• Title/Summary/Keyword: Structure refinement

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Grain Refinement of Mg-5wt%Zn Alloy by Rapid Solidification Process (급냉응고에 의한 Mg-5wt%Zn 합금의 결정립 미세화)

  • Kim, Yeon-Wook;Lee, Eun-Jong;Hur, Bo-Young
    • Journal of Korea Foundry Society
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    • v.17 no.3
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    • pp.302-308
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    • 1997
  • In spite of the fact that magnesium has low density and good machinability, its applications are restricted as a structural engineering material because of the poor strength, ductility, and corrosion resistance of the conventional ingot metallurgy alloys. Such properties can be improved by microstructural refinement via rapid solidification processing. In this study, Mg-5wt%Zn alloys have been produced as continuous strips by the melt overflow technique. In order to evaluate the influence of the cooling rate on the grain refinement and mechanical properties, seven different thickness strips were produced by means of controlling the speed of the cooling wheel. Then the microstructual observations were undertaken with the objective of evaluating the grain refinement as function of the cooling rate. The tremendous increase in hardness of Mg-Zn alloy was mainly due to the refinement of the grain structure by the effect of rapid solidification. The formation of intermetallic phases on the grain boundaries may have a positive effect on the corroion resistance. Therefore, despite competition from many other developments, the rapid solidification process emerges as a valuable method to develop superior and commercially acceptable magnesium alloys.

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Chemistry and Rietveld Structure Refinement of Nb-rich Perovskite, $Ca_2NbFe^{3+}O_6$ (네오비움 페롭스카이트($Ca_2NbFe^{3+}O_6$)의 화학조성 및 리트벨트 구조분석 연구)

  • ;Frank C. Hawthorne
    • Journal of the Mineralogical Society of Korea
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    • v.15 no.1
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    • pp.59-68
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    • 2002
  • Chemical analyses and Rietveld structural refinement with powder X-ray diffraction data were done for Nb-rich perovskite, named latrappite ($Ca_2NbFe^{3+}O_6$)from the Oka, Quebec, Canada. Latrappite is shown to be a member of a continuous solid solution of $CaTiO_3-NaNbO_3-Ca_2NbFe^{3+}O_6$ and approximately $(Ca_{1.5}Na_{0.4})\;(Nb_{0.1}Ti_{0.6}Fe_{0.4})O_6$ in composition. The crystal structure of latrappite, determined by Rietveld refinement, is similar to that of perovskite ($CaTiO_3$). It differs in that replacement of Ti by Nb and $Fe^{3+}$ results in greater distortion and tilting of the $TiO_6$ framework octahedra relative to $CaTiO_3$. Revised unit-cell parameters of latrappite are a=5.4474(4), b=5.5264(4), c=7.7519(5) ${\AA},\;V=233.4(3){\AA}^3$ space group Pbnm.

The Study on the Unidirectionally Solidified $Al-CuAl_2$ Eutectic Composites;Effect of Vibration on the Lamellar Spacing and Fault Density (일방향 응고한 $Al-CuAl_2$ 공정복합재료에 관한 연구;층상간격과 결함밀도에 미치는 응고조건과 진동의 영향)

  • Lee, Kil-Hong;Lee, Hyun-Kyu
    • Journal of Korea Foundry Society
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    • v.17 no.2
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    • pp.188-194
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    • 1997
  • The effects of solidification condition and vibration on structure refinement were investigated for unidirectionally solidified $Al-CuAl_2$ eutectic composites. Eutectic composites were unidirectionally solidified under vibration with different growth rates (R) and thermal gradient(G). The lamellar structure was varied according to growth condition (G/R ratio). For the structure refinement the effect of G/R was found out to be greater than that of vibration. The interlamellar spacing(${\lambda}$) in this materials was varied with the growth rates(R) with "${\lambda}^2R$=Constant" relationship.

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Grain Structure Analysis in Rolled 1050 Al Alloy Sheets Using EBSD (EBSD에 의한 A1050 압연판재의 결정립 구조 분석)

  • Han, Jun-Hyun;Shin, Myung-Chul
    • Analytical Science and Technology
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    • v.14 no.1
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    • pp.50-58
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    • 2001
  • The effect of cryogenic heavy rolling method on grain refinement has been studied and compared with those obtained by previous methods of cryogenic rolling and heavy rolling developed separately. Both grain structure and grain size were analyzed using electron back scattered diffraction (EBSD), which can distinguish grains each other by means of crystallographic misorientations between them. The cryogenic rolling and heavy rolling exhibit reduction in grain size of 39% and 87%, respectively, and the cryogenic heavy rolling shows reduced grain size similar to that observed in the heavy rolling. The heavy rolling was proved more effective in grain size refinement than the cryogenic rolling.

