• Transactions of Materials Processing
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• v.19 no.6
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• pp.352-356
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• 2010

This paper was designed to fabricate the micro-spur gear by the LIGA and hybrid powder extrusion process. It is important to manufacture a micro-die with a high aspect ratio and determine appropriate extrusion conditions for a microforming. Ni has been used to fabricate micro-dies. LIGA process was capable to produce micro-extrusion dies with close tolerance, longer bearing length and adequate surface quality. Superplastic Al-78Zn powders have the great advantage in achieving deformation under low stresses and exhibiting good micro-formability with average strain rate raging from $10^{-3}$ to $10^{-2} s^{-1}$ and constant temperature ranging from 503 to 563K. Al-78Zn powders were compacted into a cylindrical shape ($\Phi3\times$h10mm) under compressive force of 10kN and, subsequently, the compacted powders were extruded by the hybrid powder extrusion process controlling of the temperature holing time for a improvement on formability of Al-22Zn powder. Micro-extrusion has succeeded in forming micro-gear shafts.

• Journal of the Korean Ceramic Society
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• v.47 no.3
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• pp.205-209
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• 2010

In the last (fourth) section, the discussion will entail a silicon-nitride/silicon-carbide nanocomposite, produced by pyrolysis of liquid polymer precursors, demonstrating one of the lowest creep rates reported so far in ceramics at the comparable temperature of $1400^{\circ}C$. This was first achieved by avoiding the oxynitride glass phase at the intergrain boundaries. One important factor in the processing of these nanocomposites was the use of the electrical field assisted sintering method.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.05a
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• pp.80-83
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• 2004

High temperature deformation behavior of AZ31 Mg alloy was investigated in this study on the basis of a processing map $(\varepsilon\approx0.6)$. To construct a processing map, compression tests were carried out at wide range of temperatures and strain rates $(T=250\~500^{\circ}C,\;\varepsilon=10^{-4}\~100/s)$. Two regions of high deformation efficiency $(\eta)$ were identified as: (1) a dynamic recrystalization (DRX) domain at $250^{\circ}C$ and 1/s and (2) a superplasticity domain at $450^{\circ}C$ and $10^{-4}/s$. Possible deformation mechanisms operating at high temperature were discussed in relation to the activation energy. A two-stage deformation method was found to be effective in enhancing the superplasticity of AZ31 Mg alloy. From the two-stage deformation method, tensile elongation of $1200\%$ was obtained at the superplastic domain.

• Korean Journal of Materials Research
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• v.30 no.2
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• pp.57-60
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• 2020

Titanium aluminides have attracted special interest as light-weight/high-temperature materials for structural applications. The major problem limiting practical use of these compounds is their poor ductility and formability. The powder metallurgy processing route has been an attractive alternative for such materials. A mixture of Ti and Al elemental powders was fabricated to a mechanical alloying process. The processed powder was hot pressed in a vacuum, and a fully densified compact with ultra-fine grain structure consisting of Ti₃Al intermetallic compound was obtained. During the compressive deformation of the compact at 1173 K, typical dynamic recrystallization (DR), which introduces a certain extent of grain refinement, was observed. The compact had high density and consisted of an ultra-fine equiaxial grain structure. Average grain diameter was 1.5 ㎛. Typical TEM micrographs depicting the internal structure of the specimen deformed to 0.09 true strain are provided, in which it can be seen that many small recrystallized grains having no apparent dislocation structure are generated at grain boundaries where well-developed dislocations with high density are observed in the neighboring grains. The compact showed a large m-value such as 0.44 at 1173 K. Moreover, the grain structure remained equiaxed during deformation at this temperature. Therefore, the compressive deformation of the compact was presumed to progress by superplastic flow, primarily controlled by DR.