• Title/Summary/Keyword: Surface Contamination Level

검색결과 161건 처리시간 0.021초

Preparation of Styrene-Ethyl acylate Core-shell Structured Detection Materials for aMeasurement of the Wall Contamination by Emulsion Polymerization

  • Hwang, Ho-Sang;Seo, Bum-Kyoung;Lee, Dong-Gyu;Lee, Kune-Woo
    • 한국방사성폐기물학회:학술대회논문집
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    • 한국방사성폐기물학회 2009년도 학술논문요약집
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    • pp.84-85
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    • 2009
  • New approaches for detecting, preventing and remedying environmental damage are important for protection of the environment. Procedures must be developed and implemented to reduce the amount of waste produced in chemical processes, to detect the presence and/or concentration of contaminants and decontaminate fouled environments. Contamination can be classified into three general types: airborne, surface and structural. The most dangerous type is airborne contamination, because of the opportunity for inhalation and ingestion. The second most dangerous type is surface contamination. Surface contamination can be transferred to workers by casual contact and if disturbed can easily be made airborne. The decontamination of the surface in the nuclear facilities has been widely studied with particular emphasis on small and large surfaces. The amount of wastes being produced during decommissioning of nuclear facilities is much higher than the total wastes cumulated during operation. And, the process of decommissioning has a strong possibility of personal's exposure and emission to environment of the radioactive contaminants, requiring through monitoring and estimation of radiation and radioactivity. So, it is important to monitor the radioactive contamination level of the nuclear facilities for the determination of the decontamination method, the establishment of the decommissioning planning, and the worker's safety. But it is very difficult to measure the surface contamination of the floor and wall in the highly contaminated facilities. In this study, the poly(styrene-ethyl acrylate) [poly(St-EA)] core-shell composite polymer for measurement of the radioactive contamination was synthesized by the method of emulsion polymerization. The morphology of the poly(St-EA) composite emulsion particle was core-shell structure, with polystyrene (PS)as the core and poly(ethyl acrylate) (PEA) as the shell. Core-shell polymers of styrene (St)/ethyl acrylate (EA) pair were prepared by sequential emulsion polymerization in the presence of sodium dodecyl sulfate (SOS) as an emulsifier using ammonium persulfate (APS) as an initiator. The polymer was made by impregnating organic scintillators, 2,5-diphenyloxazole (PPO) and 1,4-bis[5-phenyl-2-oxazol]benzene (POPOP). Related tests and analysis confirmed the success in synthesis of composite polymer. The products are characterized by IT-IR spectroscopy, TGA that were used, respectively, to show the structure, the thermal stability of the prepared polymer. Two-phase particles with a core-shell structure were obtained in experiments where the estimated glass transition temperature and the morphologies of emulsion particles. Radiation pollution level the detection about under using examined the beta rays. The morphology of the poly(St-EA) composite polymer synthesized by the method of emulsion polymerization was a core-shell structure, as shown in Fig. 1. Core-shell materials consist of a core structural domain covered by a shell domain. Clearly, the entire surface of PS core was covered by PEA. The inner region was a PS core and the outer region was a PEA shell. The particle size distribution showed similar in the range 350-360 nm.

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타액에 의한 오염이 상아질 접착제의 미세전단결합강도에 미치는 영향 (EFFECT OF SALIVARY CONTAMINATION OF TEETH ON MICROTENSILE BOND STRENGTH OF VAR10US DENTIN BONDING SYSTEMS.)

  • 최경규;류길주
    • Restorative Dentistry and Endodontics
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    • 제28권3호
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    • pp.203-208
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    • 2003
  • The purpose of this study was to evaluate the effect of salivary contamination of teeth on bonding efficacy of self-priming and self-etching DBSs. The materials used were Single Bond(SB, self-priming system, 3M), Unifil Bond(UB, self-etching system, GC), and Scotchbond Multi-Purpose Plus(SM, 3M) as control. Forty five human molars randomly allocated to three groups as dentin bonding systems tested and embedded in epoxy resin. Then the specimens were wet-ground to expose flat buccal enamel surface or flat occlusal dentin surface and cut bucco-lingually to form two halves with slow speed diamond saw. One of them was used under non-contamination, other under contamination with saliva. The bonding procedure was according to the manufacturer's directions and resin composite(Z-100, 3M Dental Products, St. Paul, MN) was built-up on the bonded surface 5mm high. The specimens were ground carefully at the enamel-composite interface with fine finishing round diamond bur to create an hour-glass shape yielding bonded surface areas of $1.5{\pm}0.1\textrm{mm}^2$. The specimens were bonded to the modified microtensile testing apparatus with cyanoacrylate, attached to the universal testing machine and stressed in tension at a CHS of 1mm/min. The tensile force at failure was recorded and converted to a tensile stress(MPa). Mean values and standard deviations of the bond strength are listed in table. One-way ANOVA was used to determine significant difference at the 95% level. The bond strength of SBMP and SB were not affected by salivary contamination, but that of UB was significantly affected by salivary contamination. These results indicate that DBSs with total etch technique seems less likely affected by salivary contamination in bonding procedure.

