• Title/Summary/Keyword: Sublimation technique

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MOCVD Deposition of AlN Thin Film for Packaging Materials

  • Chang-Kyu, Ahna;Seung-Chul Choi;Seong-Hoon Cho;Sung-Hwan Han;Je-Hong Kyoung
    • Proceedings of the International Microelectronics And Packaging Society Conference
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    • 2000.04a
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    • pp.118-118
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    • 2000
  • New single-source precursor, [AlCI3:NH2tBu] was synthesized for AlN thin f film processing with AICI3 (Aluminum Chloride) and tBuNH2 (tert-butylamine). AlN thin films for packaging aspplication were deposited on sapphire substrate by a atmosph하ie-pressure MOCVD. In most of other study methyl-based AI precursors w were used for source, But herein Aluminum Chloride was used for as AI source i in order to prevent the carbon contamination in the films and stabilize the p precursor. New precursor showed the very high gas vapor pressure so it allowed to m make the film under atmospheric-pressure and get the high purified film. High q quality AlN thin film was obtained at 700 to $900^{\circ}C$. The new precursor was p purified by a sublimation technique and help to fabricate high purity film. It s showed high vapor pressure, which is able to a critieal factor for the high purity a and atmospheric CVD of AlN. High Quality AIN thin film was obtained at $700-900^{\circ}C$. The AIN film was characterized by RBS

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Heat/Mass Transfer and Friction Characteristic in a Square Duct with Various Discrete Ribs -In-Lined Gap Arrangement Ribs- (덕트내 요철의 단락위치 변화에 따른 열/물질전달 및 압력강하 특성 - 정렬 단락배열 요철 -)

  • Lee, Sei-Young;Choi, Chung;Rhee, Dong-Ho;Cho, Hyung-Hee
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.25 no.11
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    • pp.1640-1649
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    • 2001
  • The present study investigates the effects of various rib arrangements on heat/mass transfer in the cooling passage of gas turbine blades. A complex flow structure occurs in the cooling passage with rib turbulators which promote heat transfer on the wall. It is important to increase not only the heat transfer rates but also the uniformity of heat transfer in the cooling passage. A numerical computation is performed using a commercial code to calculate the flow structures and experiments are conducted to measure heat/mass transfer coefficients using a naphthalene sublimation technique. A square channel (50 mm $\times$ 50 mm) with rectangular ribs (4 mm $\times$ 5 mm) is used fur the stationary duct test. The experiments focus on the effects of rib arrangements and gap positions in the discrete ribs on the heat/mass transfer on the duct wall. The rib angle of attack is 60°and the rib-to-rib pitch is 32 mm, that is 8 times of the rib height. With the inclined rib angle of attack (60°), the parallel rib arrangements make a pair of counter rotating secondary flows in the cross section, but the cross rib arrangements make a single large secondary flow including a small secondary vortex. These secondary flow patterns affect significantly the heat/mass transfer on the ribbed wall. The heat/mass transfer in the parallel arrangements is 1.5 ∼2 times higher than that in the cross arrangements. However, the shifted rib arrangements change little the heat/mass transfer from the inline rib arrangements. The gap position in the discrete rib affects significantly the heat/mass transfer because a strong flow acceleration occurs locally through the gap.

Heat/Mass Transfer on Effusion Plate with Circular Pin Fins for Impingement/Effusion Cooling System with Intial Crossflow (초기 횡방향 유동이 존재하는 충돌제트/유출냉각에서 원형핀이 설치된 유출면에서의 열/물질전달 특성)

  • Hong Sung Kook;Rhee Dong-Ho;Cho Hyung Hee
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.29 no.7 s.238
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    • pp.828-836
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    • 2005
  • Impingement/effusion cooling technique is used for combustor liner or turbine parts cooling in gas turbine engine. In the impingement/effusion cooling system, the crossflow generated in the cooling channel induces an adverse effect on the cooling performance, which consequently affects the durability of the cooling system. In the present study, to reduce the adverse effect of the crossflow and improve the cooling performance, circular pin fins are installed in impingement/effusion cooling system and the heat transfer characteristics are investigated. The pin fins are installed between two perforated plates and the crossflow passes between these two plates. A blowing ratio is changed from 0.5 to 1.5 for the fixed jet Reynolds number of 10,000 and five circular pin fin arrangements are considered in this study. The local heat/mass transfer coefficients on the effusion plate are measured using a naphthalene sublimation method. The results show that local distributions of heat/mass transfer coefficient are changed due to the installation of pin fins. Due to the generation of vortex and wake by the pin fin, locally low heat/mass transfer regions are reduced. Moreover, the pin fin prevents the wall jet from being swept away, resulting in the increase of heat/mass transfer. When the pin fin is installed in front of the impinging let, the blockage effect on the crossflow enhances the heat/mass transfer. However, the pin fin installed just behind the impinging jet blocks up the wall jet, decreasing the heat/mass transfer. As the blowing ratio increases, the pin fins lead to the higher Sh value compared to the case without pin fins, inducing $16\%{\~}22\%$ enhancement of overall Sh value at high blowing ratio of M=1.5.

