• Korean Journal of Materials Research
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• v.31 no.12
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• pp.704-709
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• 2021

In the flux used in the batch galvanizing process, the effect of the component ratio of NH₄Cl to ZnCl₂ on the microstructure, coating adhesion, and corrosion resistance of Zn-Mg-Al ternary alloy-coated steel is evaluated. Many defects such as cracks and bare spots are formed inside the Zn-Mg-Al coating layer during treatment with the flux composition generally used for Zn coating. Deterioration of the coating property is due to the formation of AlCl_x mixture generated by the reaction of Al element and chloride in the flux. The coatability of the Zn-Mg-Al alloy coating is improved by increasing the content of ZnCl₂ in the flux to reduce the amount of chlorine reacting with Al while maintaining the flux effect and the coating adhesion is improved as the component ratio of NH₄Cl to ZnCl₂ decreases. Zn-Mg-Al alloy-coated steel products treated with the optimized flux composition of NH₄Cl·3ZnCl₂ show superior corrosion resistance compared to Zn-coated steel products, even with a coating weight of 60 %.

• Journal of Adhesion and Interface
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• v.23 no.1
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• pp.8-16
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• 2022

In this study, self-healable waterborne polyurethane (SH-WPU) as shoes and coating materials with self-healable disulfide functionalities was synthesized by mixing polyether polyol to impart excellent durability and heat resistance and polycarbonate polyol to impart excellent mechanical properties. The synthesized SH-WPU was characterized by fourier transform-infrared spectroscopy (FT-IR), and physical and self-healing properties were confirmed through universal testing machine (UTM) and scanning electron microscope (SEM) measurements. Tensile strength and hardness were increased and elongation was decreased by using polycarbonate polyol. In addition, as a result of comparison of thermal properties, thermal stability has been increased as the content of polycarbonate polyol increased. The healing efficiency showed the highest efficiency when poly(tetramethylene ether)glycol : polycarbonate polyol = 0.75 : 0.25, and it was confirmed that the damaged part was healed through surface observation using a microscope and SEM.

• Computers and Concrete
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• v.29 no.2
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• pp.107-115
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• 2022

With the improvements in computer technologies, utilization of image processing techniques has increased in many areas (such as medicine, defence industry, other industries etc.) Many different image processing techniques are used for surface analysis, detection of manufacturing defects, and determination of physical and mechanical characteristics of composite materials. In this study, cementitious composites were obtained by addition of Grounded Granulated Blast-Furnace Slag (GGBFS), Styrene Butadiene polymer (SBR), and Grounded Granulated Blast-Furnace Slag and Styrene Butadiene polymer together (GGBFS+SBR). Expanded Polystyrene (EPS) beads were added to these cementitious composites in different ratios (20%, 40% and 60%). The mechanical and physical characteristics of the composites were determined, and homogeneity indexes of the composites were determined by image processing techniques to determine EPS distribution forms in them. Physical and mechanical characteristics of the produced samples were obtained by applying consistency, density, water absorption, compressive strength (7 and 28 days), flexural strength (7 and 28 days) and tensile splitting strength (7 and 28 days) tests on them. Also, visual examination by using digital microscope, and image analysis by using image processing techniques with open source coded ImageJ program were performed. As a result of the study, it is determined that GGBFS and SBR addition strengthens the adhesion sites formed as it increases the adhesion power of the mixture and helps to get rid of the segregation problem caused by EPS. As a result of the image processing analysis it is demonstrated that GGBFS and SBR addition has positive contribution on homogeneity index.

• Composites Research
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• v.36 no.6
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• pp.441-447
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• 2023

Recently, as demand for high-strength, lightweight materials has increased, there has been great interest in joining with metals. In the case of mechanical bonding, such as bolting and riveting, chemical bonding using adhesives is attracting attention as stress concentration, cracks, and peeling occur. In this paper, surface treatment was performed to improve the adhesive strength, and the change in adhesive strength was analyzed. For the adhesive strength test were conducted with Carbon Fiber Reinforced Plastic(CFRP), CR340(Steel), and Al6061(Aluminum), and laser and plasma surface treatment were used. After plasma surface treatment, the adhesive strength improved by 7.3% and 39.2% in CFRP-CR340 and CFRP-Al6061, respectively. CR340-Al6061 was improved by 56.2% in laser surface treatment. Surface free energy(SFE) was measured by contact angle after plasma treatment, and it is thought that the adhesion strength was improved by minimizing damage through a chemical reaction mechanism. For laser surface treatment, it is thought that creates a rough bonding surface and improves adhesive strength due to the mechanical interlocking effect. Therefore, surface treatment is effect to improve adhesive strength, and based on this paper, the long-term fatigue test will be conducted to prevent fatigue failure, which is a representative cause of actual structural damage.

