• Title/Summary/Keyword: Surface hardness method

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Alkaline induced-cation crosslinking biopolymer soil treatment and field implementation for slope surface protection

  • Minhyeong Lee;Ilhan Chang;Seok-Jun Kang;Dong-Hyuk Lee;Gye-Chun Cho
    • Geomechanics and Engineering
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    • v.33 no.1
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    • pp.29-40
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    • 2023
  • Xanthan gum and starch compound biopolymer (XS), an environmentally friendly soil-binding material produced from natural resources, has been suggested as a slope protection material to enhance soil strength and erosion resistance. Insufficient wet strength and the consequent durability concerns remain, despite XS biopolymer-soil treatment showing high strength and erosion resistance in the dried state, even with a small dosage of soil mass. These concerns need to be solved to improve the field applicability and post-stability of this treatment. This study explored the utilization of an alkaline-based cation crosslinking method using calcium hydroxide and sodium hydroxide to induce non-thermal gelation, resulting in the enhancement of the wet strength and durability of biopolymer-treated soil. Laboratory experiments were conducted to assess the unconfined compressive strength and cyclic wetting-drying durability performance of the treated soil using a selected recipe based on a preliminary gel formation test. The results demonstrated that the uniformity of the gel structure and gelling time varied depending on the ratio of crosslinkers to biopolymer; consequently, the strength of the soil was affected. Subsequently, site soil treated with the recipe, which showed the best performance in indoor assessment, was implemented on the field slope at the bridge abutment via compaction and pressurized spraying methods to assess feasibility in field implementation. Moreover, the variation in surface soil hardness was monitored periodically for one year. Both slopes implemented by the two construction methods showed sufficient stability against detachment and scouring, with a higher soil hardness index than the natural slope for a year.

Optimization of Ultrasound-Assisted Pretreatment for Accelerating Rehydration of Adzuki Bean (Vigna angularis)

  • Hyengseop Kim;Changgeun Lee;Eunghee Kim;Youngje Jo;Jiyoon Park;Choongjin Ban;Seokwon Lim
    • Journal of Microbiology and Biotechnology
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    • v.34 no.4
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    • pp.846-853
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    • 2024
  • Adzuki bean (Vigna angularis), which provides plant-based proteins and functional substances, requires a long soaking time during processing, which limits its usefulness to industries and consumers. To improve this, ultrasonic treatment using high pressure and shear force was judged to be an appropriate pretreatment method. This study aimed to determine the optimal conditions of ultrasound treatment for the improved hydration of adzuki beans using the response surface methodology (RSM). Independent variables chosen to regulate the hydration process of the adzuki beans were the soaking time (2-14 h, X1), treatment intensity (150-750 W, X2), and treatment time (1-10 min, X3). Dependent variables chosen to assess the differences in the beans post-immersion were moisture content, water activity, and hardness. The optimal conditions for treatment deduced through RSM were a soaking time of 12.9 h, treatment intensity of 600 W, and treatment time of 8.65 min. In this optimal condition, the values predicted for the dependent variables were a moisture content of 58.32%, water activity of 0.9979 aw, and hardness of 14.63 N. Upon experimentation, the results obtained were a moisture content of 58.28 ± 0.56%, water activity of 0.9885 ± 0.0040 aw, and hardness of 13.01 ± 2.82 g, confirming results similar to the predicted values. Proper ultrasound treatment caused cracks in the hilum, which greatly affects the water absorption of adzuki beans, accelerating the rate of hydration. These results are expected to help determine economically efficient processing conditions for specific purposes, in addition to solving industrial problems associated with the low hydration rate of adzuki beans.

Effect of Furnace Temperature on the Property of TiN-Coated Layer on Hard Metal by Arc Ion Plating (AIP 코팅법에서 로의 온도가 초경합금의 TiN 코팅층 성질에 미치는 영향)

  • Kim Hae-Ji;Joun Man-Soo;Kim Nam-Kyung
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.15 no.1
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    • pp.49-55
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    • 2006
  • The effect of coating temperature with regard to surface properties of TiN-coated layer on hard metal(WC-Co) are experimentally investigated. Hardness, surface roughness, TiN coating thickness and adsorption force were measured in order to evaluate the effect of coating temperature. The two-way ANOVA method is used in order to evaluate the experimental data. In AIP processing, It is concluded that the furnace temperature in the range of $400^{\circ}C\~500^{\circ}C$ affected to a little increasing the number of production with the coating temperature.

