• Title/Summary/Keyword: Surface hardness method

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Characteristics of Micro-hardness and Corrosion of Electroless Nickel-Phosphorus Plating depending on Heat Treatment

  • Jung Seung-Jun;Park Soo-Gil
    • Journal of the Korean Electrochemical Society
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    • v.3 no.4
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    • pp.196-199
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    • 2000
  • Electroless plating is the desirable surface treatment method which is being widely used to all kinds of material such as requiring corrosion resistance, wear resistance and conductivity, especially plating of nonconductive material. Electroless nickel deposit has particular characteristics including non-magnetic property, amorphous structure, wear resistance, corrosion protection and thermal stability. In this study, electroless nickel plating was studied with an change in hardness and corrosion resistance of electroless nickel-phosphorus deposit depending on heat treatment. The highest hardness value was obtained by heat treatment at $500^{\circ}C$ Corrosion resistance of deposit, which had been heated at $300^{\circ}C$, was excellent when it was immersed in 1M $H_2SO_4$ solution for 60 hrs.

Quantitative Estimation of Surface Roughness Affecting the Fatigue Limit (피로한도(疲勞限度)에 영향을 미치는 표면(表面)거칠기의 정량적 평가)

  • Kim, Jin-Hak;Kim, Min-Gun
    • Journal of Industrial Technology
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    • v.17
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    • pp.5-10
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    • 1997
  • Fatigue tests were performed to investigate how much vary the fatigue limit under the different surface conditions on Carbon Steel(SM55C). Four types of specimen which have different surface roughness each other, Series A by turning, Series B by grinding, Series C by polishing and Series D by roller finishing showed the fatigue limit of 265, 320, 335 and 365MPa, respectively. Series D show 36% higher than Series A, which is caused by compressive residential stress on the surface. Therefore, roller finishing machining is helpful not only increase the fatigue limit but also improve the surface roughness. Moreover, to predict the fatigue limit under the conditions of knowing surface roughness and hardness of specimen, ${\sqrt{area}}$ area parameter method is very useful.

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Surface Strengthening of 3Y-TZP Ceramics by Boehmite Sol Infiltration (Boehmite Sol 함침에 의한 3Y-TZP 소결체의 표면 강화)

  • Choi, Ki-Sik;Kim, Young-Jung;Kim, Hwan
    • Journal of the Korean Ceramic Society
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    • v.31 no.6
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    • pp.671-677
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    • 1994
  • To improve the low resistance of ceramics to tensile stress, many techniques, for introducing and retaining surface compressive stress have been suggested. In present work, in order to introduce the compressive stress on the surface of TZP ceramics TZP-Al2O3 composites were made with infiltration technique. Highly porous 3Y-TZP pre-sintered specimens were submerged in AlOOH(boehmite) sol and the sol penetrated into them through open pore channels with moderate depth after that specimens were sintered. It was known that controlling the number of infiltration time can vary the amount of Al2O3 phase and the fraction of alumina at surface reached up to 18%. The depth of composite surface layer were 100~200 ${\mu}{\textrm}{m}$, and these were acceptable in surface strengthening which were proved by Vickers hardness indentation method.

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The surface profile of Wire-cut EDMed Surface by Lapping Process (래핑가공에 의한 와이어 방전가공면의 표면형상)

  • 이재명;김원일;왕덕현;이윤경
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2001.04a
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    • pp.956-959
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    • 2001
  • In die and mould industry, major material such as cemented carbide is broadly used for increasing the life time and decreasing the cost. It is also required the development for the skills of wire-cut electrical discharge machining(WEDM), but the WEDMed surface was found to be worst due to the attached components of wire. Precision machining method like lapping is necessary for obtaining high quality surface. The lapping compound such as Al2O3 and SiC and cast iron lap can be used for lapping process. The components of Cu and Zn were found WEDMed surface of the specimen. As the result, the low quality of precision was obtained and the heat damage layer of the specimen was occurred. The value of surface hardness was deteriorated, and therefore finish process was required.

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Surface Texture and Roughness of inclined surface milled by Long neck ball endmill (리브가공용 롱엔드밀의 경사면 가공시 표면형상 및 조도)

  • Yang J.S.;Jung T.S.;Kim Y.G.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2006.05a
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    • pp.565-566
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    • 2006
  • High speed machining experiment on the inclined surfaces of hardened mold steel(STAVAX at hardness HRC 53) is carried out using the long-neck type ball endmill. Surface texture and roughness are compared fur various cutting conditions. Tool overhang length greatly affects the roughness of machined surface. It is found that, fur this type of long-neck endmill, the chip load should be carefully selected by reducing either the axial depth of cut or feedrate to avoid tool vibration. Feedrate adjustment is more appropriate method in terms of tool wear.

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Surface Characteristics of Stainless Steel Wire for Dental and Medical Use (치과 및 의료용 스테인리스강선의 표면특성)

  • 최한철;고영무
    • Journal of the Korean institute of surface engineering
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    • v.36 no.4
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    • pp.339-346
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    • 2003
  • Stainless steel wire has been used in industry, dental and medical parts. Especially, it has been used widely for the dental orthodontic materials. The orthodontic wire requires good mechanical properties, such as elastic strength, combined with a high resistance to corrosion. To increase elastic strength and good corrosion resistance, drawing methods(one-step and two-step drawing) have been used and the electrochemical characteristics of drawed wire have been researched using potentiodynamic method in 0.9%NaCl and field emission scanning electron microscope. The one-step drawed wire showed the formation of rough surface. The hardness and tensile strength of two-step drawed wire increased. For the case of two-step drawed wire, the corrosion resistance and pitting potential increased compared with one-step drawed wire due to the drawing induced small surface roughness, such as scratch. The passivation and active current density decreased as the reduction in area for drawing increased.

