• 제목/요약/키워드: Surface concentration

검색결과 6,117건 처리시간 0.035초

반응표면분석에 의한 만가닥 버섯의 추출조건 최적화 (Optimization of Extraction Conditions for Lyophyllum ulmarium by Response Surface Methodology)

  • 김현구;최맑음;김미옥;김공환
    • 한국식품영양과학회지
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    • 제32권4호
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    • pp.574-580
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    • 2003
  • 만가닥 버섯 추출물의 수율 및 전자공여작용, 총폴리페놀 함량, tyrosinase 저해작용, 갈색도, 아질산염 소거작용에 대하여 반응표면분석에 의해 추출조건을 최적화하였다. 만가닥 버섯의 경우 수율은 에탄올 농도에 가장 큰 영향을 받았으며, 전자공여작용의 경우 에탄올 농도가 높고 microwave power가 높은 조건에서 높은 추출률을 나타내었다. 갈변도 및 tyrosinase 저해작용의 경우 에탄을 농도가 증가할수록 microwave power가 증가할수록 더욱 크게 나타났다. 아질산염 소거 작용의 경우 에탄을 농도와 추출시간의 조건에 크게 영향을 받지 않는 것으로 판단되었으며 총 폴리페놀 함량은 에탄을 농도가 증가할수록 증가폭이 크고, microwave power가 증가할수록 추출물의 생리활성이 우수한 것으로 나타났다. 따라서 만가닥버섯의 최적 추출조건 범위는 microwave power 60.15~102.75 watt, ethanol 농도 53.20~64.01%, 추출시간 7.77분으로 예측되었다.

수소첨가반응용 니켈 폐촉매의 활성재생에 관한 연구 (II) (A Study on the Regeneration of Ni Catalyst for Hydrogenation(II))

  • 김정훈;이근대;이호인
    • 공업화학
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    • 제2권1호
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    • pp.47-55
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    • 1991
  • 탄소침적된 수소첨가반응용 Ni 촉매의 활성재생에 관하여 연구하였다. 침적된 탄소는 여러 가지 농도의 산소로 산화시켜 제거하였으며, 촉매의 활성은 아닐린 수소첨가반응을 model 반응으로 하여 측정하였다. 탄소침적된 촉매를 산화처리할 경우 처리온도가 증가함에 따라 표면적이 증가하다가 감소하는 현상을 보였으며, 최대 표면적을 나타내는 처리온도는 처리 산소농도가 감소함에 따라 증가하였다. 처리 산소농도가 높을수록 침적탄소의 산화에 의한 반응열로 인하여 Ni 입자의 소결현상 및 담체의 기공감소가 심하게 나타났다. 5 % 산소로 처리한 촉매의 경우, 촉매의 활성이 약 90% 까지 회복되었으나 20% 산소로 처리한 촉매의 경우, 활성의 회복을 기대할 수 없었다. 5 % 산소로 재생처리할 경우, 촉매의 활성은 산화처리 시간이 증가할수록 증가하였으나, 1 시간 이후에는 거의 일정하였다.

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알긴산 코팅에 의한 골판지 상자 제조용 라이너 원지의 수분저항성 증진 (Improvement of Water Resistant Properties of a Linerboard for Corrugated Fiberboard Box by Coating with Na-alginate)

  • 김은정;임종환;김병용
    • 한국식품과학회지
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    • 제38권6호
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    • pp.762-766
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    • 2006
  • 골판지 상자의 수분저항성을 증진시키기 위해 골판지 상자 제조에 사용되는 라이너지의 표면을 알긴산으로 표면코팅을 하기 위한 최적 조건을 결정하기 위하여 농도, 가소제의 종류와 사용량, 알긴산의 불용화를 위한 다가 금속이온의 종류와 최적농도 및 침지시간 등을 결정하였다. 라이너지의 표면코팅을 위한 알긴산의 농도는 2.5%(w/w)가 적합하였으며, 가소제인 글리세롤은 알긴산 대비 35%의 농도로 사용하는 것이 적합하였고, 알긴산 필름의 불용화를 위해서는 2% $CaCl_2$ 용약을 사용하여 3분간 처리하는 것이 라이너지의 수분에 대한 저항성 증진에 최적조건을 결정되었다. 다가 금속이온으로 $CA^{2+}$ 이외에 $Cu^{2+}$를 사용했을 때 낮은 투습계수와 수분용해도를 나타냈다. 가소재의 종류에 따라서는 수분 흡습에 대한 저항성이 큰 솔비톨을 첨가 했을 때 라이너지의 수분저항성이 유의적인 차이를 보이며 증가하였다.

