• 제목/요약/키워드: Surface concentration

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Silane coupling agent인 MPS 농도별처리에 따른 열중합 레진과 자가중합 레진 간의 전단결합강도 (Effects of Treatment of Silane Coupling Agent in MPS Concentration on the Shear Bond Strength between Self Curing Resins and Heat Curing Resin)

  • 최에스더;권은자
    • 한국콘텐츠학회논문지
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    • 제15권2호
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    • pp.344-351
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    • 2015
  • 본 논문은 치과에서 많이 사용되고 있는 silane coupling agent로 표면 처리한 의치상 레진과 자가중합 레진 간의 전단 결합력에 미치는 영향에 대해 알아보고자 하였다. 의치상 레진에 silane coupling agent 농도별 표면 처리 후 자가중합레진을 주입하여 전단결합강도를 측정하였다. Silane coupling agent(MPS)의 농도별 표면 처리에 따른 의치상 레진과 자가중합레진 간의 전단결합강도에서는 Vertex self curing resin에서 5%, 7%에서 유의적으로 높게 나타났고(P<0.05), Kooliner에서는 5%에서 유의적으로 가장 높게 나타났다(P<0.05). 따라서 의치상 레진과 자가중합레진 사이에 MPS 5%를 이용한 표면처리가 전단결합강도에 효과적으로 영향을 미치는 것이라 사료된다.

Studies on the Development for Sustained Release Preparation (II):Preparation and Evaluation of Eudragit Microcapsules of Sodium Naproxen

  • Shin, Sang-Chul;Lee, Keong-Ran
    • Archives of Pharmacal Research
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    • 제16권1호
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    • pp.50-56
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    • 1993
  • The microencapsulation of sodium naproxen with Eudragit. RS was studied by coacrtvation/phase separation process using Span 80 in mineral oil/acetone system. Various factors which affect the mciroencapsulation, e.g., stirring speed, and surfactant concentraction, Eudagit RS concentration and loading drug amounts were examined. For the evaluation of the prepared microcapsules, release rate, particle size distribution and surface appearance as well as in vivo test were carried out. The addition of n-hexane and freezing of microcapsules accelerated the hardening of microcapsules. The optimum concentration of Span 80 ti prepare the smallest microcapsules was the same value with the CMC of Span 80 in solvent system. When 1.5% (w/w) Span 80 was used, the smallest microcapsules were formed $(30.02\pm5.05\mu$ in diameter) belonging to the powder category showing smooth, round and uniform surface. The release of sodium naproxen was retarded by microencapsulation with Eudragit RS. The Eudragit RS microcapsules showed significantly increased AUC and MRT and deceased Cl/F in rabbits.

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Bending Behavior of Coated Yarns

  • Koo, Young-Seok
    • Fibers and Polymers
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    • 제2권3호
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    • pp.148-152
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    • 2001
  • Cotton yarns were coated with a polymer solution to hold surface fibers to the yam body, which caused fiber-fly generation during knitting process. The physical property of the coated yarn, especially a bending rigidity was investigated in order to evaluate the performance of the coated yam during knitting. SEM images showing the surface condition of the coated yarn demonstrated that the thickness of a coating material increased as the concentration of the coating solution increased. The results of the bending rigidity measured using KES-FB2 system showed that the bending rigidity of the coated yam increased as the concentration of the coating solution increased. The results also revealed the possibility that yarn coated with a low amount of coating material should be employed for further research of reducing fiber-fly generation during knitting process.

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黃酸溶液에서의 硬質陽極酸化에 關한 硏究 (Studies on the Hard Anodizing in Sulphuric Acid Solution)

  • 김종찬;박용진
    • 한국표면공학회지
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    • 제13권1호
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    • pp.8-15
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    • 1980
  • The critical voltage of hard coat range of Al alloys (K 186, 43S) at various electrolytes and the effects of voltage, temperature of electrolytes and concentration of sulfric acid were investigated, m the hope that to find the adequate voltage. Two kind of A1 alloys were anodized in three typical electrolytes and micro vickers hardness of the films were measured. With respect to the relationship between the hardness of the film and the voltage The result of this experiment are as fallows. 1. The critical voltage of hard coat rangs for the electrolytes $H_2SO_4\;10%,\;H_2SO_4\;10%\;+\;H_2C_2O_4\;2H_2O\;10g/l,\;H_2SO_4\;10%\;+\;NaHSO_4\;5%$ was 20V 22V 24V respectively. 2. $H_2SO_4\;10%\;+\;NaHSO_4$ 5% electrolyte was most adventageous among the three electrolyte in the respect of hardness. 3. The effect of concentration of sulphuric acid was not appeared.

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Corrosion Inhibition of Mild Steel in Acidic Medium by Jathropha Curcas Leaves Extract

  • Odusote, Jamiu K.;Ajayi, Olorunfemi M.
    • Journal of Electrochemical Science and Technology
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    • 제4권2호
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    • pp.81-87
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    • 2013
  • Inhibition of corrosion of mild steel in sulphuric acid by acidic extract of Jatropha Curcas leaves has been studied using weight loss and thermometric measurements. It was found that the leaves extract act as a good corrosion inhibitor for mild steel in all concentrations of the extract. The inhibition action depends on the concentration of the Jatropha Curcas leaves extract in the acid solution. Results for weight loss and thermometric measurements indicate that inhibition efficiency increase with increasing inhibitor concentration. The adsorption of Jatropha curcas leaves extract on the surface of the mild steel specimens obeys Langmuir adsorption isotherm. Based on the results, Jatropha curcas leaves extract is recommended for use in industries as a replacement for toxic chemical inhibitors.