여러 환경조건에 대한 고분자애자의 누설전류 특성 변화 (Variation in Leakage Current Characteristics of Polymer Insulator for Various Environmental Condition)

  • 박재준;최인혁;이동일
    • 한국전기전자재료학회논문지
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    • 제19권2호
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    • pp.169-175
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    • 2006
  • This study investigated variation leakage current maximum value and waveform considering applied voltage phase angel by simulating three environmental conditions, such as fog, salt fog, and kaolin contamination .As the result of applied voltage phase angel characteristics, leakage currents presented almost in phases in the early stage regardless of environmental conditions just after applying the voltage, and the phase of leakage currents certain phase lags for the discharge of the applied voltage when surface discharges occurred due to the continuous environmental contamination. In addition, the difference in phase significantly increased according to the intensity of discharges. The change in distortion rates according to the environmental contamination presented a nearly same level just after applying the voltage. The distortion rate of third harmonic for the fundamental wave presented by the order of fog>salt fog>kaolin when surface discharges occurred due to the applied voltage for certain continued periods. In the case of the fog and salt fog, the scale of spectrums decreased according to the increase in frequencies from the results of the analysis of high frequencies. In addition, the even number frequency presented a relatively large level compared to the odd number frequency under the kaolin contamination.

Post-CMP Cleaning에서 PVA 브러시 오염이 세정 효율에 미치는 영향 (Effect of PVA Brush Contamination on Post-CMP Cleaning Performance)

  • 조한철;유민종;김석주;정해도
    • 한국전기전자재료학회논문지
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    • 제22권2호
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    • pp.114-118
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    • 2009
  • PVA (polyvinyl alcohol) brush cleaning method is a typical cleaning method for semiconductor cleaning process especially post-CMP cleaning. PVA brush contacts with the wafer surface and abrasive particle, generating the contact rotational torque of the brush, which is the removal mechanism. The brush rotational torque can overcome theoretically the adhesion force generated between the abrasive particle and wafer by zeta potential. However, after CMP (chemical mechanical polishing) process, many particles remained on the wafer because the brush was contaminated in previous post-CMP cleaning step. The abrasive particle on the brush redeposits to the wafer. The level of the brush contamination increased according to the cleaning run time. After cleaning the brush, the level of wafer contamination dramatically decreased. Therefore, the brush cleanliness effect on the cleaning performance and it is important for the brush to be maintained clearly.

Si 기판에서 구리와 철 금속불순물의 제거에 대한 연구 (A Study on the Removal of Cu and Fe Impurities on Si Substrate)

  • 최백일;전형탁
    • 한국재료학회지
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    • 제8권9호
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    • pp.837-842
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    • 1998
  • ULSI급 소자의 집적도가 높아짐에 따라 공정의 신뢰도 및 수율 향상을 위한 세정 방법에 대한 관심이 더욱 높아지고 있다. 그중 가장 관심을 집중시키는 분야는 구리나 철과 같은 금속불순물의 제거에 관한 것이다. 본 연구에서는 금속 불순물 중 실제 공정에서 잘 오염되는 것으로 알려진 구리와 철 불순물을 인위적으로 오염시킨 후 $\textrm{H}_2\textrm{O}_2$와 HF의 혼합용액과 UV/$\textrm{O}_3$과 HF처리의 조합을 이용한 세정 방법을 이용하여 금속불순물을 제거하였다. 세정후 제정효과는 TXRF를 이용하여 측정하였고 Si 기판의 표면 거칠기를 AFM을 이용하여 측정하였다. 또한 금속 불순물의 흡착형태와 흡착기구 등을 SEM을 이용해 관찰하였고 AES를 이용하여 화학적 성분 분석을 실시하였다. 실험 결과 인위적 오염 후 구리의 오염도는 $\textrm{10}^{14}$ atoms/$\textrm{cm}^2$이었으며 각각의 세정을 통하여 $\textrm{10}^{10}$ atoms/$\textrm{cm}^2$으로 감소되었으며 반복된 세정으로 더욱 우수한 세정효과와 표면 거칠기의 개선 효과를 얻을 수 있었다. 구리는 박막의 형태가 아닌 구형의 입자 형태로 화학적 흡착에 의해 오염되는 것으로 관찰되었다. 철의 경우는 오염도가 $\textrm{10}^{13}$ atoms/$\textrm{cm}^2$ 이며 세정효과는 구리의 경우와 유사한 결과를 보여주었다. 철 불순물은 물리적 흡착에 의해 Si 표면에 오염되는 것으로 보이며 역시 구형의 입자형태로 표면에 흡착하는 것으로 관찰되었다.