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The Structure Determination of La2/3-xLi3x1/3-2xTiO3 by the Powder Neutron and X-ray Diffraction

  • Kang, Eun-Tae;Kwon, Young-Jean
    • Journal of the Korean Ceramic Society
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    • v.40 no.6
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    • pp.513-518
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    • 2003
  • La/sub 2/3-x/Li/sub 3x/□/sub 1/3-2x/TiO₃ compounds with x=0.13 and 0.12 were prepared by slow cooling (x=0.13) and rapid quenching (x=0.12) into the liquid nitrogen after sintering at 1350℃ for 6 h. Their crystal structure has been determined by Rietveld refinement of both the powder neutron and X-ray diffraction data. From neutron diffraction data, we found that the main phase was not tetragonal (P4/mmm), but trigonal (R3cH). The refinement of neutron diffraction for the slow cooled samples were in a good agreement with a new model; a mixture of trigonal (R3cH, 45.7 wt%), tetragonal (p4/mmm, 37.0 wt%), and Li/sub 0.57/Ti/sub 0.86/O₂(pbnm, 17.2 wt%), but the quenched sample was found not to contain tetragonal (p4/mmm). X-ray diffraction data couldn't be well fitted because of the Poor scattering factor of lithium ions and the similar reflection patterns among trigonal (R3cH), tetragonal (p4/mmm), and cubic (Pm3m). We also knew that one transport bottlenecks is destroyed by one La vacancy in the case of trigonal (R3cH).

LiDAR Image Segmentation using Convolutional Neural Network Model with Refinement Modules (정제 모듈을 포함한 컨볼루셔널 뉴럴 네트워크 모델을 이용한 라이다 영상의 분할)

  • Park, Byungjae;Seo, Beom-Su;Lee, Sejin
    • The Journal of Korea Robotics Society
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    • v.13 no.1
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    • pp.8-15
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    • 2018
  • This paper proposes a convolutional neural network model for distinguishing areas occupied by obstacles from a LiDAR image converted from a 3D point cloud. The channels of a LiDAR image used as input consist of the distances to 3D points, the reflectivities of 3D points, and the heights of 3D points from the ground. The proposed model uses a LiDAR image as an input and outputs a result of a segmented LiDAR image. The proposed model adopts refinement modules with skip connections to segment a LiDAR image. The refinement modules with skip connections in the proposed model make it possible to construct a complex structure with a small number of parameters than a convolutional neural network model with a linear structure. Using the proposed model, it is possible to distinguish areas in a LiDAR image occupied by obstacles such as vehicles, pedestrians, and bicyclists. The proposed model can be applied to recognize surrounding obstacles and to search for safe paths.

Application Examples Applying Extended Data Expression Technique to Classification Problems (패턴 분류 문제에 확장된 데이터 표현 기법을 적용한 응용 사례)

  • Lee, Jong Chan
    • Journal of the Korea Convergence Society
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    • v.9 no.12
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    • pp.9-15
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    • 2018
  • The main goal of extended data expression is to develop a data structure suitable for common problems in ubiquitous environments. The greatest feature of this method is that the attribute values can be represented with probability. The next feature is that each event in the training data has a weight value that represents its importance. After this data structure has been developed, an algorithm has been devised that can learn it. In the meantime, this algorithm has been applied to various problems in various fields to obtain good results. This paper first introduces the extended data expression technique, UChoo, and rule refinement method, which are the theoretical basis. Next, this paper introduces some examples of application areas such as rule refinement, missing data processing, BEWS problem, and ensemble system.

Effects of the Processing Temperature and the Number of Passes of Equal Channel Angular Pressing on the Microstructure and Hardness of IF Steel (IF강의 미세조직과 경도에 미치는 ECAP 가공온도와 가공횟수의 효과)

  • Yoon, S.C.;Ryu, W.S.;Baik, S.C.;Kim, H.S.
    • Transactions of Materials Processing
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    • v.16 no.5 s.95
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    • pp.406-411
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    • 2007
  • The microstructure and the hardness of interstitial free steel processed by equal channel angular pressing (ECAP) was investigated experimentally. ECAP processing of route A and route C was compared with regard to grain refinement by transmission electron micrographs. Micro hardness evolution was correlated with the gram structure produced by ECAP. Especially, the effects of the ECAP processing temperature and the number of processing passes were discussed in terms of grain refinement.