• Korean Journal of Veterinary Service
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• v.26 no.1
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• pp.67-71
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• 2003

A 8 months old, female domestic Shorthair cat with long-term signalment of anorexia, lacrimation, uveitis and coughing was submitted to the Pathology and Diagnosis Reference Division, NVRQS, Korea, for necropsy. Main gross lesions were characterized by ascities, some grayish-white nodular formation and fibrous adhesion on the surface of visceral organs including liver and kidney. Principle histopathological findings were fibrinous serositis, multifocal granuloma and necrosis, vasculitis, perivasculitis in various pharenchymal organs. Paraffin-embedded tissue sections taken from most of organs with granulomatous lesions were confirmed specific reaction to the monoclonal antibody of feline infectious peritonitis virus in the cytoplasm of many infiltrating macrophages by immunohistochemistry. The report was to describe the pathological lesions of the first naturally-occuring FIP case in companion cat of Korea.

• Tribology and Lubricants
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• v.22 no.6
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• pp.335-341
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• 2006

This paper reports the wear characteristics of two types of coating materials, which are $Cr_2O_3$ and $ZrO_2$, by coated plasma thermal spray method. The wear test was carried out under air, grease, and bearing fluid conditions. The wear testing machine of a pin-on disk type were used to measure friction forces, friction coefficients and the weight losses of the coating specimens on the various sliding velocity and loading condition. The wear surface of specimens were observed by scanning electron microscope (SEM) photographs.

• Proceedings of the KSR Conference
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• 2011.10a
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• pp.724-730
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• 2011

A turnout serves to switch train from one line to another. The turnout consists of a Point which is switchs the rail to induce direction, and a Crossing which is cross over two line on the plane surface, and a Lead where is middle section in Point to Crossing. Point machine, consists of a turnout, is important facilities in railway signal, that is safety issue relates in derailment of the train. Recently, train delay and accident frequently occurred because of the turnout include in a point machine trouble of electrical and mechanical. So in order to prevent train accident the research is advanced, install of normal and reverse indication lamp in a point machine, development of adherence detector for sensing the status of adhesion between the stock rails and tongue rails etc. In this paper investigates the problem which is connected with a turnout trouble, include in a point machine, occurrence at the time of train accident, and then proposed to the safety system model in order to prevent the train accident in turnout.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2009.11a
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• pp.123-123
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• 2009

In our experiment, a PTFE was sputter-coated on substrates to induce water-repellent properties and the RF-magnetron sputtering method for fabrication of PTFE film is used due to the advantages of the simple process, time saving, environmentally friendly, insulating property, and a good adhesion property to substrates. As a result of the correlation between surface roughness of PTFE films and contact angle with water, we found that the roughness surfaces are proportioned to contact angles related to low interfacial energy.

• Korean Journal of Computational Design and Engineering
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• v.20 no.3
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• pp.230-237
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• 2015

Soil deformation on the off-load ground is significantly affected by soil conditions, such as soil type, water content, and etc. Thus, the soil characteristics should be estimated for predicting vehicle movements on the off-load conditions. The plate-sinkage test, a widely-used experimental test for predicting the wheel-soil interaction, provides the soil characteristic parameters from the relationship between soil stress and plate sinkage. In this study, soil stress under the plate-sinkage situation is calculated by the DEM (Discrete Element Method) model. We developed a virtual soil bin with DEM to obtain the vertical reaction forces under the plate pressing the soil surface. Also parametric studies to investigate effects of DEM model parameters, such as, particle density, Young's modulus, dynamic friction, rolling friction, and adhesion, on the characteristic soil parameters were performed.

• Proceedings of the Korean Vacuum Society Conference
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• 2016.02a
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• pp.354.1-354.1
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• 2016

Nanoporous gold (NPG) is a very promising material in various fields such as sensor, actuator, and catalysis because of its high surface to volume ratio and conducting nature. In this study, we fabricated a NPG based amperometric sensor on a glass substrate by means of co-sputtering of Au and Si. During the sputtering process, we found the optimum conditions for heat treatment to reduce the residual stress and to improve adhesion between NPG films and the glass substrate. Subsequently, Si was selectively etched from Au-Si alloy by KOH solution, which forms nanoporous structures. Scanning electron microscopy (SEM) and auger electron spectroscopy (AES) were used to estimate the structure of NPG films and their composition. By employing appropriate heat treatments, we could make very stable NPG films. We tested the performance of NPG sensor with aniline molecules, which shows high sensitivity for sensing low concentration of aniline.