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HACCP 적용을 위한 도계처리 공정내 미생물 오염의 분석 (Analysis of Microbial Contamination in Poultry Slaughtering Operations for the Application of HACCP)

  • 홍종해;권혁무;고주언
    • 한국환경보건학회지
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    • 제22권1호
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    • pp.45-50
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    • 1996
  • The application of HACCP system, which was adopted by Codex Alimentarius Committee for the safe meat and poultry production, is one of the urgent task for competing in the world trade markets. But there have been no useful analytical studies to identify the causes of contamination in the poultry meat processing plants in Korea. This study was conducted to investigate the potential hazards during the operations by the microbiological examination for the poultry meat processing plant (20,000 birds capacity a day) located in Kangwon province. In spite of air contamination of work places, it may not directly affect the surface contamination of poultry meats. But the risk of Campylobacter jejuni/coli contamination was high. The number of total count was decreased about ten times, but remarkable changes of microbial contamination could not be recognized in each procedure during the operations. The washing water was already contaminated as much as $10^{3-6}CFU/ml$ in SPC before the operations. It means that to keep water tanks hygienic is a primary step to prevent the occurrences of microbial contamination. The overflow and recirculation of water in scalding, washing, and chilling was aslo an important factor for a hygienic control. Based on this study, the followings could be regarded as an important factors for hygenic control in the poultry slaughtering plants on a small scale. The temperature of water used for scalding should be constantly maintained on a required temperature, and the overflow rate of 1~1.5 liter per bird. The carcass surface and the body cavity should be washed thoroughly and the cross-contamination due to facilities, workers, and tools should be prevented. The chilling water sholud be maintained under 5$\circ$C of temperature with ice and overflow, and residual chlorine level of 50 ppm.

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Film Cassette의 세균 오염도와 소독에 관한 연구 (A Study on Contamination and Disinfection of Film Cassette)

  • 권대철;정경모;최지원
    • 대한방사선기술학회지:방사선기술과학
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    • 제23권2호
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    • pp.55-61
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    • 2000
  • In July 2000, a bacteria infection on film cassette contact surface was examined at the diagnostic radiology department of the S. hospital. The objective of this study was to assess the contamination level on film cassette contact surface as a predictor of patient to prevent from nosocomial infection. The study showed that the laboratory result was identified non-pathologic bacterial in the four different cassette size of the contact surface. The study concludes that presence of a bacterial infection wilt prevent a using antiseptic technique on film cassette contact surface. Also the education of nosocomial infection for radiographer will be required.

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방사성옥소 치료환자의 환의 및 침구류에 대한 표면오염 측정에 관한 고찰 (A Study of Measuring the Surface Contamination for Patient's Clothes and Bedclothes after Ablation Therapy)

  • 문재승;박대성;김수근;정희일
    • 핵의학기술
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    • 제12권1호
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    • pp.3-12
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    • 2008
  • 목적: 방사성옥소 치료시 환자의 배설물(침, 소변)을 통해 표면 오염된 환의 및 침구류를 방사선 측정기로 측정하여 방사성 폐기물의 적정보관기간을 산출하고자 하였다. 대상 및 방법: 2005년도 8월부터 2006년 2월까지 방사성옥소 치료를 받은 환자 70명(남자: 12명, 여자: 58명)이 사용한 환의 및 침구류를 대조군(60 case)과 비대조군(10 case)으로 나누어 측정하였다. 결과: 세탁하지 않고 자체보관한 대조군과 세탁 후 자체 보관한 비대조군의 적정보관기간은 대조군 $44{\pm}16$일, 비대조군 $32{\pm}13$일으로 대조군과 비대조군의 보관기간에 있어서 유의미한 차이가 있는 것으로 나타났다(p<0.001). 환의 및 침구류에 대한 세탁전후의 표면오염도 제염효과는 평균 $83.66{\pm}15.15%$로 나타났으며, 오염 확산여부를 측정하기 위해 실시 된 결과에서 최초 표면오염 되지 않았던 환의에 미치는 영향은 미비하였다(p<0.05). 그러나 세탁과정 중에 발생된 세탁폐액에 대한 오염도는 최초 표면오염의 정도에 따라 허용표면 오염도 수준을 벗어난 것도 있었다. 결론: 표면 오염된 환의 및 침구류 전체를 방사선 측정기로 측정한 후 표면오염도의 정도에 따라 분류하고 적정 보관 기간이후 관리구역 밖으로 불출하는 것이 유용할 것이다.