Effect of Induction Hardening on Mechanical Properties in Gas Nitrocarburized SM35C Steel (가스 침질탄화처리한 SM3SG강의 기계적 성질에 미치는 고주파퀜칭의 영향)

  • Kim, H.S.;Lee, K.B.;Yu, C.H.;Kim, H.T.;Jang, H.Y.
    • Journal of the Korean Society for Heat Treatment
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    • v.13 no.4
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    • pp.224-230
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    • 2000
  • Garbon steel(SM35C) was gas nitrocarburized at $580^{\circ}C$ in $55%N_2-40%NH_3-5%CO_2$ mixed gas atmosphere, and then the steel was induction hardened at $850^{\circ}C$. The microstructure of gas nitrocarburized surface layer was observed by optical microscope and SEM. The phase analysis was carried out by X-ray diffraction method. The mechanical properties of gas nitrocarburized SM35C steel was evaluated by hardness, wear and fatigue test. The thickness of compound and diffusion layer were increased with increasing the gas nitrocarburizing time and the densest compound layer was obtained at 3 hours gas nitrocarburizing time. In case of 15sec induction hardening after gas nitrocarburizing, the surface hardness was decreased from 800Hv to 630Hv owing to the decomposition of compound layer, but wear resistance was increased because of increased hardness of diffusion layer. The fatigue strength of induction hardened steel after gas nitrocarburizing, $58kgf/mm^2$, was higher than $41.5kg/mm^2$ of gas nitrocarburized steel and $45kg/mm^2$ of induction hardened steel, respectively.

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Effect analysis in Laser Metal Deposition of SKD61 using AISI M2 power (AISI M2 파우더를 이용한 SKD61 재질의 레이저 메탈 디포지션 기초 특성 분석)

  • Kim, Won-Hyuck;Jung, Byung-Hun;Oh, Myeong-Hwan;Choi, Seong-Won;Kang, Dae-Min
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.14 no.3
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    • pp.50-56
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    • 2015
  • In this study, AISI M2 powder was selected primarily through various pieces of literature in order to improve the hardness and wear resistance. Among the laser metal deposition parameters, laser power was studied to improve the deposition efficiency in the laser metal deposition using a diode-pumped disk laser. An SKD61 hot work steel plate and AISI M2 powder were used as a substrate and powder for laser metal deposition, respectively. Experiments for the laser metal deposition were carried out by changing the laser power and track layer. The quality of the track surface and cross-section after applying the single-layer method was better than that obtained from applying the multi-layer method. As the laser power increased, the track thickness was increased, and the surface roughness deviation was decreased. In laser power condition of 1.6kW, the maximum hardness of the deposition track was 790Hv. This value was 40% better than the hardness of the SKD61 after heat treatment.

Characteristics of Carbon-Doped Mo Thin Films for the Application in Organic Thin Film Transistor (유기박막트랜지스터 응용을 위한 탄소가 도핑된 몰리브덴 박막의 특성)

  • Dong Hyun Kim;Yong Seob Park
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.36 no.6
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    • pp.588-593
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    • 2023
  • The advantage of OTFT technology is that large-area circuits can be manufactured on flexible substrates using a low-cost solution process such as inkjet printing. Compared to silicon-based inorganic semiconductor processes, the process temperature is lower and the process time is shorter, so it can be widely applied to fields that do not require high electron mobility. Materials that have utility as electrode materials include carbon that can be solution-processed, transparent carbon thin films, and metallic nanoparticles, etc. are being studied. Recently, a technology has been developed to facilitate charge injection by coating the surface of the Al electrode with solution-processable titanium oxide (TiOx), which can greatly improve the performance of OTFT. In order to commercialize OTFT technology, an appropriate method is to use a complementary circuit with excellent reliability and stability. For this, insulators and channel semiconductors using organic materials must have stability in the air. In this study, carbon-doped Mo (MoC) thin films were fabricated with different graphite target power densities via unbalanced magnetron sputtering (UBM). The influence of graphite target power density on the structural, surface area, physical, and electrical properties of MoC films was investigated. MoC thin films deposited by the unbalanced magnetron sputtering method exhibited a smooth and uniform surface. However, as the graphite target power density increased, the rms surface roughness of the MoC film increased, and the hardness and elastic modulus of the MoC thin film increased. Additionally, as the graphite target power density increased, the resistivity value of the MoC film increased. In the performance of an organic thin film transistor using a MoC gate electrode, the carrier mobility, threshold voltage, and drain current on/off ratio (Ion/Ioff) showed 0.15 cm2/V·s, -5.6 V, and 7.5×104, respectively.

Effects of Specimen Preparation Method and Contact Resistance on the Formation of Anodizing Films on Aluminum Alloys (시편의 준비 방법 및 접촉저항이 알루미늄 합금의 아노다이징 피막 형성에 미치는 영향)

  • Moon, Sungmo
    • Journal of the Korean institute of surface engineering
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    • v.53 no.1
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    • pp.29-35
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    • 2020
  • In this study, five different specimen preparation methods were introduced and their advantages and disadvantages were presented. One of them, an epoxy mounting method has advantages of constant exposure area, ease of surface preparation without touching the specimen surface during polishing or cleaning, use of small amount of material and ease of specimen reuse by polishing or etching. However, in order to eliminate unexpected errors resulting from preferable reaction at the specimen/epoxy interface and contact resistance between the specimen and copper conducting line for electrical connection, it is recommended to cover the wall side of the specimen with porous anodic oxide films and to remain the contact resistance lower than 1 ohm. The increased contact resistance between the specimen and Cu conducting line appeared to result in increases of anodizing voltage and solution temperature during anodizing by which thickness and hardness of anodizing film on Al2024 alloy were drastically decreased and color of the films became more brightened.