Improvement of Anthocyanin Encapsulation Efficiency into Yeast Cell by Plasmolysis, Ethanol, and Anthocyanin Concentration Using Response Surface Methodology

  • Dong, Lieu My;Hang, Hoang Thi Thuy;Tran, Nguyen Huyen Nguyet;Thuy, Dang Thi Kim
    • 한국미생물·생명공학회지
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    • 제48권3호
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    • pp.267-275
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    • 2020
  • Anthocyanins are antioxidant compounds susceptible to environmental factors. Anthocyanin encapsulation into yeast cells is a viable solution to overcome this problem. In this study, the optimal factors for anthocyanin encapsulation were investigated, including anthocyanin concentration, plasmolysis contraction agent, and ethanol concentration, and response surface methodology was evaluated, for the first time. Anthocyanin from Hibiscus sabdariffa L. flowers was encapsulated into Saccharomyces cerevisiae using plasmolysis contraction agent (B: 3%-20% w/v), ethanol concentration (C: 3%-20% v/v), and anthocyanin concentration (A: 0.15-0.45 g/ml). The encapsulation yield and anthocyanin loss rate were determined using a spectrometer (520 nm), and color stability evaluation of the capsules was performed at 80℃ for 30 min. The results of the study showed that these factors have a significant impact on the encapsulation of anthocyanin, in which ethanol agents have the highest encapsulation yield compared to other factors in the study. Statistical analysis shows that the independent variables (A, B, C), their squares (A2, B2, C2), and the interaction between B and C have a significant effect on the encapsulation yield. The optimized factors were anthocyanin, 0.25 g/ml; NaCl, 9.5% (w/v); and ethanol, 11% (v/v) with an encapsulation yield of 36.56% ± 0.55% and anthocyanin loss rate of 15.15% ± 0.98%; This is consistent with the expected encapsulation yield of 35.46% and loss rate of 13.2%.

농업용 저수지 수질과 경험적 인자들과의 관계 (The Relationships Between Empirical Factors and Water Quality in Agricultural Reservoirs)

  • 김호섭;최은미;박주현;황하선;김범철;공동수;황순진
    • 한국물환경학회지
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    • 제24권3호
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    • pp.333-339
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    • 2008
  • This study was carried out to assay the relationships between empirical factors and water quality in 23 agricultural reservoirs. Based on the trophic state index (TSI) deviation analysis, phosphorus in type II and III was the primary limiting factor on algal growth. BOD, COD, TP and chl.a concentration in type III reservoirs showed higher concentration than those of other types, while SS and TN concentration was no noticeable difference among three types. Characteristics of type III reservoirs showed large reservoir surface and drainage area, large surface area to volume (SAV) ratio, small drainage area to reservoir area (DA/RA) ratio, relatively old age, large paddy field and upland field to drainage area ratio (Mean 17.4%) and high generation and discharge loads compared to other types of reservoirs. In type I and II reservoirs, trends of BOD, TN, TP concentration in water column, were similar to those of the discharge load of pollutants. Although type II reservoirs generally showed low phosphorus discharge loads compared to type I reservoirs, TP and chl.a concentration in water column was greater than that of type I. Characteristics of type II reservoirs showed relatively large SAV ratio and old age compared to type I reservoirs and was similar to those of type III including eutrophic reservoirs.

반응표면분석에 의한 산수유 추출물의 추출조건 최적화 (Optimization of Corni fructus Extracts by Response Surface Methodology)

  • 이혜진;도정룡;권중호;김현구
    • 한국식품영양과학회지
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    • 제41권3호
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    • pp.390-395
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    • 2012
  • 산수유의 추출조건별 추출물의 최적 추출조건을 설정하기 위해 중심합성법에 따라 마이크로웨이브에너지(30, 60, 90, 120 및 150 watt), 에탄올 농도(0, 25, 50, 75 및 100%), 추출시간별(1, 3, 5, 7 및 9분)로 추출조건에 따라 생리활성을 측정하였다. 이때 반응표면의 회귀식 $R^2$값이 전자공여작용, tyrosinase 저해효과, SOD 유사활성, 총 폴리페놀 함량에서 각각 0.8937, 0.9254, 0.9552와 0.9708로 분석되었다. 4차원 반응표면분석에 의해 superimposing 하여 최적 추출조건을 얻은 범위는 산수유의 경우 마이크로웨이브 에너지 78~98 watt, 에탄올 농도 3~33%, 추출시간 3.6~9분으로 예측되었다.

셀루라아제에 의한 면직물의 유연가공에 관한 연구 (A Study on Softening Finish of Cotton Fabric using Cellulase)

  • 강지연;류효선
    • 한국의류학회지
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    • 제14권4호
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    • pp.262-273
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    • 1990
  • The purpose of this study is to investigate the softening effect of cellulase-treated cotton fabric and the damage on the fabric which is accompanied by the treatemnt. Cotton fabric is treated with cellulase under various concentrations and time, and the weight loss, hand values (by KES), surface characteristics, moisture regain, tensile strength, copper number and intrinsic viscosity of the treated samples and untreated samples have been compared. The results are as follows: 1. The weight loss of cotton fabric increased as the concentration of cellulase and the treating time increased. 2. The enzyme treatment had little effect on the stiffness of the treated samples but anti- drape stiffness decreased for the treated samples. Fullness and softness of the treated samples increased and crispness decreased with the lowest level reaching after two hours of the treatment for all concentrations. Scrooping feeling of the treated samples increased and flexibility with soft feeling increased as the treating time and the concentration of cellulase increased. 3. Moisture regain of the samples decreased as the treating time and the concentration of the enzyme increased and the treated fabric showed cracks on the fiber surface, and much surface fibers on the fabric have been removed after the treatment. 4. Tensile strength of the samples decreased as the treating time and as the concentration of cellulase increased, and the copper number increased while the intrinsic viscosity decreased as the treating time increased, but cellulase concentration had a little effect.