Effect of Tip Gap Height on Heat/Mass Transfer over a Cavity Squealer Tip (팁간극높이가 전면스퀼러팁 표면의 열전달 특성에 미치는 영향)

  • Kang, Dong Bum;Moon, Hyun Suk;Lee, Sang Woo
    • The KSFM Journal of Fluid Machinery
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    • v.16 no.6
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    • pp.19-25
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    • 2013
  • The effect of tip gap height on heat/mass transfer characteristics on the floor of cavity squealer tip has been investigated in a turbine cascade for power generation by employing the naphthalene sublimation technique. The squealer rim height is chosen to be an optimal one of $h_{st}/c$ = 5.51% for the tip gap height-to-chord ratios of h/c = 1.0, 2.0, 3.0 and 4.0%. The results show that heat transfer on the cavity floor is strongly dependent upon the behavior of the cavity flow falling down onto the floor. For lower h/c, the floor heat transfer is influenced by the tip leakage flow falling down along the inner face of the suction-side squealer, whereas the floor heat transfer for higher h/c is augmented mainly due to the impingement of leakage flow on the floor near the leading edge. Compared to the plane tip surface heat transfer, the cavity floor heat transfer is less influenced by h/c. For h/c = 1.0%, the average thermal load is as low as a half of the plane tip surface one, and the difference in the thermal load between the two cases tends to decrease with increasing h/c.

Experimental Study on Local Convective Mass Transfer From a Circular Cylinder in Uniform Shear Flow (균일 전단류내에 있는 원봉주위의 국소 대류 물질 전달에 관한 실험적 연구)

  • 류명석;성형진;정명균
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.13 no.4
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    • pp.789-798
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    • 1989
  • A naphthalene sublimation technique based on the heat/mass transfer analogy is used to investigate the circumferential mass transfer from a circular cylinder in an approaching uniform shear flow. Experiments are performed in a wind tunnel (450*450m $m^{2}$ with a shear flow generator which is specially manufactured for generating variable shear rates(S). The effects of an approaching shear flow are correlated with mass transfer coefficients. It is found that the local mass transfer rate on a circular cylinder is characterized with the shear parameter $K^{d}$ defined as Sd/ $U^{c}$ , where d is the radius of cylinder and $U^{c}$ is the approaching velocity at the center of cylinder. The angle on the corresponding to minimum Sherwood number is approximately proportional to the shear parameter on an upper and down number is approximately proportional to the shear parameter on an upper and down circular cylinder (0< $K^{d}$ <0.132). Changes on the averaged mass transfer rate are not significant for small $K^{d}$ , which are slightly proportional to K$d^{2}$ but the local mass transfer rates are significantly changed with the approaching shear flow.

Effect of Vane/Blade Relative Position on Heat/Mass Transfer Characteristics on the Tip and Shroud for Stationary Turbine Blade (고정된 터빈 블레이드의 베인에 대한 상대위치 변화가 끝단면 및 슈라우드의 열/물질전달 특성에 미치는 영향)

  • Rhee Dong-Ho;Cho Hyung-Hee
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.30 no.5 s.248
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    • pp.446-456
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    • 2006
  • The effect of relative position of the stationary turbine blade for the fixed vane has been investigated on blade tip and shroud heat transfer. The local mass transfer coefficients were measured on the tip and shroud fur the blade fixed at six different positions within a pitch. A low speed stationary annular cascade with a single turbine stage was used. The chord length of the tested blade is 150 mm and the mean tip clearance of the blade having flat tip is 2.5% of the blade chord. A naphthalene sublimation technique was used for the detailed mass transfer measurements on the tip and the shroud. The inlet flow Reynolds number based on chord length and incoming flow velocity is fixed to $1.5{\times}10^5$. The results show that the incoming flow condition and heat transfer characteristics significantly change when the relative position of the blade changes. On the tip, the size of high heat/mass transfer region along the pressure side varies in the axial direction and the difference of heat transfer coefficient is up to 40% in the upstream region of the tip because the position of flow reattachment changes. On shroud, the effect of tip leakage vortex on the shroud as well as tip gap entering flow changes as the blade position changes. Thus, significantly different heat transfer patterns are observed with various blade positions and the periodic variation of heat transfer is expected with the blade rotation.