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핵의학과 전용화장실에서 측정된 표면오염도 및 공간선량율에 대한 연구 (A Study on the Surface Contamination Level and Spatial Dose Rate Measured from NM Patients-Only Bathroom)

  • 문재승;정희일;정해성;신민용;김수근;박대성;김현기;김화산;이형남;안병필;이동호
    • 핵의학기술
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    • 제16권1호
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    • pp.38-43
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    • 2012
  • 목적 : $^{18}F$-FDG 방사성핵종이 투여된 환자가 사용하는 전용화장실의 표면오염도 및 공간선량율을 측정하여 같은 구역 내에 근무하고 있는 작업종사자들에 미치는 영향에 대하여 고찰해 보고자 한다. 대상 및 방법 : 2011년 1월부터 2011년 6월까지 $^{18}F$-FDG 370 MBq (10 mCi) 방사성핵종이 투여된 후 전용화장실을 1회 사용한 대상 환자는 본원이 60case(그룹1), 부천성모병원은 일평균 환자 수에 따라 50case(그룹2)와 10case(그룹3)으로 분류하였다. 방사선 측정기를 이용한 측정시간은 08:00, 10:00, 13:00, 15:00, 17:00이었으며 측정부위는 좌변기 4부위, 세면대, 휴지통이었다. 병원별 전용화장실의 3개월간 피폭누적량을 측정하였으며 PET/CT를 운영하는 병원을 대상으로 설문조사를 실시하여 전용화장실 유무 및 종사자들의 이용현황에 대하여 알아보았다. 결과 : 그룹1, 그룹2, 그룹3에 대한 일평균 환자 수는 $12.18{\pm}1.33$명, $6.62{\pm}2.21$명, $10.5{\pm}1.58$명이었다. 그룹1, 그룹2, 그룹3에 대한 좌변기의 평균 표면오염도($Bq/cm^2$)는 $8.38{\pm}4.56$, $2.64{\pm}3.90$, $4.59{\pm}4.38$로 그룹1에서의 표면오염도가 그룹2, 그룹3보다 높은 것으로 나타났으나($p$<0.05) 1 m 높이에서의 표면오염도 및 공간선량율에서는 그룹3, 그룹2, 그룹1순으로 높게 나타났다($p$<0.05). 그룹1에서의 세면대 및 휴지통의 표면오염도($Bq/cm^2$)는 $0.12{\pm}0.12$, $25.26{\pm}22.55$이었다. 표면오염도 수준을 단계별로 구분하여 제시하여 보았을 때 측정시간별 표면오염도 차이는 그룹1이 그룹2, 그룹3보다 높게 나타났다($p$<0.05). 개인피폭선량계를 이용하여 측정된 피폭누적량은 본원이 0.78 mSv/3개월, 부천성가병원이 0.37 mSv/3개월이었다. 전용화장실의 공동사용에 대한 설문조사에서 조사대상 31개 병원 중에 16.12%인 5개병원에서 환자와 함께 이용하는 것으로 나타났다. 결론 : 일평균 환자수가 많을수록 전용화장실의 표면오염도가 높아지는 것으로 나타났다. 특히 휴지통의 표면오염도는 원자력법에서 고시하고 있는 기준값인 $4Bq/cm^2$를 훨씬 초과한 것으로 나타났으나 화장실 전체공간에 대한 피폭누적량은 작게 나타났다. 설문조사 결과를 참조해 볼 때 환자들과 같이 사용하는 기관들이 있었음으로 전용화장실 이용에 대한 특별한 주의와 적절한 제염이 필요할 것으로 사료된다.

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소규모 돼지도축공정에서 도체오염 미생물의 변화 (Microbial change of pork carcass during processing in small size slaughterhouse)

  • 홍종해;이경환;이성모
    • 한국동물위생학회지
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    • 제25권1호
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    • pp.31-37
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    • 2002
  • Major hazards existed in slaughterhouse are pathogenic microorganisms originated from intestinal microflora of slaughtered animals. This study was intended for the identification of microbial contamination sources during pork slaughtering in small plants. Total aerobic bacteria, Coliform group, Salmonella spp, Listeria monocytogenes, and Campylobacter jejuni/coli were isolated from the surface sample of pork carcasses. Contamination level among different sampling points of ham, belly and neck did not showed statistical differences. Therefore, the mixed sampling from belly and neck of carcass could be effective for microbiological monitoring. Isolation rates of pathogenic microorganisms showed Salmonella spp 20.9%, Listeria monocytogenes 10.5%, and Campylobacter jejuni/coli 8.1% from 296 sampling points. High prevalence rate of Salmonella spp indicated that the contamination of intestinal microflora occurred due to unsanitary processing control, which required HACCP system in small plants. It was recommended that the prerequisite program should be a key factor for a successful HACCP system implementation especially in small size slaughterhouse.