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Optical analysis of low concentration evacuated tube solar collector

  • Teles, Mavd R.;Carvalho, Raquel;Ismail, Kamal A.R.
    • Advances in Energy Research
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    • 제5권3호
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    • pp.227-237
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    • 2017
  • The continuous increase of emission rates of green house gases and the effects on global warming added a new dimension to the problem of substituting the petroleum and its derivatives by environment friendly and sustainable energy sources for the world. Solar and wind energy appear at the top of the list of renewable of high potential, widely available, of dominated technology and well accepted. Brazil is one of the few countries in the world that receives number hours of sunshine exceeding 3,000 hours per year with a daily average of 4.5 to 6 kWh. However, this potential is largely unexplored and poorly tapped. The number of renewable systems implanted in Brazil has grown in recent years, but still insignificant when compared, for example, with Germany and Spain among others. This paper presents the results of an optical study on small concentration solar collector with evacuated tube enveloping the absorber and internal reflective surface fixed on the bottom part of the evacuated tube. The designed collector has a 2D geometrical concentration ratio between 2.455 and 4.91. The orientation of the solar collector, the ratio of the radius of the receiver to the radius of the absorber, the incidence angle for each period of the year, the collector inclination angle, the aperture angle of the reflective surface, concentration and optical efficiency were determined. The ray traces and flux distribution on the absorber of the evacuated tube solar collector were determined by using the program Ray Optics Simulation. The optical efficiency varies during the year according to the solar declination. For the periods were the solar declination is close to zero the efficiencies are maximum, and the variation during the day is around 25.88% and 99.9%. For the periods were the solar declination is maximum the efficiencies are minimum, and the variation during the day is around 23.78% and 91.79%.

쇄파대의 저질부유에 관한 현지관측 (Field observation of sediment suspension in the surf zone)

  • 신승호;율산서소
    • 한국항해항만학회:학술대회논문집
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    • 한국항해항만학회 2003년도 춘계공동학술대회논문집
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    • pp.141-146
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    • 2003
  • 저질의 부유 현상이 일련의 쇄파라고 하는 파동 현상에 어떠한 형태로 연동하는가를 면밀히 조사하기 위하여 현지해안의 쇄파대내에 주 관측지점을 설치하고 부유사 농도와 유속, 수위변동 등의 관련 파랑 제원을 계측하였다. 분석을 위해 수위변동, 유속변동치의 부유사농도에 대한 상관관계를 조사하였으며, 상관이 탁월한 주기대에 대한 ensemble 평균 분석으로 유속 및 수위변동의 위상에 따른 부유사 농도의 변화와의 관계를 명백히 하여 다음의 결론을 얻었다. 1) 부유사의 농도 변동은 유속 및 수위변동의 에너지가 가장 큰 장주기 성분(100s)에 있서 상관이 높았으며, 2) 또한, 1차mode의 장주기중복파의 유속 성분이 해안으로 향하여 가속하는 위상 즉, 수면 경사가 상대적으로 해안선측보다 외해측이 높은 위상에서 부유사 농도가 가장 높아짐을 명백히 하였다.

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Characteristics of electrodeposited bismuth telluride thin films with different crystal growth by adjusting electrolyte temperature and concentration

  • Yamaguchi, Masaki;Yamamuro, Hiroki;Takashiri, Masayuki
    • Current Applied Physics
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    • 제18권12호
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    • pp.1513-1522
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    • 2018
  • Bismuth telluride ($Bi_2Te_3$) thin films were prepared with various electrolyte temperatures ($10^{\circ}C-70^{\circ}C$) and concentrations [$Bi(NO_3)_3$ and $TeO_2:1.25-5.0mM$] in this study. The surface morphologies differed significantly between the experiments in which these two electrodeposition conditions were separately adjusted even though the applied current density was in the same range in both cases. At higher electrolyte temperatures, a dendrite crystal structure appeared on the film surface. However, the surface morphology did not change significantly as the electrolyte concentration increased. The dendrite crystal structure formation in the former case may have been caused by the diffusion lengths of the ions increasing with increasing electrolyte temperature. In such a state, the reactive points primarily occur at the tops of spiked areas, leading to dendrite crystal structure formation. In addition, the in-plane thermoelectric properties of $Bi_2Te_3$ thin films were measured at approximately 300 K. The power factor decreased drastically as the electrolyte temperature increased because of the decrease in electrical conductivity due to the dendrite crystal structure. However, the power factor did not strongly depend on the electrolyte concentration. The highest power factor [$1.08{\mu}W/(cm{\cdot}K^2$)] was obtained at 3.75 mM. Therefore, to produce electrodeposited $Bi_2Te_3$ films with improved thermoelectric performances and relatively high deposition rates, the electrolyte temperature should be relatively low ($30^{\circ}C$) and the electrolyte concentration should be set at 3.75 mM.