Effect of Free Stream Turbulence Intensity on Heat/Mass Transfer Characteristics Around a Film Cooling Hole (주유동의 난류강도가 막냉각홀 주위의 열/물질전달 특성에 미치는 영향)

  • 이동호;김병기;조형희
    • Journal of the Korean Society of Propulsion Engineers
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    • v.2 no.2
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    • pp.56-63
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    • 1998
  • The present study investigated local heat transfer characteristics around a film cooling hole with variations of free stream turbulence intensity The film cooling jet is injected through a single hole inclined at $30^{\cire}$ to the surface and laterally at $45^{\cire}$ for the blowing rates of 0.5, 1.0 and 2.0. Turbulence generating grids are used at upstream of the film cooling hole to change the turbulence intensity of free stream. Free stream turbulence intensity without grids is 0.5%. Two different turbulence generating grid is installed at different at locations upstream of the film cooling hole so that turbulence intensity of free stream varies from 3% to 10%. The naphthalene sublimation technique has been employed to determine local heat/ mass transfer coefficients. With low free stream turbulence intensity, heat/mass transfer augmented area by coolant or free stream is distinguished evidently. However, when free stream turbulence intensity is high, heat transfer is enhanced in all region and heat transfer enhanced regions are not clearly divided due to vigorous mixing of coolant and free stream. The peak values of heat/mass coefficients are decreased and the distributions of heat/mass transfer coefficients are more uniform with high turbulence intensity. The effect of turbulence intensity on heat transfer characteristics is more evident as blowing rate is higher.

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Studies on the Optical and the Electrical Characterization of Organic Electroluminescence Devices of Europium Complex Fabricated with PVD(Physical Vopor Deposition) Technique (진공 증착법에 의하여 제작한 Europium complex 유기 박막 전기발광소자의 광학적.전기적 특성에 관한 연구.)

  • Lee, Myeong-Ho;Lee, Han-Seong;Kim, Yeong-Gwan;Kim, Jeong-Su
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.48 no.5
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    • pp.285-295
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    • 1999
  • Electroluminescent(EL) devices based on organic materials have been of great interest due to their possible applications for large-area flat-panel displays. They are attractive because of their capability of multi-color emission, and low operation voltage. An approach to realize such device characteristics is to use active layers of lanthanide complexes with their inherent extremely sharp emission bands in stead of commonly known organic dyes. In general, organic molecular compounds show emission due to their $\pi$-$\pi*$ transitions resulting in luminescence bandwidths of about 80 to 100nm. Spin statistic estimations lead to an internal quantum efficiency of dye-based EL devices limited to 25%. On the contrary, the fluorescence of lanthanide complexes is based on an intramolecular energy transfer from the triplet of the organic ligand to the 4f energy states of the ion. Therefore, theoretical internal quantum efficiency is principally not limited. In this study, Powders of TPD, $Eu(TTA)_3(phen) and AlQ_3$ in a boat were subsequently heated to their sublimation temperatures to obtain the growth rates of 0.2~0.3nm/s. Organic electrolumnescent devices(OELD) with a structure of $glass substrate/ITO/Eu(TTA)_3(phen)/AI, glass substrate/ITO/TPD/Eu(TTA)_3(phen)/AI and glass substrate/ITO/TPD/Eu(TTA)_3(phen)/AIQ_3AI$ structures were fabricated by vacuum evaporation method, where aromatic diamine(TPD) was used as a hole transporting material, $Eu(TTA)_3(phen)$ as an emitting material, and Tris(8-hydroxyquinoline)Aluminum$(AlQ_3)$ as an electron transporting layer. Electroluminescent(EL) and current density-voltage(J-V) characteristics of these OELDs with various thickness of $Eu(TTA)_3(phen)$ layer were investigated. The triple-layer structure devices show the red EL spectrum at the wavelength of 613nm, which is almost the same as the photoluminescent(PL) spectrum of $Eu(TTA)_3(phen)$.It was found from the J-V characteristics of these devices that the current density is not dependent on the applied field, but on the electric field.

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Convergence of Korean Traditional Dance and K-Pop Dance : An Analysis of Comments on 2018 MMA BTS 'IDOL' Videos on YouTube (한국 전통춤과 K-pop 댄스의 융합 : 2018 MMA 방탄소년단 'IDOL' 유튜브 댓글 분석)

  • Yoo, Ji-Young;Kim, Mi-Kyung
    • Journal of Korea Entertainment Industry Association
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    • v.13 no.8
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    • pp.189-198
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    • 2019
  • This study aims to make meaning of the reactions of the Korean people through the text mining of comments on videos of the December 2018 MMA performance of intro on YouTube. For this, comments on 15 YouTube videos were collected over the past 10 months. With the collected data, a total of 5,135 comments were analyzed through crawling using the Python and BeautifulSoup programs, data was refined over a total of 3 sessions, and a final total of 5,080 comments were used as analysis material. A mining technique was used for data analysis and the process of refinement, analysis, and visualization was achieved using the Textom program. Research results showed that keyword analysis showed the keywords of 'performance', 'Korea', 'video', 'top', 'cool', 'dance', 'idol', 'legend', 'love', and 'gratitude' in that order and keywords such as 'patriotism' and 'Olympics' also appeared frequently. N-gram analysis showed that comments with contexts such as 'a top performance that will remain a legend among Korean idol performances', and 'an idol performance that displayed the traditional culture of Korea' were in higher ranks. Based on such keyword analysis results, topic modeling was applied and 5 top keywords were extracted from a total of 5 topics. Analysis results of topic contents and distribution showed that topics in the comments of this performance's videos largely consisted of the 3 reactions of 'high praise regarding the stage performance', 'affection towards the fusion and artistic sublimation of Korean traditional dance', and 'gratitude towards the uploading of cool dance videos'