노면퇴적물의 입자 크기에 따른 중금속 오염에 관한 연구 (A Study On Heavy Metal Contamination in the Different Size Fractions of Deposited Road Particles(DRPs))

  • 김부길;이병철
    • 한국환경과학회지
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    • 제15권12호
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    • pp.1171-1175
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    • 2006
  • Deposited road particles (DRPs) were analysed for heavy metal concentrations at four different roads in a city, Korea. The samples were collected using a roadway surface vacuum cleaning vehicle which was commonly used in collecting roadway surface particles. Six particle size ranges were analyzed separately for twelve heavy metal elements (Cd, Cr, Pb, Ni, Al, As, Co, Cu, Fe, Mn, Zn and Hg). At all sampling sites, the high concentration of the heavy metals occurred in the <74um particle size range, which conventional roadway cleaning vehicles do not remove efficiently. The Pb concentration significantly increased with decreasing particle size of DRPs, and other toxic heavy metals (Cd, Cr and Ni) also showed similar results. The heavy metal concentrations in the smaller size fraction of DRPs is important because they are contaminants that are preferentially transported by road runoff during rainfall.

$CaCO_3$침전능 조절에 의한 금속시편에서의 부식방지 (The Corrosion Control Using CCPP(Calcium Carbonate Precipitation Potential )Index in Metallic Coupons)

  • 이재인;임진경;서상훈;김동윤;신춘환
    • 한국환경과학회지
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    • 제9권6호
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    • pp.505-509
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    • 2000
  • The purpose of this study was to evaluate the effects of $Ca(OH)_2$ and $CO_2$ additions on the corrosion of metal coupons(ductile iron, galvanized steel, copper and stainless steel). Corrosion rate and released metal ion concentration of ductile iron and galvanized steel decreased by adjusting alkalinity, calcium hardness and pH with $Ca(OH)_2$ & $CO_2$ additions on copper and stainless steel were less than those on ductile iron and galvanized steel. When ductile iron coupon was exposed to water treated with Ca(OH)$_2$&$CO_2$, additions, the main components of corrosion product formed on its surface were $CaCO_3$ and $Fe_2 O_3 or Fe_2 O_4$ which often reduce the corrosion rate by prohibiting oxygen transport to the metal surface.

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rf 플라즈마 화학기상증착기의 제작 및 특성 (Characterization and Construction of Chemical Vapor Deposition by using Plasma)

  • 김경례;김용진;현준원;이기호;노승정;최병구
    • 한국표면공학회지
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    • 제33권2호
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    • pp.69-76
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    • 2000
  • The rf plasma chemical vapor deposition is a common method employed for diamond or amorphous carbon deposition. Diamond possesses the strongest bonding, as exemplified by a number of unique properties-extraordinary hardness, high thermal conductivity, and a high melting tempera tore. Therefore, it is very important to investigate the synthesis of semiconducting diamond and its use as semiconductor devices. An inductively coupled rf plasma CVD system for producing amorphous carbon films were developed. Uniform temperature and concentration profiles are requisites for the deposition of high quality large-area films. The system consists of rf matching network, deposition chamber, pumping lines for gas system. Gas mixtures with methane, and hydrogen have been used and Si (100) wafers used as a substrate. Amorphous carbon films were deposited with methane concentration of 1.5% at the process pressure of S torr~20 torr, and process temperature of about $750^{\circ}C$. The nucleation and growth of the amorphous carbon films have been characterized by several methods such as SEM and XRD.

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쵸크랄스키 단결정 장치에서의 실리콘유동 (Silicon melt motion in a Czochralski crystal puller)

  • 이재희;이원식
    • 한국결정성장학회지
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    • 제7권1호
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    • pp.27-40
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    • 1997
  • The heat in Czochralski method is transfered by all transport mechanisms such as convection, conduction and radiation and convection is caused by the temperature difference in the molden pool, the rotations of crystal or crucible and the difference of surface tension. This study delvelops the simulation model of Czochralski growth by using the finite difference method with fixed grids combined with new latent heat treatment model. The radiative heat transfer occured in the surfce of the system is treated by calculating the view factors among surface elements. The model shows that the flow is turbulent, therefore, turbulent modeling must be used to simulate the transport phenomena in the real system applied to 8" Si single crystal growth process. The effects of a cusp magnetic field imposed on the Czochralski silicon melt are studied by numerical analysis. The cusp magnetic field reduces the natural and forced convection due to the rotation of crystal and crucible very effectively. It is shown that the oxygen concentration distribution on the melt/crystal interface is sensitively controlled by the change of the magnetic field intensity. This provides an interesting way to tune the desired O concentration in the crystal during the crystal growing.

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석유증발법에 의한 Cobalt Oxide의 분말제조 (Preparation of the Cobalt Oxide Powder by Hot Petroleum Drying Method)

  • 윤상옥;정형진
    • 한국세라믹학회지
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    • 제24권3호
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    • pp.257-262
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    • 1987
  • The characteristics of cobalt oxide powders prepared by hot petroleum drying method from the cobalt acetate were evaluated by DTA/TGA, XRD, BET, SEM and density measurement. The cobalt oxide powder could be prepared by hot petroleum drying of the emulsion of cobalt acetate salt solution and the subsequent thermal decomposition of the acetate at 300$^{\circ}C$. As the concentration of the salt solution and the calcination temperature of the dried powder increased, the surface area of the synthesized powder decreased due to the particle growth, so that after sintering the density and grain size decreased. For the same concentration of the salt solution, the surface area and sinterability of the powder by hot petroleum drying increased in comparision with those by conventional drying.

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