress 2 from this study were insignificant. Therefore the possibility of recycling of IPS Empress 2 can be suggested from the results.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.11 no.5
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• pp.29-34
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• 2012

This study describes the selection of optimum machining conditions for a high-hardness resin by using a large 5-axis machine. The experiments were conducted to examine the main factors that affect the surface roughness, such as the spindle speed, axial and radial depths of the cut, and pattern of the cutter path. To analyze the experiment results, the factor with the biggest impact on machining was determined using the smaller-the-better characteristic of the Taguchi method; the effectiveness of the experiment was then confirmed by verifying the selected optimum machining condition.

• Journal of Korea Foundry Society
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• v.13 no.3
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• pp.238-247
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• 1993

Microstructure, hardness and wear characteristics of $SiC_p/Al-6.5wt%Si-1.7wt%Mg$ alloy composites fabricated by the method of rheo-compocasting and hot pressing are investigated in this study. The dispersion of SiC particles in the composites is homogeneous and the hardness improves as additional amount increases. The wear amount of the matrix metal increases highly as wear rates increase, for the wear mechanism changes from adhesive wear to melt wear, and the matrix metal was coated on the surface of revolving disc and its weight increases. In the 5vol% composites, Fe is adhered on the surface of specimen by the projection of the dispersed hard SiC particles which have net-work structure and the coating layer is about $300{\mu}m$. But in the composite more than 20vol%, the wear amount of composite decreases because the SiC particles which have superior hardness, wear resistance and heat resistance properties resist wear, the abrasive wear turn out predominant wear mechanism and so the wear amount of revolving disc increases.

• Journal of Ocean Engineering and Technology
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• v.22 no.2
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• pp.99-105
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• 2008

Ultrasonic nanocrystal surface modification (UNSM) is a method to induce severe plastic deformation to a material surface, so that the structure of the material surface becomes a nanocrystal structure from the surface to a certain depth. It improves the mechanical properties, namely hardness, compressive residual stress, and fatigue characteristics. Specimens of SKD61 were tested to verify the effects of the variation of UNSM static load level on fatigue characteristics. The results were as follows: the grain size of SKD61 treated with UNSM became very fine from the material surface to a $100{\mu}m$ depth. The surface hardness of SKD61 was increased up to 37% after UNSM. And fatigue strength at $10^7$ cycles was increased by 8.3, 11.2, and 17.9% respectively, when the static load levels of UNSM were 4, 6, 8 kgf.

• Journal of the Korean institute of surface engineering
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• v.34 no.5
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• pp.510-515
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• 2001

It was first time that low frequency R.F. derived plasma enhanced MOCVD with frimethylborate precursor was used to fabricate a new ternary compound $BO_{x}$ $N_{y}$ . The formation of BON molecule was resulted from nitrogen nitrifying B-O, and forming the angular molecule structure proved by XPS and FT-IR results. The relationship between hardness and film thickness was studied. An thickness-independent hardness was fond about 10 GPa. The empirical calculation of band-gap and UV test result showed that our deposited $BO_{x}$ $N_{y}$ thin film was semiconductor material with 3.4eV of wide band gap. The electrical conductivity, $4.8$\times$10^{-2}$ /($\Omega$.cm)$^{-1}$ also confirmed that $BO_{x}$ $N_{y}$ has a semiconductor property. The roughness detected from the as-grown films showed that there was no serious bombarding effect due to anion in the plasma occurring in the RF frequency derived plasma.

• Tribology and Lubricants
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• v.34 no.6
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• pp.217-225
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• 2018

In this study, we spray a Ni-Cr composite powder onto AISI 4340 steel using the high velocity oxygen fuel method. We subsequently subject the Ni-Cr coating (as-sprayed) to ultrasonic nanocrystal surface modification (UNSM) process to improve the tribological performance. This study aims at increasing the wear resistance and durability of the Ni-Cr coating by altering the surface integrity and microstructure via the UNSM process. The UNSM process reduces the surface roughness of the as-sprayed coating by about 64%, which is explained by observing the elimination of high peaks and valleys and filling up micro-pores. Furthermore, a change in the microstructure of the coating due to continuous high-frequency strikes to the surface by a tip can lead to an increase in hardness from about 48 to 60 HRC. Furthermore, we investigate the characterization of the friction and wear behavior of Ni-Cr coating by a ball-on-disc tribometer in the dry conditions. We determine that after the UNSM process, there is a significant reduction in the friction coefficient of the as-sprayed coating from approximately 1.1 to 0.75. This is owing to the increased hardness and smoothed surface roughness. In addition, we investigate the surface morphology and wear track of the coatings before and after the UNSM process using a scanning electron microscope, energy dispersive spectrometer, and three-dimensional laser scanning microscope. We observe that the wear track of the Ni-Cr coating after the UNSM process is lower than that of the as-sprayed one. Thus, we confirm that the UNSM process has a significant influence on the improvement of the tribological performance of the Ni-Cr composite coating.

• Journal of the Korean institute of surface engineering
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• v.45 no.3
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• pp.130-135
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• 2012

Hydrogen charging was electrochemically conducted at high strength DP steels and TRIP steel with varying charging time. The penetration depths and the mechanical properties with charging conditions were investigated through the distribution of micro-hardness and the microstructural observation of the subsurface zone. The micro-Vickers hardness was measured to evaluate the hydrogen embrittlement of subsurface zone in addition to the microscope investigation. It was shown that the hydrogen amounts decreased in DP steels and TRIP steel with increasing hydrogen charging time. As shown by micro-Vickers hardness test and small punch test results, micro-Vickers hardness and SP energy for DP steels and TRIP steel decreased with increasing hydrogen charging time, for constant value of charging current density. SEM investigation results for the hydrogen contained samples showed that the major fracture behavior was brittle fracture which results in dimples on fractured surface and the size of dimples were decreased with increasing hydrogen charging time. These results indicate that hydrogen embrittlement is the major cause for the fracture of high strength steels and also micro-Vickers hardness test and small punch test is a valuable test method for hydrogen embrittlement of high strength sheet steels.