Characterization of Nanocomposite Ti-Si-N Films Prepared by a Hybrid Deposition System of A If and Sputtering Techniques (하이브리드 증착 시스템을 이용한 나노복합체 Ti-Si-N 박막의 특성 연구)

  • 윤순영;최성룡;이미혜;김광호
    • Journal of the Korean institute of surface engineering
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    • v.36 no.2
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    • pp.122-127
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    • 2003
  • Ti - Si - N hard films were deposited on SKD11 steel substrates by a hybrid deposition system, where TiN was deposited by AIP method while Si was incorporated by sputtering one. The microstructure of Ti-Si-N films was revealed to be a composite of TiN crystallites and amorphous Si3N4 by instrumental analyses. The highest hardness value of about 45 Gpa was obtained at the Si content of around 7.7 at.%. With increase of Si content, the size of TiN crystallites was reduced and their distribution was changed from aligned to randomly orientated states. Surface roughness of Ti-Si-N film also decreased with increase of Si content.

The hybrid film characteristics of UV-curable organic-inorganic coating solutions (자외선 경화형 유/무기 코팅제의 복합 필름 특성)

  • Lee, Chang-Ho;Kim, Sung-Rae;Lee, Jong-Dae
    • Journal of the Korean Applied Science and Technology
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    • v.28 no.2
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    • pp.240-246
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    • 2011
  • UV-Curable hybrid coatings were synthesized to improve the surface properties of plastic film. Organic-inorganic coating solutions were prepared by the sol-gel method using urethane-acrylate oligomer, acrylate monomer, photo initiator and tetraethoxysilane (TEOS). Methacryloyloxypropyltrimethoxysilane(MPTMS) was used as a silane coupling agent to improve chemical interaction between inorganic phases and UV curable acrylate. In this study, the surface hardness and adhesive properties were improved with the use of inorganic component. The experimental results showed that UV-Curable hybrid films containing aliphatic urethane oligomer, hexanedioldiacrylate, trimethylolpropanetriacrylate, hydroxy dimethyl acetophenone exhibited good surface properties. Also, the optimum curing conditions were investigated.

Chemical Mechanical Polishing Characteristics of PZT Thin Films (PZT 박막의 화학.기계적 연마 특성)

  • Seo, Yong-Jin;Lee, Woo-Sun
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.55 no.12
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    • pp.549-554
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    • 2006
  • In this paper we first applied the chemical mechanical polishing (CMP) process to the planarization of ferroelectric film in order to obtain a good planarity between electrode and ferroelectric film. $Pb_{1.1}(Zr_{0.52}Ti_{0.48})O_3$ (shortly PZT) ferroelectric film was fabricated by the sol-gel method. And then, we compared the structural characteristics before and after CMP process of PZT films. Removal rate, WIWNU% and surface roughness have been found to depend on slurry abrasive types and their hardness, especially, surface roughness and planarity were strongly depends on its pH value. A maximum in the removal rate is observed in the silica slurry, in contrast with the minimum removal rate occurs at ceria slurry. We found that the surface roughness of PZT films can be significantly reduced using the CMP technique.

Preparation of Hard Coating Solutions using Colloidal Silica and Glycidoxypropyl Trimethoxysilane by the Sol-Gel Method (Sol-Gel 법에 의해 Colloidal Silica와 Glycidoxypropyl Trimethoxysilane으로 부터 하드코팅 용액의 제조)

  • Kim, Dae Hyun;Song, Ki Chang;Chung, Jae Shik;Lee, Bum Suk
    • Korean Chemical Engineering Research
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    • v.45 no.5
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    • pp.442-447
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    • 2007
  • In order to improve the surface hardness of transparent plastic films, organic-inorganic hybrid coating solutions were synthesized by the sol-gel method. The coating solutions were prepared by adding GPTMS (glycidoxypropyl trimethoxysilane) to a colloidal silica (12 nm) suspension. PC(polycarbonate) substrates were dipped into the coating solutions and dried at room temperature for 10 min before being cured at $80^{\circ}C$ for 30 min. The effect of the solution pH and GPTMS content was investigated on the properties of coating films. The pencil hardness and adhesion to substrates of the coating films, prepared at acidic condition (pH 4), showed better properties than those at neutral or basic conditions. Also, the pencil hardness and adhesion to substrates of the coating films increased with increasing GPTMS content.

A Study in the Heat Resistance Properties of STD61 Steel using the Surface Hardening Method (STD61 강의 내열특성향상을 위한 표면경화에 관한 연구)

  • Lee, Gu-Hyeon
    • 연구논문집
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    • s.26
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    • pp.121-132
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    • 1996
  • The carburising surface modification treatment of the die steel has been used for improving wear resistance and heat cycle strength of the die and preventing a pitting on the surface because the carbides are forming in the matrix during carburising. Generally, the hot forging die was used after quenching-tempering treatment or nitriding after quenching-tempering treatment. The nitriding after carburising on the surface of a hot die steel and a wear resistance die steels was suggested by SOUCHARD, JACQUOT. and BUVRON. This surface modification treatment improved the adhesive and abrasive wear resistance and friction coefficient. The process was introduced to the forging die of stainless steel, titanium alloy steel, alloy and medium carbon steel and the physical properties of the die after the treatment were improved. The surface hardening treatment of the nitriding, the carburising, the boriding, and TD process were used to improved the life time of the forging die. Also, the coating process of PVD, CVD and PCVD were used and the hard chromium plating was occasionally used. Therefore, this study analyzed the effects of the carburising time and the conditions of nitriding on STD61 steel. The case depth, the surface hardness, the forming carbide size and shape during overcarburising process on the die steel were also examined.

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Novel Coatable Polarizer Based on Polymer-Stabilized Lyotropic Chromonic Liquid Crystals

  • Bae, Yun-Ju;Jeong, Kwang-Un;Shin, Seung-Han;Lee, Myong-Hoon
    • 한국정보디스플레이학회:학술대회논문집
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    • 2009.10a
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    • pp.517-519
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    • 2009
  • We fabricated thin film polarizer by coating lyotropic chromonic liquid crystals (LCLCs) dissolved in anionic monomer solution. Compared to water-based technique, the new method provided many advantages such as excellent coatability, good adhesion to various substrates, and superb surface hardness.

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Surface Properties of Artificial Suedes (인조 스웨이드의 표면특성)

  • Roh, Eui Kyung;Oh, Kyung Wha
    • Fashion & Textile Research Journal
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    • v.15 no.2
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    • pp.309-315
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    • 2013
  • This study examines the difference of surface properties according to napping characteristic of artificial suedes, measuring surface structure observation, the contact/non-contact method roughness, warm-cool feeling of touch, and subjective hand evaluation. Surface and cross-section observations showed a discernible difference in fineness, curl, length, mount of napping, and covering power of base fabric. The surface properties of artificial suede evaluated by KES-FB4 showed that the shorter napping length the more smooth surface and the roughness increased reciprocally with friction resistance and surface contour when the nap length reaches a high level. The surface roughness measuring system applied a laser displacement sensor by a non-contact method to assess napping characteristic and the base fabric and napping height. Surface roughness decreased when napping was uniformly covered with base fabric; however, the surface roughness increased specifically with the uneven covering power of the base fabric. For qmax of the suedes, those that had short and smaller amounts of napping increased; however, the napping of length and amount at some stage generated a low qmax value. The warm sensation in all suedes were strongly perceived, but the cool sensation of the perception was lower in the subjective evaluation. Smoothness and softness were perceived when the suede has a long and large amount napping; however, smoothness and hardness were perceived when the suede was short and with the uneven covering power.